RU97111813A - METHOD FOR PRODUCING CARBON PRODUCT AND PRODUCT - Google Patents

METHOD FOR PRODUCING CARBON PRODUCT AND PRODUCT

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Publication number
RU97111813A
RU97111813A RU97111813/25A RU97111813A RU97111813A RU 97111813 A RU97111813 A RU 97111813A RU 97111813/25 A RU97111813/25 A RU 97111813/25A RU 97111813 A RU97111813 A RU 97111813A RU 97111813 A RU97111813 A RU 97111813A
Authority
RU
Russia
Prior art keywords
carbon
diazonium salt
reaction
product
medium
Prior art date
Application number
RU97111813/25A
Other languages
Russian (ru)
Other versions
RU2155707C2 (en
Inventor
А.Бельмон Джеймс
Original Assignee
Кабот Корпорейшн
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US08/356,653 external-priority patent/US5554739A/en
Application filed by Кабот Корпорейшн filed Critical Кабот Корпорейшн
Publication of RU97111813A publication Critical patent/RU97111813A/en
Application granted granted Critical
Publication of RU2155707C2 publication Critical patent/RU2155707C2/en

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Claims (19)

1. Способ получения продукта из углерода, имеющего органическую группу, присоединенную к углеродному материалу, отличающийся тем, что проводят реакцию по меньшей мере одной соли диазония с углеродным материалом, выбранным из графитного порошка, графитированного волокна, углеродного волокна, углеродной ткани, продукта из стеклообразного углерода и продукта из активированного угля, в отсутствии приложенного извне электрического тока, достаточного для того, чтобы восстановить соль диазония.1. A method of obtaining a product from carbon having an organic group attached to a carbon material, characterized in that at least one diazonium salt is reacted with a carbon material selected from graphite powder, graphite fiber, carbon fiber, carbon fabric, glassy product carbon and activated carbon product, in the absence of an externally applied electric current sufficient to restore the diazonium salt. 2. Способ по п. 1, отличающийся тем, что реакцию осуществляют в апротонной среде. 2. The method according to p. 1, characterized in that the reaction is carried out in an aprotic environment. 3. Способ по п. 1, отличающийся тем, что реакцию осуществляют в протонной среде. 3. The method according to p. 1, characterized in that the reaction is carried out in a proton medium. 4. Способ по п. 1, отличающийся тем, что соль диазония образуют in situ. 4. The method according to p. 1, characterized in that the diazonium salt is formed in situ. 5. Способ получения продукта из углерода, имеющего органическую группу, присоединенную к углеродному материалу, отличающийся тем, что проводят реакцию по меньшей мере одной соли диазония с углеродным материалом, выбранным из графитного порошка, графитированного волокна, углеродного волокна, углеродной ткани, продукта из стеклообразного углерода и продукта из активированного угля, в протонной реакционной среде. 5. A method of producing a product from carbon having an organic group attached to a carbon material, characterized in that at least one diazonium salt is reacted with a carbon material selected from graphite powder, graphite fiber, carbon fiber, carbon fabric, glassy product carbon and an activated carbon product in a proton reaction medium. 6. Способ по п. 5, отличающийся тем, что соль диазония образуют in situ из первичного амина. 6. The method according to p. 5, characterized in that the diazonium salt is formed in situ from a primary amine. 7. Способ по п. 6, отличающийся тем, что соль диазония образуют in situ путем реакции первичного амина, нитрита и кислоты. 7. The method according to p. 6, characterized in that the diazonium salt is formed in situ by reaction of a primary amine, nitrite and acid. 8. Способ по п. 7, отличающийся тем, что нитрит является нитритом металла и используют один эквивалент кислоты. 8. The method according to p. 7, characterized in that the nitrite is a metal nitrite and use one equivalent of acid. 9. Способ по п. 6, отличающийся тем, что соль диазония образуют in situ путем реакции первичного амина с нитритом и первичный амин содержит группу сильной кислоты. 9. The method according to p. 6, characterized in that the diazonium salt is formed in situ by reaction of the primary amine with nitrite and the primary amine contains a strong acid group. 10. Способ по п. 6, отличающийся тем, что соль диазония образуют in situ путем реакции первичного амина с водным раствором диоксида азота. 10. The method according to p. 6, characterized in that the diazonium salt is formed in situ by reaction of the primary amine with an aqueous solution of nitrogen dioxide. 11. Способ по п. 6, отличающийся тем, что протонная среда является водной средой, и первичный амин является амином формулы AyArNH2, в которой Аr является ароматическим радикалом, выбираемым из группы, состоящей из фенила, нафтила, антраценила, фенантренила, дифенила и пиpидинилa; А независимо является заместителем в ароматическом радикале, выбранным из функциональной группы, выбираемой из группы, состоящей из OR, COR, COOR, OCOR, COONa, COOK, COO-NR + 4 , галогена, CN, NR2, Sn, SO3H, SO3Na, SO3K, SO - 3 NR + 4 , NR(COR), CONR2, NO2, PO3H2, PO3HNa, PO3Na2, N=NR, N + 2 X-, NR + 3 X- и PR + 3 X-; и линейного разветвленного или циклического углеводородного радикала, незамещенного или замещенного одной или несколькими указанными функциональными группами; R независимо представляет водород, С1-С20-алкил или арил; n - целое число от 1 до 8; X- - галогенид или анион, произведенный из минеральной или органической кислоты; и y - целое число от 1 до 5, когда Ar представляет собой фенил, от 1 до 7, когда Ar представляет собой нафтил, от 1 до 9, когда Ar представляет собой антраценил, фенантренил или дифенил, или от 1 до 4, когда Ar представляет собой пиридинил.11. The method according to p. 6, characterized in that the proton medium is an aqueous medium, and the primary amine is an amine of the formula A y ArNH 2 in which Ar is an aromatic radical selected from the group consisting of phenyl, naphthyl, anthracene, phenanthrenyl, diphenyl and pyridinyl; And independently, it is a substituent in the aromatic radical selected from a functional group selected from the group consisting of OR, COR, COOR, OCOR, COONa, COOK, COO - NR + 4 , halogen, CN, NR 2 , S n , SO 3 H, SO 3 Na, SO 3 K, SO - 3 Nr + 4 , NR (COR), CONR 2 , NO 2 , PO 3 H 2 , PO 3 HNa, PO 3 Na 2 , N = NR, N + 2 X - , NR + 3 X - and PR + 3 X is ; and a linear branched or cyclic hydrocarbon radical unsubstituted or substituted by one or more of these functional groups; R independently represents hydrogen, C 1 -C 20 alkyl or aryl; n is an integer from 1 to 8; X - - a halide or anion produced from a mineral or organic acid; and y is an integer from 1 to 5 when Ar is phenyl, from 1 to 7 when Ar is naphthyl, from 1 to 9 when Ar is anthracene, phenanthrenyl or diphenyl, or from 1 to 4 when Ar represents pyridinyl. 12. Способ по п. 5, отличающийся тем, что соль диазония образуют in situ. 12. The method according to p. 5, characterized in that the diazonium salt is formed in situ. 13. Способ по п. 5, отличающийся тем, что соль диазония образуют из первичного амина отдельно от стадии реакции. 13. The method according to p. 5, characterized in that the diazonium salt is formed from a primary amine separately from the reaction stage. 14. Способ по п. 5, отличающийся тем, что протонной реакционной средой является водная среда. 14. The method according to p. 5, characterized in that the proton reaction medium is an aqueous medium. 15. Способ по п. 5, отличающийся тем, что органическая группа соли диазония является замещенной или незамещенной, и ее выбирают из группы, состоящей из алифатической группы, циклической органической группы, или органического соединения, имеющего алифатическую часть и циклическую часть. 15. The method according to p. 5, characterized in that the organic group of the diazonium salt is substituted or unsubstituted, and it is selected from the group consisting of an aliphatic group, a cyclic organic group, or an organic compound having an aliphatic part and a cyclic part. 16. Способ по п. 5, отличающийся тем, что протонной реакционной средой является вода. 16. The method according to p. 5, characterized in that the proton reaction medium is water. 17. Способ по п. 5, отличающийся тем, что протонной средой является среда на основе спирта. 17. The method according to p. 5, characterized in that the proton medium is an alcohol-based medium. 18. Продукт из углерода, полученный согласно способу по п. 1. 18. The carbon product obtained according to the method of claim 1. 19. Продукт из углерода, полученный согласно способу по п. 5. 19. The carbon product obtained according to the method of claim 5.
RU97111813/12A 1994-12-15 1995-12-14 Method of preparing product from carbon, and product RU2155707C2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US08/356,653 US5554739A (en) 1994-12-15 1994-12-15 Process for preparing carbon materials with diazonium salts and resultant carbon products
US08/356,653 1994-12-15

