RU2015114018A - Low-voltage pulsed electric arc method for producing nanoparticles in liquid media - Google Patents

Low-voltage pulsed electric arc method for producing nanoparticles in liquid media Download PDF

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Publication number
RU2015114018A
RU2015114018A RU2015114018A RU2015114018A RU2015114018A RU 2015114018 A RU2015114018 A RU 2015114018A RU 2015114018 A RU2015114018 A RU 2015114018A RU 2015114018 A RU2015114018 A RU 2015114018A RU 2015114018 A RU2015114018 A RU 2015114018A
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Russia
Prior art keywords
electrodes
low
formation
voltage
liquid
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RU2015114018A
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Russian (ru)
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RU2604283C2 (en
Inventor
Валентин Степанович Щербак
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Валентин Степанович Щербак
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Priority to RU2015114018/02A priority Critical patent/RU2604283C2/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/02Making metallic powder or suspensions thereof using physical processes
    • B22F9/14Making metallic powder or suspensions thereof using physical processes using electric discharge
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00Nanotechnology for materials or surface science, e.g. nanocomposites
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00Manufacture or treatment of nanostructures
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01TSPARK GAPS; OVERVOLTAGE ARRESTERS USING SPARK GAPS; SPARKING PLUGS; CORONA DEVICES; GENERATING IONS TO BE INTRODUCED INTO NON-ENCLOSED GASES
    • H01T1/00Details of spark gaps
    • H01T1/24Selection of materials for electrodes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2304/00Physical aspects of the powder
    • B22F2304/05Submicron size particles
    • B22F2304/054Particle size between 1 and 100 nm

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Nanotechnology (AREA)
  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Composite Materials (AREA)
  • Materials Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

Низковольтный импульсный электродуговой метод получения нано частиц в жидких средах, включающий установку электродов в жидкой среде, формирование и подачу на электроды импульсного напряжения для генерации сильноточного разряда между электродами, образование плазмы в жидкости, формирование нано частиц из материала электродов и выпадение их в осадок, отличающийся тем, что один электрод устанавливается на механическом вибраторе частотой (2-20)10Гц, вибрирующие электроды осуществляют принудительное замыкание и разрыв электрической цепи; на электроды подаются двухполярные импульсы от генератора низкого напряжения 10-30 В, обеспечивающие в момент разрыва сильноточной электрической цепи (с плотностью тока свыше 10ампер/м) высокую напряженность электрического поля (свыше 10В/м) и электрический пробой всех известных в природе жидкостей. При этом залипание электродов при их размыкании устраняется следующими параметрами импульсов низковольтного генератора: длительность импульса - (20-250)10с, частота следования импульсов - (2-6)10Гц.A low-voltage pulsed electric arc method of producing nanoparticles in liquid media, including the installation of electrodes in a liquid medium, the formation and supply of pulsed voltage to the electrodes to generate a high-current discharge between the electrodes, the formation of plasma in the liquid, the formation of nanoparticles from the electrode material and their precipitation, which differs the fact that one electrode is installed on a mechanical vibrator with a frequency of (2-20) 10 Hz, the vibrating electrodes carry out forced closure and rupture of the electric circuit; bipolar pulses from the low-voltage generator 10-30 V are supplied to the electrodes, providing at the moment of breaking a high-current electric circuit (with a current density of more than 10 amperes / m) a high electric field strength (more than 10 V / m) and an electrical breakdown of all liquids known in nature. In this case, sticking of the electrodes when they are opened is eliminated by the following parameters of the pulses of the low-voltage generator: pulse duration - (20-250) 10 s, pulse repetition rate - (2-6) 10 Hz.

Claims (1)

