RU2010123680A - IMPROVED DETECTION OF LABELING SUBSTANCES - Google Patents

IMPROVED DETECTION OF LABELING SUBSTANCES Download PDF

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Publication number
RU2010123680A
RU2010123680A RU2010123680/05A RU2010123680A RU2010123680A RU 2010123680 A RU2010123680 A RU 2010123680A RU 2010123680/05 A RU2010123680/05 A RU 2010123680/05A RU 2010123680 A RU2010123680 A RU 2010123680A RU 2010123680 A RU2010123680 A RU 2010123680A
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RU
Russia
Prior art keywords
polar liquid
polar
marking
contaminated
contaminated non
Prior art date
Application number
RU2010123680/05A
Other languages
Russian (ru)
Inventor
Рюдигер ЗЕНС (DE)
Рюдигер Зенс
Кристос ВАМВАКАРИС (DE)
Кристос Вамвакарис
Вольфганг АЛЕРС (BE)
Вольфганг Алерс
Original Assignee
Басф Се (De)
Басф Се
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Publication date
Application filed by Басф Се (De), Басф Се filed Critical Басф Се (De)
Publication of RU2010123680A publication Critical patent/RU2010123680A/en

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    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10LFUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00Liquid carbonaceous fuels
    • C10L1/10Liquid carbonaceous fuels containing additives
    • C10L1/14Organic compounds
    • C10L1/22Organic compounds containing nitrogen
    • C10L1/222Organic compounds containing nitrogen containing at least one carbon-to-nitrogen single bond
    • C10L1/224Amides; Imides carboxylic acid amides, imides
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10LFUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00Liquid carbonaceous fuels
    • C10L1/003Marking, e.g. coloration by addition of pigments
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10LFUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00Liquid carbonaceous fuels
    • C10L1/10Liquid carbonaceous fuels containing additives
    • C10L1/14Organic compounds
    • C10L1/22Organic compounds containing nitrogen
    • C10L1/222Organic compounds containing nitrogen containing at least one carbon-to-nitrogen single bond
    • C10L1/223Organic compounds containing nitrogen containing at least one carbon-to-nitrogen single bond having at least one amino group bound to an aromatic carbon atom
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/62Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
    • G01N21/63Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light optically excited
    • G01N21/64Fluorescence; Phosphorescence
    • G01N21/6428Measuring fluorescence of fluorescent products of reactions or of fluorochrome labelled reactive substances, e.g. measuring quenching effects, using measuring "optrodes"
    • G01N21/643Measuring fluorescence of fluorescent products of reactions or of fluorochrome labelled reactive substances, e.g. measuring quenching effects, using measuring "optrodes" non-biological material
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/26Oils; Viscous liquids; Paints; Inks
    • G01N33/28Oils, i.e. hydrocarbon liquids
    • G01N33/2835Specific substances contained in the oils or fuels
    • G01N33/2882Markers

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Organic Chemistry (AREA)
  • Immunology (AREA)
  • General Physics & Mathematics (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Pathology (AREA)
  • Food Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Molecular Biology (AREA)
  • Optics & Photonics (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)

Abstract

1. Способ обнаружения маркирующих веществ в загрязненных неполярных жидкостях, отличающийся тем, что ! a) в загрязненных неполярных жидкостях находятся одно или несколько, одинаковых или различных маркирующих веществ, ! b) полярную жидкость подвергают контакту с загрязненной неполярной жидкостью, и ! c) маркирующее вещество обнаруживают в загрязненной неполярной жидкости. ! 2. Способ по п.1, отличающийся тем, что неполярная жидкость содержит масло. ! 3. Способ по п.2, отличающийся тем, что масло содержит минеральное масло. ! 4. Способ по п.3, отличающийся тем, что минеральное масло содержит дизельное топливо. ! 5. Способ по п.1, отличающийся тем, что полярная жидкость имеет диэлектрическую константу более 30. ! 6. Способ по п.1, отличающийся тем, что полярная жидкость является N-метил-2-пирролидоном, сульфоланом, ДМФА или ДМСО. ! 7. Способ по п.1, отличающийся тем, что на стадии (b) проводят экстракцию загрязнений. ! 8. Способ по пп.1-7, отличающийся тем, что на дальнейшей стадии (b') полярную жидкость отделяют от неполярной жидкости, перед тем как маркирующее вещество обнаруживают на стадии (c). ! 9. Способ маркирования загрязненных неполярных жидкостей, отличающийся тем, что обнаружение маркирующих веществ происходит в соответствии со способом согласно пп.1-8. 1. A method for detecting marking substances in contaminated non-polar liquids, characterized in that! a) contaminated non-polar fluids contain one or more, same or different marking substances,! b) the polar liquid is exposed to contaminated non-polar liquid, and! c) the marking substance is detected in a contaminated non-polar liquid. ! 2. The method according to claim 1, characterized in that the non-polar liquid contains oil. ! 3. The method according to claim 2, characterized in that the oil contains mineral oil. ! 4. The method according to claim 3, characterized in that the mineral oil contains diesel fuel. ! 5. The method according to claim 1, characterized in that the polar liquid has a dielectric constant of more than 30.! 6. The method according to claim 1, characterized in that the polar liquid is N-methyl-2-pyrrolidone, sulfolane, DMF or DMSO. ! 7. The method according to claim 1, characterized in that at the stage (b) carry out the extraction of contaminants. ! 8. The method according to claims 1 to 7, characterized in that in the next step (b ') the polar liquid is separated from the non-polar liquid before the marking substance is detected in step (c). ! 9. A method for marking contaminated non-polar liquids, characterized in that the detection of marking substances occurs in accordance with the method according to claims 1 to 8.

