SE538488C2 - Method for thermal treatment of raw materials comprising lignocellulose - Google Patents

Method for thermal treatment of raw materials comprising lignocellulose Download PDF

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Publication number
SE538488C2
SE538488C2 SE1451097A SE1451097A SE538488C2 SE 538488 C2 SE538488 C2 SE 538488C2 SE 1451097 A SE1451097 A SE 1451097A SE 1451097 A SE1451097 A SE 1451097A SE 538488 C2 SE538488 C2 SE 538488C2
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SE
Sweden
Prior art keywords
gas
organic material
drying
chamber
organic
Prior art date
Application number
SE1451097A
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English (en)
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SE1451097A1 (en
Inventor
Åbyhammar Tomas
Original Assignee
Tomas Åbyhammar Med Enskild Firma Scandry
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Application filed by Tomas Åbyhammar Med Enskild Firma Scandry filed Critical Tomas Åbyhammar Med Enskild Firma Scandry
Priority to SE1451097A priority Critical patent/SE538488C2/sv
Priority to PCT/SE2015/050967 priority patent/WO2016043651A1/en
Priority to EP15841547.1A priority patent/EP3194536B1/en
Publication of SE1451097A1 publication Critical patent/SE1451097A1/sv
Publication of SE538488C2 publication Critical patent/SE538488C2/sv

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10B—DESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
    • C10B53/00—Destructive distillation, specially adapted for particular solid raw materials or solid raw materials in special form
    • C10B53/02—Destructive distillation, specially adapted for particular solid raw materials or solid raw materials in special form of cellulose-containing material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10B—DESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
    • C10B57/00—Other carbonising or coking processes; Features of destructive distillation processes in general
    • C10B57/02—Multi-step carbonising or coking processes
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10B—DESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
    • C10B57/00—Other carbonising or coking processes; Features of destructive distillation processes in general
    • C10B57/08—Non-mechanical pretreatment of the charge, e.g. desulfurization
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10B—DESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
    • C10B57/00—Other carbonising or coking processes; Features of destructive distillation processes in general
    • C10B57/08—Non-mechanical pretreatment of the charge, e.g. desulfurization
    • C10B57/10—Drying
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10K—PURIFYING OR MODIFYING THE CHEMICAL COMPOSITION OF COMBUSTIBLE GASES CONTAINING CARBON MONOXIDE
    • C10K1/00—Purifying combustible gases containing carbon monoxide
    • C10K1/32—Purifying combustible gases containing carbon monoxide with selectively adsorptive solids, e.g. active carbon
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L5/00—Solid fuels
    • C10L5/02—Solid fuels such as briquettes consisting mainly of carbonaceous materials of mineral or non-mineral origin
    • C10L5/04—Raw material of mineral origin to be used; Pretreatment thereof
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L5/00—Solid fuels
    • C10L5/40—Solid fuels essentially based on materials of non-mineral origin
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L5/00—Solid fuels
    • C10L5/40—Solid fuels essentially based on materials of non-mineral origin
    • C10L5/44—Solid fuels essentially based on materials of non-mineral origin on vegetable substances
    • C10L5/447—Carbonized vegetable substances, e.g. charcoal, or produced by hydrothermal carbonization of biomass
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L9/00—Treating solid fuels to improve their combustion
    • C10L9/08—Treating solid fuels to improve their combustion by heat treatments, e.g. calcining
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L2200/00—Components of fuel compositions
    • C10L2200/04—Organic compounds
    • C10L2200/0461—Fractions defined by their origin
    • C10L2200/0469—Renewables or materials of biological origin
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L2290/00—Fuel preparation or upgrading, processes or apparatus therefore, comprising specific process steps or apparatus units
    • C10L2290/02—Combustion or pyrolysis
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L2290/00—Fuel preparation or upgrading, processes or apparatus therefore, comprising specific process steps or apparatus units
    • C10L2290/06—Heat exchange, direct or indirect
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L2290/00—Fuel preparation or upgrading, processes or apparatus therefore, comprising specific process steps or apparatus units
    • C10L2290/08—Drying or removing water
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L2290/00—Fuel preparation or upgrading, processes or apparatus therefore, comprising specific process steps or apparatus units
    • C10L2290/54—Specific separation steps for separating fractions, components or impurities during preparation or upgrading of a fuel
    • C10L2290/541—Absorption of impurities during preparation or upgrading of a fuel
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L9/00—Treating solid fuels to improve their combustion
    • C10L9/08—Treating solid fuels to improve their combustion by heat treatments, e.g. calcining
    • C10L9/083—Torrefaction
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/30—Fuel from waste, e.g. synthetic alcohol or diesel

