RU2006143086A - METHOD FOR STRUCTURED FILLING OF CONTACT PIPES BEAM OF CONTACT PIPES - Google Patents

METHOD FOR STRUCTURED FILLING OF CONTACT PIPES BEAM OF CONTACT PIPES Download PDF

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RU2006143086A
RU2006143086A RU2006143086/15A RU2006143086A RU2006143086A RU 2006143086 A RU2006143086 A RU 2006143086A RU 2006143086/15 A RU2006143086/15 A RU 2006143086/15A RU 2006143086 A RU2006143086 A RU 2006143086A RU 2006143086 A RU2006143086 A RU 2006143086A
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Russia
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catalyst
package
contact
filling
filled
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RU2006143086/15A
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Russian (ru)
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RU2393915C2 (en
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Мартин ДИТЕРЛЕ (DE)
Мартин ДИТЕРЛЕ
Кнут ЭГЕР (DE)
Кнут ЭГЕР
Клаус Йоахим МЮЛЛЕР-ЭНГЕЛЬ (DE)
Клаус Йоахим МЮЛЛЕР-ЭНГЕЛЬ
Ульрих ХАММОН (DE)
Ульрих ХАММОН
Фолькер ШЛИПХАКЕ (DE)
Фолькер ШЛИПХАКЕ
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БАСФ Акциенгезельшафт (DE)
Басф Акциенгезельшафт
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/0015—Feeding of the particles in the reactor; Evacuation of the particles out of the reactor
    • B01J8/003—Feeding of the particles in the reactor; Evacuation of the particles out of the reactor in a downward flow
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/002—Mixed oxides other than spinels, e.g. perovskite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/0015—Feeding of the particles in the reactor; Evacuation of the particles out of the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B01J8/067—Heating or cooling the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00743—Feeding or discharging of solids
    • B01J2208/00752—Feeding
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00743—Feeding or discharging of solids
    • B01J2208/00769—Details of feeding or discharging
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796—Details of the reactor or of the particulate material
    • B01J2208/00805—Details of the particulate material
    • B01J2208/00814—Details of the particulate material the particulate material being provides in prefilled containers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/02—Processes carried out in the presence of solid particles; Reactors therefor with stationary particles
    • B01J2208/023—Details
    • B01J2208/024—Particulate material
    • B01J2208/025—Two or more types of catalyst
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/30—Details relating to random packing elements
    • B01J2219/308—Details relating to random packing elements filling or discharging the elements into or from packed columns
    • B01J2219/3086—Filling of the packing elements into the column or vessel, e.g. using a tube
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B01J23/888—Tungsten
    • B01J23/8885—Tungsten containing also molybdenum
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00—Constitutive chemical elements of heterogeneous catalysts
    • B01J35/19—
    • B01J35/50—