Низковольтный импульсный электродуговой метод получения нано частиц в жидких средах, включающий установку электродов в жидкой среде, формирование и подачу на электроды импульсного напряжения для генерации сильноточного разряда между электродами, образование плазмы в жидкости, формирование нано частиц из материала электродов и выпадение их в осадок, отличающийся тем, что один электрод устанавливается на механическом вибраторе частотой (2-20)103 Гц, вибрирующие электроды осуществляют принудительное замыкание и разрыв электрической цепи; на электроды подаются двухполярные импульсы от генератора низкого напряжения 10-30 В, обеспечивающие в момент разрыва сильноточной электрической цепи (с плотностью тока свыше 109 ампер/м2) высокую напряженность электрического поля (свыше 107 В/м) и электрический пробой всех известных в природе жидкостей. При этом залипание электродов при их размыкании устраняется следующими параметрами импульсов низковольтного генератора: длительность импульса - (20-250)10-6 с, частота следования импульсов - (2-6)103 Гц. A low-voltage pulsed electric arc method of producing nanoparticles in liquid media, including the installation of electrodes in a liquid medium, the formation and supply of pulsed voltage to the electrodes to generate a high-current discharge between the electrodes, the formation of plasma in a liquid, the formation of nanoparticles from electrode material and their precipitation, which differs the fact that one electrode is installed on a mechanical vibrator with a frequency of (2-20) 10 3 Hz, the vibrating electrodes carry out forced closure and rupture of the electric circuit; bipolar pulses from the low-voltage generator 10-30 V are supplied to the electrodes, providing at the moment of breaking a high-current electric circuit (with a current density of over 10 9 ampere / m 2 ) high electric field strength (over 10 7 V / m) and electrical breakdown of all known in the nature of liquids. In this case, sticking of the electrodes when they are opened is eliminated by the following parameters of the pulses of the low-voltage generator: pulse duration - (20-250) 10 -6 s, pulse repetition rate - (2-6) 10 3 Hz.
RU2015114018/02A 2015-04-15 2015-04-15 Low-voltage pulse electric arc method of producing metal nanopowder in liquid medium RU2604283C2 (en)

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RU2015114018/02A RU2604283C2 (en) 2015-04-15 2015-04-15 Low-voltage pulse electric arc method of producing metal nanopowder in liquid medium

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RU2015114018/02A RU2604283C2 (en) 2015-04-15 2015-04-15 Low-voltage pulse electric arc method of producing metal nanopowder in liquid medium

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RU2604283C2 RU2604283C2 (en) 2016-12-10

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113458404A (en) * 2021-07-06 2021-10-01 上海科技大学 Alloy nanoparticles, preparation method and application thereof
CN115038535A (en) * 2019-07-31 2022-09-09 米科拉·莫纳斯蒂罗夫 Metal particles and method of making same using electroerosion dispersion
CN115635092A (en) * 2022-11-04 2023-01-24 北京航空航天大学 A method and device for preparing ultrafine powder using strip material as a pulse discharge electrode

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2756189C1 (en) * 2019-12-19 2021-09-28 Федеральное государственное бюджетное образовательное учреждение высшего образования "Московский авиационный институт" (национальный исследовательский университет)" Unit for electric pulse controlled production of nanoparticles of current-conductive materials
RU2748277C1 (en) * 2020-02-18 2021-05-21 Валентин Степанович Щербак Low-voltage pulsed electric arc method for producing metal nanopowder in liquid medium

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7883606B2 (en) * 2003-09-10 2011-02-08 Nahum Parkansky Production of nanoparticles and microparticles
EP2112670B1 (en) * 2007-02-15 2018-04-18 Kankyou Engineering Co., Ltd. Method for producing conductor fine particles
RU94492U1 (en) * 2010-02-26 2010-05-27 Владимир Владимирович Слепцов DEVICE FOR PRODUCING NANOPARTICLES OF CONDUCTIVE MATERIALS
RU2475298C1 (en) * 2011-07-12 2013-02-20 Федеральное государственное бюджетное учреждение "Национальный исследовательский центр "Курчатовский институт" Method of making nanopowders from various electrically conducting materials
RU2496920C1 (en) * 2012-03-11 2013-10-27 Сергей Дмитриевич Терентьев Method of preparation of nanomaterials

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115038535A (en) * 2019-07-31 2022-09-09 米科拉·莫纳斯蒂罗夫 Metal particles and method of making same using electroerosion dispersion
US12485483B2 (en) 2019-07-31 2025-12-02 Mykola MONASTYROV Metal particles and method for preparation thereof using electroerosion dispersion
CN113458404A (en) * 2021-07-06 2021-10-01 上海科技大学 Alloy nanoparticles, preparation method and application thereof
CN115635092A (en) * 2022-11-04 2023-01-24 北京航空航天大学 A method and device for preparing ultrafine powder using strip material as a pulse discharge electrode

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