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Materials Engineering (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Geology (AREA)
  • Sustainable Development (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Solid Fuels And Fuel-Associated Substances (AREA)

Claims (13)

PATE NTK RAV
1. Förfarande för termisk behandling av fuktigt organiskt material, speciellt organisktmaterial innehållande biomassa, varvid det fuktiga organiska materialet förs in i en tork-kammare i vilken en torkgas cirkuleras mellan det organiska materialet och en värmeväx-lare för att överföra värme till det organiska materialet, och varvid ånga som bildas undertorkning av det organiska materialet bringas i kontakt med en adsorbent för att återvinnavärme för att upprätthålla torkprocessen genom återvärmning av den cirkulerande gasen,k ä n n e t e c k n a t av att efter torkning i torkkammaren bringas det organiska materi-alet till en rostningskammare i vilken gas (ånga) som ursprungligen kommer från torkkam-maren värms och förs genom materialet så att temperaturen hos det organiska materialetökas till omkring 250°C, varigenom det organiska materialet släpper ut gaser innefattande i huvudsak vatten, kolmonoxid, organiska syror, metanol och ammoniak.
2. Förfarande enligt krav 1, varvid det organiska materialet hålls kvari rostningskammaren under en begränsad tidsperiod av 10-200 min.
3. Förfarande enligt krav 1 eller 2, varvid värmningen av materialet i rostningskammaren utförs under en tvingad konvektion av en värmd gas genom rostningskammaren.
4. Förfarande enligt något av de förgående kraven, varvid det organiska materialet förs in ien karboniseringskammare efter rostningskammaren, i vilken temperaturen hos det orga-niska materialet ökas ytterligare, initialt till en temperatur av omkring 350-450°C, genom användning av en värmd gas under tvingad konvektion, varvid gasen huvudsakligen består av ånga som härstammar från torkkammaren.
5. Förfarande enligt krav 4, varvid det organiska materialet hålls i en fast bädd genom vil- ken den värmda gasen tvingas passera.
6. Förfarande enligt krav 5, varvid vätska som bildats från det organiska materialet dräne- ras ut från det organiska materialet i den fasta bädden för att samlas in. ”160512 kravöversättning.20160513095549621, 2016-05-12
7. Förfarande enligt något av kraven 4 till 6, varvid det organiska materialet efter den initi-ala värmningen i karboniseringskammaren till en temperatur av åtminstone 350-450°Cvärms ytterligare till en högre temperatur för en slutlig karbonisering av det organiska materialet.
8. Förfarande enligt krav 7, varvid den initiala värmningen och den ytterligare värmningenutförs i separata zoneri karboniseringskammaren, och varvid den värmda gasen har olika temperaturer i de separata zonerna.
9. Förfarande enligt något av de föregående kraven, varvid komponenterna i gaserna somavges från det organiska materialet i rostningskammaren och/eller karboniseringskamma- ren absorberas selektivt i polära och icke-polära lösningsmedel.
10. Förfarande enligt något av kraven 4 till 9, varvid karboniserat organiskt material efterkarboniseringskammaren förs in i en kylkammare i vilken det karboniserade materialet till- låts svalna genom en forcerad cirkulation av en kylgas.
11. Förfarande enligt krav 10, varvid kylgasen är en del av torkgasen från torkkammaren med en liten tillsats av luft för att bränna hetfläckar (hot spots) i materialet.
12. Förfarande enligt krav 6, varvid vätskeinnehållet som samlas in är tjära.
13. Förfarande enligt krav 12, varvid den insamlade tjäran separeras till olika fraktioner. ”160512 kravöversättning.20160513095549621, 2016-05-12
SE1451097A 2014-09-18 2014-09-18 Method for thermal treatment of raw materials comprising lignocellulose SE538488C2 (sv)