Abstract

1. Способ структурированного заполнения контактных труб пучка контактных труб, при котором отдельные контактные трубы пучка контактных труб заполняют единым образом снизу вверх по отрезкам различимыми друг от друга составами катализаторных формованных изделий, отличающийся тем, что для получения определенного отрезка заполнения в контактных трубах сначала создают единые количественные порции соответствующего состава из катализаторных формованных изделий, обертыванием таких порций упаковочным средством получают заполненные единым количеством состава катализаторных формованных изделий упаковки и опорожняют в каждую из индивидуальных контактных труб одно число упаковок.2. Способ по п.1, отличающийся тем, что количество состава катализаторных формованных изделий в одной упаковке составляет 50 г до 5 кг.3. Способ по п.1, отличающийся тем, что продольное распространение подлежащих заполнению катализаторных формованных изделий составляет от 1 мм до 20 мм.4. Способ по п.1, отличающийся тем, что заполненные контактные трубы имеют, по меньшей мере, три различимых друг от друга отрезков заполнения.5. Способ по одному из пп.1-4, отличающийся тем, что соотношение внутреннего диаметра D контактной трубы к продольному распространению L, содержащихся в одной упаковке катализаторных формованных изделий, составляет от 2:1 до 20:1.6. Способ по п.1, отличающийся тем, что активная масса содержащихся в одной упаковке катализаторных формованных изделий представляет собой содержащий Мо, Bi и Fe и/или Мо и V оксид мультиметаллов.7. Способ по п.1, отличающийся тем, что количественная порция упаковки такова, что ее опорожнением в контактную тр�1. A method of structured filling of the contact tubes of a bundle of contact tubes, in which the individual contact tubes of the bundle of contact tubes are filled in a uniform manner from bottom to top along the segments with distinguishable compositions of catalyst molded articles, characterized in that to obtain a certain segment of filling in the contact tubes, uniform quantitative portions of the corresponding composition of the catalyst shaped articles, by wrapping such portions with a packaging means, packages filled with a single amount of the composition of the catalyst shaped articles are obtained and one number of packages are emptied into each of the individual contact tubes. 2. The method according to claim 1, characterized in that the amount of the composition of the catalyst shaped bodies in one package is 50 g to 5 kg. The method according to claim 1, characterized in that the longitudinal spread of the catalyst shaped bodies to be filled is from 1 mm to 20 mm. The method according to claim 1, characterized in that the filled contact tubes have at least three distinct filling segments. A method according to one of claims 1 to 4, characterized in that the ratio of the inner diameter D of the contact tube to the longitudinal expansion L of the catalyst shaped bodies contained in one package is from 2: 1 to 20: 1.6. The method according to claim 1, characterized in that the active mass of the catalyst shaped bodies contained in one package is a multimetal oxide containing Mo, Bi and Fe and / or Mo and V. The method according to claim 1, characterized in that the quantitative portion of the package is such that emptying it into a contact tube

Claims (15)

