SE9403779L - Ways to precipitate transition metals and alkaline earth metals from bleaching liquids by adding a sulfide and carbonate-containing liquid - Google Patents

Ways to precipitate transition metals and alkaline earth metals from bleaching liquids by adding a sulfide and carbonate-containing liquid

Info

Publication number
SE9403779L
SE9403779L SE9403779A SE9403779A SE9403779L SE 9403779 L SE9403779 L SE 9403779L SE 9403779 A SE9403779 A SE 9403779A SE 9403779 A SE9403779 A SE 9403779A SE 9403779 L SE9403779 L SE 9403779L
Authority
SE
Sweden
Prior art keywords
metals
carbonate
chelate
chelating agent
solution
Prior art date
Application number
SE9403779A
Other languages
Swedish (sv)
Other versions
SE504424C2 (en
SE9403779D0 (en
Inventor
Olle Wennberg
Original Assignee
Kvaerner Pulping Tech
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kvaerner Pulping Tech filed Critical Kvaerner Pulping Tech
Priority to SE9403779A priority Critical patent/SE504424C2/en
Publication of SE9403779D0 publication Critical patent/SE9403779D0/en
Priority to BR9509570A priority patent/BR9509570A/en
Priority to AT95936828T priority patent/ATE197614T1/en
Priority to CA002203392A priority patent/CA2203392A1/en
Priority to PCT/SE1995/001281 priority patent/WO1996014467A1/en
Priority to PT95936828T priority patent/PT803008E/en
Priority to ES95936828T priority patent/ES2153904T3/en
Priority to EP95936828A priority patent/EP0803008B1/en
Priority to DE69519441T priority patent/DE69519441T2/en
Publication of SE9403779L publication Critical patent/SE9403779L/en
Publication of SE504424C2 publication Critical patent/SE504424C2/en
Priority to US08/850,737 priority patent/US6024833A/en

Links

Classifications

    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C11/00—Regeneration of pulp liquors or effluent waste waters
    • D21C11/0021—Introduction of various effluents, e.g. waste waters, into the pulping, recovery and regeneration cycle (closed-cycle)
    • D21C11/0028—Effluents derived from the washing or bleaching plants
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C11/00—Regeneration of pulp liquors or effluent waste waters
    • D21C11/0064—Aspects concerning the production and the treatment of green and white liquors, e.g. causticizing green liquor
    • D21C11/0078—Treatment of green or white liquors with other means or other compounds than gases, e.g. in order to separate solid compounds such as sodium chloride and carbonate from these liquors; Further treatment of these compounds
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S210/00—Liquid purification or separation
    • Y10S210/928—Paper mill waste, e.g. white water, black liquor treated

Landscapes

  • Paper (AREA)
  • Removal Of Specific Substances (AREA)
  • Heat Treatment Of Water, Waste Water Or Sewage (AREA)
  • Detergent Compositions (AREA)

Abstract

Provided is a process for removing metals from a bleaching plant spent liquor and recovering a chelating agent which includes the steps of: heating a spent liquor containing a chelate comprising metals bound in a chelating agent to a temperature of at least about 140 DEG C. to break bonds in the chelate and release metals from the chelate; increasing the content of at least one of carbonate or sulphide in an alkaline material comprising at least one of green liquor or white liquor to form a carbonate or sulphide enhanced alkaline material; contacting the heated spent liquor with the alkaline material to form a solution containing precipitated metals, wherein the alkaline material is added in an amount sufficient to precipitate a majority of the released metals out of the solution; filtering the solution to separate the precipitated metals from the solution and form a filtrate containing recovered chelating agent; and supplying at least a portion of the recovered chelating agent to a chelating washing stage in a bleaching plant to bond with metals released from pulp and form a chelate. Also provided is a method of reducing encrustations.
SE9403779A 1994-11-04 1994-11-04 Ways to precipitate transition metals and alkaline earth metals from bleaching liquids by adding alkaline liquid SE504424C2 (en)

Priority Applications (10)