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RU97111813A true RU97111813A (en) 1999-06-10
RU2155707C2 RU2155707C2 (en) 2000-09-10

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US (1) US5554739A (en)
EP (1) EP0799282B1 (en)
JP (1) JP3980637B2 (en)
CN (2) CN1087756C (en)
AR (1) AR000350A1 (en)
AT (1) ATE191493T1 (en)
AU (1) AU692349B2 (en)
BR (1) BR9510057A (en)
CA (1) CA2207475C (en)
CO (1) CO4440602A1 (en)
CZ (1) CZ291819B6 (en)
DE (1) DE69516179T2 (en)
EG (1) EG21047A (en)
HK (1) HK1003645A1 (en)
HU (1) HU218155B (en)
IL (1) IL116375A (en)
IN (1) IN193026B (en)
MX (1) MX198173B (en)
MY (1) MY112022A (en)
NO (1) NO316384B1 (en)
NZ (1) NZ298987A (en)
PE (1) PE36696A1 (en)
PH (2) PH11995051931B1 (en)
PL (1) PL185247B1 (en)
RO (1) RO120200B1 (en)
RU (1) RU2155707C2 (en)
SI (1) SI9520130B (en)
TW (1) TW415976B (en)
UA (1) UA48156C2 (en)
WO (1) WO1996018690A1 (en)
YU (1) YU48904B (en)
ZA (1) ZA9510666B (en)

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