1. Способ структурированного заполнения контактных труб пучка контактных труб, при котором отдельные контактные трубы пучка контактных труб заполняют единым образом снизу вверх по отрезкам различимыми друг от друга составами катализаторных формованных изделий, отличающийся тем, что для получения определенного отрезка заполнения в контактных трубах сначала создают единые количественные порции соответствующего состава из катализаторных формованных изделий, обертыванием таких порций упаковочным средством получают заполненные единым количеством состава катализаторных формованных изделий упаковки и опорожняют в каждую из индивидуальных контактных труб одно число упаковок.1. A method of structured filling of the contact tubes of the contact tube bundle, in which the individual contact tubes of the contact tube bundle are filled in a unified manner from the bottom up along the segments with catalyst compositions formed from each other, characterized in that, to obtain a certain length of filling, the contact tubes are first created with uniform quantitative portions of the appropriate composition from the catalyst molded products, wrapping such portions with a packaging agent, get filled units the number of trains catalyst bodies and empty packaging in each of the individual catalyst tube number one packages. 2. Способ по п.1, отличающийся тем, что количество состава катализаторных формованных изделий в одной упаковке составляет 50 г до 5 кг.2. The method according to claim 1, characterized in that the amount of the composition of the catalyst molded products in one package is 50 g to 5 kg 3. Способ по п.1, отличающийся тем, что продольное распространение подлежащих заполнению катализаторных формованных изделий составляет от 1 мм до 20 мм.3. The method according to claim 1, characterized in that the longitudinal distribution of the to be filled catalyst molded products is from 1 mm to 20 mm 4. Способ по п.1, отличающийся тем, что заполненные контактные трубы имеют, по меньшей мере, три различимых друг от друга отрезков заполнения.4. The method according to claim 1, characterized in that the filled contact tubes have at least three distinct from each other segments of the filling. 5. Способ по одному из пп.1-4, отличающийся тем, что соотношение внутреннего диаметра D контактной трубы к продольному распространению L, содержащихся в одной упаковке катализаторных формованных изделий, составляет от 2:1 до 20:1.5. The method according to one of claims 1 to 4, characterized in that the ratio of the inner diameter D of the contact tube to the longitudinal distribution L contained in one package of the catalyst molded products is from 2: 1 to 20: 1. 6. Способ по п.1, отличающийся тем, что активная масса содержащихся в одной упаковке катализаторных формованных изделий представляет собой содержащий Мо, Bi и Fe и/или Мо и V оксид мультиметаллов.6. The method according to claim 1, characterized in that the active mass of the catalyst molded articles contained in one package is a multimetal oxide containing Mo, Bi and Fe and / or Mo and V oxide. 7. Способ по п.1, отличающийся тем, что количественная порция упаковки такова, что ее опорожнением в контактную трубу полностью производят в ней желаемый отрезок заполнения.7. The method according to claim 1, characterized in that the quantitative portion of the package is such that by emptying it into the contact tube completely produce the desired length of filling in it. 8. Способ по п.1, отличающийся тем, что число упаковок опорожняют в контактную трубу вручную.8. The method according to claim 1, characterized in that the number of packages is emptied into the contact tube manually. 9. Способ по п.1, отличающийся тем, что число упаковок опорожняют в контактную трубу машиной заполнения катализатора.9. The method according to claim 1, characterized in that the number of packages is emptied into the contact tube by the catalyst filling machine. 10. Способ по п.9, отличающийся тем, что машина заполнения катализатора имеет запасную емкость, вместимость которой соответствует количественной порции одной упаковки.10. The method according to claim 9, characterized in that the catalyst filling machine has a spare capacity, the capacity of which corresponds to a quantitative portion of one package. 11. Способ по одному из пп.1-4 и 6-10, отличающийся тем, что число опорожняемых на одну контактную трубу упаковок составляет ≥1.11. The method according to one of claims 1 to 4 and 6-10, characterized in that the number of packages emptied per contact tube is ≥1. 12. Способ по п.5, отличающийся тем, что число опорожняемых на одну контактную трубу упаковок составляет ≥1.12. The method according to claim 5, characterized in that the number of packages emptied per contact tube is ≥1. 13. Упаковка, полученная обертыванием упаковочным средством количественной порции катализаторных формованных изделий.13. The package obtained by wrapping the packaging means of a quantitative portion of the catalyst molded products. 14. Упаковка по п.13, которая содержит от 50 г до 5 кг количественной порции катализаторных формованных изделий.14. The package according to item 13, which contains from 50 g to 5 kg of a quantitative portion of the catalyst molded products. 15. Упаковка по одному из пп.13 и 14, содержащая катализаторные формованные изделия, активная масса которых представляет собой содержащий Мо, Bi и Fe и/или Мо и V оксид мультиметаллов.15. Packaging according to one of paragraphs.13 and 14, containing a catalyst molded product, the active mass of which is containing Mo, Bi and Fe and / or Mo and V oxide of multimetals.
RU2006143086/15A 2004-05-07 2005-04-22 Method of structured filling of contact tubes of contact tube bundle and package produced on wrapping by quantitative portion of formed catalyst product composition RU2393915C2 (en)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US56869904P 2004-05-07 2004-05-07
DE102004023249.0 2004-05-07
DE102004023249A DE102004023249A1 (en) 2004-05-07 2004-05-07 Process to insert selected catalyst rings into battery of reactor tubes followed by manual removal as required
US60/568,699 2004-05-07

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RU2006143086A true RU2006143086A (en) 2008-06-20
RU2393915C2 RU2393915C2 (en) 2010-07-10

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JP (1) JP4768726B2 (en)
KR (1) KR101431365B1 (en)
CN (3) CN103894117A (en)
DE (1) DE102004023249A1 (en)
RU (1) RU2393915C2 (en)
ZA (1) ZA200610181B (en)

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JP2007536078A (en) 2007-12-13
KR101431365B1 (en) 2014-08-18
CN1956773A (en) 2007-05-02
ZA200610181B (en) 2008-05-28
CN103894117A (en) 2014-07-02
CN103908927A (en) 2014-07-09
RU2393915C2 (en) 2010-07-10
DE102004023249A1 (en) 2005-03-10
JP4768726B2 (en) 2011-09-07
KR20120134146A (en) 2012-12-11

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