Application Number Priority Date Filing Date Title
SE9403779A SE504424C2 (en) 1994-11-04 1994-11-04 Ways to precipitate transition metals and alkaline earth metals from bleaching liquids by adding alkaline liquid
DE69519441T DE69519441T2 (en) 1994-11-04 1995-10-31 METHOD FOR SEPARATING TRANSITIONAL METALS AND EARTH ALKALINE METALS FROM WHITE WASTE WATER
PCT/SE1995/001281 WO1996014467A1 (en) 1994-11-04 1995-10-31 Method of precipitating transition metals and alkaline earth metals from bleach plant effluents
AT95936828T ATE197614T1 (en) 1994-11-04 1995-10-31 METHOD FOR THE SEPARATION OF TRANSITION METALS AND ALKALINE EARTH METALS FROM BLEACHING WASTEWATER
CA002203392A CA2203392A1 (en) 1994-11-04 1995-10-31 Method of precipitating transition metals and alkaline earth metals from bleach plant effluents
BR9509570A BR9509570A (en) 1994-11-04 1995-10-31 Process for precipitation of transition metals and / or alkaline earth metals from spent liquor from bleaching section
PT95936828T PT803008E (en) 1994-11-04 1995-10-31 METHOD FOR PRECIPITATING ALKALINE-TERROSAL TRANSIENT METALS AND METALS FROM EFFLUENTS OF A BLEACHING INSTALLATION
ES95936828T ES2153904T3 (en) 1994-11-04 1995-10-31 PROCEDURE FOR PRECIPITATING TRANSITION METALS AND ALKALINOTERREAL METALS OF EFFLUENTS OF A WHITENING INSTALLATION.
EP95936828A EP0803008B1 (en) 1994-11-04 1995-10-31 Method of precipitating transition metals and alkaline earth metals from bleach plant effluents
US08/850,737 US6024833A (en) 1994-11-04 1997-05-02 Process for removing metals and recovering a chelating agent from a bleach plant waste liquor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SE9403779A SE504424C2 (en) 1994-11-04 1994-11-04 Ways to precipitate transition metals and alkaline earth metals from bleaching liquids by adding alkaline liquid

Publications (3)

Publication Number Publication Date
SE9403779D0 SE9403779D0 (en) 1994-11-04
SE9403779L true SE9403779L (en) 1996-05-05
SE504424C2 SE504424C2 (en) 1997-02-10

Family

ID=20395847

Family Applications (1)

Application Number Title Priority Date Filing Date
SE9403779A SE504424C2 (en) 1994-11-04 1994-11-04 Ways to precipitate transition metals and alkaline earth metals from bleaching liquids by adding alkaline liquid

Country Status (10)

Country Link
US (1) US6024833A (en)
EP (1) EP0803008B1 (en)
AT (1) ATE197614T1 (en)
BR (1) BR9509570A (en)
CA (1) CA2203392A1 (en)
DE (1) DE69519441T2 (en)
ES (1) ES2153904T3 (en)
PT (1) PT803008E (en)
SE (1) SE504424C2 (en)
WO (1) WO1996014467A1 (en)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SE9603029D0 (en) * 1996-08-20 1996-08-20 Svenska Traeforskningsinst Method for lowering the level of oxalic acid
SE511794C2 (en) * 1997-06-30 1999-11-29 Sunds Defibrator Ind Ab Ways to reduce the content of calcium in the liquid phase in a pulp suspension
SE9803384L (en) * 1998-03-02 1999-09-03 Kemira Kemi Ab Process for treating process water
SE522436C2 (en) 1998-05-26 2004-02-10 Andritz Oy Procedure for preventing contamination of heat transfer surfaces in a multi-stage evaporation plant for black liquor and bleaching emissions
US20070000628A1 (en) * 2005-06-30 2007-01-04 Sealey James E Ii Method for removal of metals from a bleach plant filtrate stream

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SE417114B (en) * 1977-07-25 1981-02-23 Mo Och Domsjoe Ab PROCEDURE FOR PREVENTION OF INSTRUCTIVE EDUCATION IN CELLULOS FACTORIES
DE2834259A1 (en) * 1978-08-04 1980-02-28 Dsi Sportartikel Ski-stock clamping device - is made from elongated shaped plastics material forming stay with two legs holding two ski-stocks in parallel
ES2038097T5 (en) * 1989-06-06 2001-05-01 Eka Chemicals Ab PROCEDURE FOR WHITENING PAPER PASTES CONTAINING LIGNOCELLULOSE.
AT395028B (en) * 1990-02-07 1992-08-25 Chemiefaser Lenzing Ag METHOD FOR CHLORINE-FREE BLEACHING OF FIBER FIBER
US5509999A (en) * 1993-03-24 1996-04-23 Kamyr, Inc. Treatment of bleach plant effluents
SE9301161L (en) * 1993-04-07 1994-10-08 Sunds Defibrator Ind Ab Process for treating process water
SE501613C2 (en) * 1993-08-03 1995-03-27 Kvaerner Pulping Tech Method of integrating bleaching and recycling in pulp production

Also Published As

Publication number Publication date
ATE197614T1 (en) 2000-12-15
CA2203392A1 (en) 1996-05-17
PT803008E (en) 2001-04-30
DE69519441D1 (en) 2000-12-21
EP0803008B1 (en) 2000-11-15
SE504424C2 (en) 1997-02-10
SE9403779D0 (en) 1994-11-04
ES2153904T3 (en) 2001-03-16
US6024833A (en) 2000-02-15
DE69519441T2 (en) 2001-06-21
EP0803008A1 (en) 1997-10-29
BR9509570A (en) 1997-09-16
WO1996014467A1 (en) 1996-05-17

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Legal Events

Date Code Title Description
NUG Patent has lapsed