Claims (9)

1. Способ обнаружения маркирующих веществ в загрязненных неполярных жидкостях, отличающийся тем, что1. A method for detecting marking substances in contaminated non-polar liquids, characterized in that a) в загрязненных неполярных жидкостях находятся одно или несколько, одинаковых или различных маркирующих веществ,a) contaminated non-polar liquids contain one or more, same or different marking substances, b) полярную жидкость подвергают контакту с загрязненной неполярной жидкостью, иb) the polar liquid is contacted with a contaminated non-polar liquid, and c) маркирующее вещество обнаруживают в загрязненной неполярной жидкости.c) the marking substance is detected in a contaminated non-polar liquid. 2. Способ по п.1, отличающийся тем, что неполярная жидкость содержит масло.2. The method according to claim 1, characterized in that the non-polar liquid contains oil. 3. Способ по п.2, отличающийся тем, что масло содержит минеральное масло.3. The method according to claim 2, characterized in that the oil contains mineral oil. 4. Способ по п.3, отличающийся тем, что минеральное масло содержит дизельное топливо.4. The method according to claim 3, characterized in that the mineral oil contains diesel fuel. 5. Способ по п.1, отличающийся тем, что полярная жидкость имеет диэлектрическую константу более 30.5. The method according to claim 1, characterized in that the polar liquid has a dielectric constant of more than 30. 6. Способ по п.1, отличающийся тем, что полярная жидкость является N-метил-2-пирролидоном, сульфоланом, ДМФА или ДМСО.6. The method according to claim 1, characterized in that the polar liquid is N-methyl-2-pyrrolidone, sulfolane, DMF or DMSO. 7. Способ по п.1, отличающийся тем, что на стадии (b) проводят экстракцию загрязнений.7. The method according to claim 1, characterized in that at the stage (b) carry out the extraction of contaminants. 8. Способ по пп.1-7, отличающийся тем, что на дальнейшей стадии (b') полярную жидкость отделяют от неполярной жидкости, перед тем как маркирующее вещество обнаруживают на стадии (c).8. The method according to claims 1 to 7, characterized in that in the next step (b '), the polar liquid is separated from the non-polar liquid before the marking substance is detected in step (c). 9. Способ маркирования загрязненных неполярных жидкостей, отличающийся тем, что обнаружение маркирующих веществ происходит в соответствии со способом согласно пп.1-8. 9. A method for marking contaminated non-polar liquids, characterized in that the detection of marking substances occurs in accordance with the method according to claims 1 to 8.
RU2010123680/05A 2007-11-14 2008-11-10 IMPROVED DETECTION OF LABELING SUBSTANCES RU2010123680A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP07120650 2007-11-14
EP07120650.2 2007-11-14

Publications (1)

Publication Number Publication Date
RU2010123680A true RU2010123680A (en) 2011-12-20

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ID=40394193

Family Applications (1)

Application Number Title Priority Date Filing Date
RU2010123680/05A RU2010123680A (en) 2007-11-14 2008-11-10 IMPROVED DETECTION OF LABELING SUBSTANCES

Country Status (6)

Country Link
EP (1) EP2209875A1 (en)
CN (1) CN101855324A (en)
BR (1) BRPI0820313A2 (en)
PE (1) PE20091290A1 (en)
RU (1) RU2010123680A (en)
WO (1) WO2009062899A1 (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109096166B (en) * 2017-12-27 2020-02-14 南京晓庄学院 Preparation method of anthraquinone derivative

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1913612A1 (en) * 1969-03-18 1970-09-24 Hoechst Ag Process for coloring hydrocarbons
US4049393A (en) * 1974-11-18 1977-09-20 Morton-Norwich Products, Inc. Colored petroleum-derived product
DE3700329A1 (en) * 1987-01-08 1988-07-21 Basf Ag Method for detecting identifying substances in dark-coloured mineral oil products
JPH05202367A (en) * 1991-10-15 1993-08-10 General Sekiyu Kk Method for desulfurizing and denitrating light oil by extraction
US5723338A (en) * 1994-11-04 1998-03-03 Amoco Corporation Tagging hydrocarbons for subsequent identification
US6320090B1 (en) * 1999-03-10 2001-11-20 Miami University Method of removing contaminants from petroleum distillates
GB2354070A (en) * 1999-09-07 2001-03-14 Duncan William John Mccallien Markers for identifying liquids
US20020036158A1 (en) * 2000-08-08 2002-03-28 Austin Douglas P. Batch process for refining used oil
US6514917B1 (en) * 2001-08-28 2003-02-04 United Color Manufacturing, Inc. Molecular tags for organic solvent systems
US6977177B1 (en) * 2004-05-26 2005-12-20 Rohm And Haas Company Method for marking hydrocarbons with substituted anthraquinones

Also Published As

Publication number Publication date
CN101855324A (en) 2010-10-06
WO2009062899A1 (en) 2009-05-22
EP2209875A1 (en) 2010-07-28
BRPI0820313A2 (en) 2015-05-26
PE20091290A1 (en) 2009-09-25

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Effective date: 20111226