Priority Applications (3)

Application Number Priority Date Filing Date Title
SE1451097A SE538488C2 (sv) 2014-09-18 2014-09-18 Method for thermal treatment of raw materials comprising lignocellulose
PCT/SE2015/050967 WO2016043651A1 (en) 2014-09-18 2015-09-15 Method for thermal treatment of raw materials comprising lignocellulose
EP15841547.1A EP3194536B1 (en) 2014-09-18 2015-09-15 Method for thermal treatment of raw materials comprising lignocellulose

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SE1451097A SE538488C2 (sv) 2014-09-18 2014-09-18 Method for thermal treatment of raw materials comprising lignocellulose

Publications (2)

Publication Number Publication Date
SE1451097A1 SE1451097A1 (en) 2016-03-19
SE538488C2 true SE538488C2 (sv) 2016-08-02

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Country Status (3)

Country Link
EP (1) EP3194536B1 (sv)
SE (1) SE538488C2 (sv)
WO (1) WO2016043651A1 (sv)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10144874B2 (en) 2013-03-15 2018-12-04 Terrapower, Llc Method and system for performing thermochemical conversion of a carbonaceous feedstock to a reaction product
CA3056784A1 (en) 2017-03-24 2018-09-27 Terrapower, Llc Method and system for recycling pyrolysis tail gas through conversion into formic acid
US10787610B2 (en) 2017-04-11 2020-09-29 Terrapower, Llc Flexible pyrolysis system and method
WO2018229520A1 (en) * 2017-06-16 2018-12-20 Arcelormittal Operating method of an iron making installation and associated operating installation
CN107619672B (zh) * 2017-08-11 2020-04-24 东南大学 一种采用生物质制取氨、氢气及尿素的方法
CN110283608A (zh) * 2019-06-06 2019-09-27 马天牧 一种生物质炭化、热、电三联生产系统
CN113061445B (zh) * 2021-03-19 2022-09-13 重庆大学 生物质与低阶煤分离耦合传热板和低品位铁矿石共热解系统

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL1030864C2 (nl) * 2006-01-06 2007-07-09 Stichting Energie Werkwijze en inrichting voor het behandelen van biomassa.
US7942942B2 (en) * 2006-05-21 2011-05-17 Paoluccio John A Method and apparatus for biomass torrefaction, manufacturing a storable fuel from biomass and producing offsets for the combustion products of fossil fuels and a combustible article of manufacture
ITTO20070438A1 (it) * 2007-06-19 2008-12-20 Martini Aldo Apparato per la decomposizione di sostanze organiche vegetali e la produzione di gas combustibile per via termochimica, e relativo metodo
EP2189512A1 (fr) * 2008-11-24 2010-05-26 Sa Cockerill Maintenance Et Ingenierie Procédé de torrefaction de la biomasse et controle de celui-ci
US8449724B2 (en) * 2009-08-19 2013-05-28 Andritz Technology And Asset Management Gmbh Method and system for the torrefaction of lignocellulosic material
WO2011159244A1 (en) * 2010-06-17 2011-12-22 Aabyhammar Tomas A method in treating solvent containing gas
SE1050619A2 (sv) * 2010-06-17 2014-03-04 Tomas Aabyhammar Sätt vid torkning där en delström av den cirkulerande gasen kontaktas med en absorptionslösning i medström
DE102012109919A1 (de) * 2012-10-17 2014-04-17 Dieffenbacher GmbH Maschinen- und Anlagenbau Verfahren und Vorrichtung zur Regelung einer Torrefizierungsanlage für Biomasse

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EP3194536A4 (en) 2017-08-02
WO2016043651A1 (en) 2016-03-24
EP3194536A1 (en) 2017-07-26
SE1451097A1 (en) 2016-03-19
EP3194536B1 (en) 2022-04-20

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