RU2003107850A - POLYMER, POLYMERIC MICROFIBER, POLYMERIC NANOFIBER AND AREAS OF APPLICATION INCLUDING FILTER DESIGNS - Google Patents

POLYMER, POLYMERIC MICROFIBER, POLYMERIC NANOFIBER AND AREAS OF APPLICATION INCLUDING FILTER DESIGNS

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Publication number
RU2003107850A
RU2003107850A RU2003107850/04A RU2003107850A RU2003107850A RU 2003107850 A RU2003107850 A RU 2003107850A RU 2003107850/04 A RU2003107850/04 A RU 2003107850/04A RU 2003107850 A RU2003107850 A RU 2003107850A RU 2003107850 A RU2003107850 A RU 2003107850A
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polymer
fiber
additive
thin fiber
nylon
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RU2003107850/04A
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Russian (ru)
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RU2300543C2 (en
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Ху. Й. ЧАНГ
Джон Р. Б. ХОЛЛ
Марк А. ГОГИНС
Дуглас Г. КРОФУТ
Томас М. УИК
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Дональдсон Компани, Инк.
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Priority claimed from US09/871,583 external-priority patent/US6743273B2/en
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Claims (24)

1. Полимерный состав, включающий полимер присоединения и приблизительно от 2 до 25 вес.% добавки, причем добавка содержит смолистый материал, имеющий молекулярный вес приблизительно от 500 до 3000 и ароматическую природу, в котором указанная добавка смешивается в полимере.1. A polymer composition comprising an addition polymer and from about 2 to 25 wt.% Additives, the additive containing a resinous material having a molecular weight of from about 500 to 3000 and an aromatic nature in which said additive is mixed in the polymer. 2. Состав по п.1, отличающийся тем, что добавка включает олигомер, содержащий третичный бутилфенол.2. The composition according to claim 1, characterized in that the additive includes an oligomer containing tertiary butylphenol. 3. Полимерный состав, содержащий полимер конденсации, отличающийся от сополимера, сформированного из циклического лактама и диамин мономера С6-10 или двукислотного мономера С6-10, и смолистая добавка, включающая олигомер, имеющий молекулярный вес приблизительно от 500 до 3000 и ароматическую природу, в котором добавка, смешивается в полимере конденсации.3. A polymer composition comprising a condensation polymer, different from a copolymer formed from cyclic lactam and a diamine monomer C 6-10 or a di-acid monomer C 6-10 , and a resinous additive comprising an oligomer having a molecular weight of from about 500 to 3000 and aromatic nature in which the additive is mixed in a condensation polymer. 4. Состав по п.3, отличающийся тем, что нейлоновый сополимер объединен со вторым нейлоновым полимером, причем второй нейлоновый полимер отличается по составу мономера или по молекулярному весу.4. The composition according to claim 3, characterized in that the nylon copolymer is combined with the second nylon polymer, and the second nylon polymer differs in the composition of the monomer or in molecular weight. 5. Состав по п.4, отличающийся тем, что полимеры обрабатываются с возможностью сформировать единственный полимерный состав, как он измерен дифференциальным сканирующим калориметром, показывающим однофазный материал.5. The composition according to claim 4, characterized in that the polymers are processed with the ability to form a single polymer composition, as it is measured by a differential scanning calorimeter showing a single-phase material. 6. Состав тонкого волокна, включающий полимер присоединения и приблизительно от 2 до 25 вес.% добавки, причем добавка содержит смолистый материал, имеющий молекулярный вес приблизительно от 500 до 3000 и ароматическую природу, в котором добавка смешивающийся в полимере.6. A fine fiber composition comprising an addition polymer and from about 2 to 25% by weight of the additive, the additive containing a resinous material having a molecular weight of from about 500 to 3000 and an aromatic nature in which the additive is miscible in the polymer. 7. Тонкое волокно по п.6, отличающееся тем, что добавка содержит гидрофобное покрытие на поверхности тонкого волокна.7. Thin fiber according to claim 6, characterized in that the additive contains a hydrophobic coating on the surface of the thin fiber. 8. Состав тонкого волокна, включающий полимер конденсации, отличающийся от сополимера циклического лактама и мономера диамина С6-10 или двукислотного мономера С6-10, и аддитивный состав, имеющий молекулярный вес приблизительно от 500 до 3000,8. The composition of the thin fiber, including a condensation polymer, different from a copolymer of cyclic lactam and monomer diamine C 6-10 or dicarbon monomer C 6-10 , and an additive composition having a molecular weight of from about 500 to 3000, 9. Тонкое волокно по п.8, отличающееся тем, что гидрофобное и олеофобное покрытие сформировано на волокне, имеющем гидрофильный состав.9. A thin fiber according to claim 8, characterized in that the hydrophobic and oleophobic coating is formed on a fiber having a hydrophilic composition. 10. Тонкое волокно, включающее волокно, имеющее диаметр приблизительно от 0,1 до 0,5 мкм и содержит продукт реакции реагента альдегида и смеси нейлона 4,6 и нейлона 6,6.10. A thin fiber comprising a fiber having a diameter of from about 0.1 to 0.5 microns and contains a reaction product of an aldehyde reagent and a mixture of nylon 4.6 and nylon 6.6. 11. Тонкое волокно по п.10, отличающееся тем, что тонкое волокно включает продукт реакции реагента альдегида и смеси нейлона 6 и нейлона 6,6 в присутствии спирта С1-24 и воды.11. The thin fiber of claim 10, wherein the thin fiber includes a reaction product of an aldehyde reagent and a mixture of nylon 6 and nylon 6.6 in the presence of alcohol C 1-24 and water. 12. Полимерный состав, содержащий полимерный продукт реакции нейлона 6 и нейлонового сополимера, включающего циклический лактам, мономер диамина С6-10 и двухкислотный мономер С6-10, и смолистая добавка, содержащая олигомер, имеющий молекулярный вес приблизительно от 500 до 3000 и ароматическую природу, в котором добавка смешивающийся в полимере конденсации.12. A polymeric composition comprising a polymeric reaction product of nylon 6 and a nylon copolymer comprising a cyclic lactam, a C 6-10 diamine monomer and a diacid monomer is a C 6-10, and the resinous additive comprising an oligomer having a molecular weight from about 500 to 3000 and an aromatic nature in which the additive is miscible in polymer condensation. 13. Полимерный Состав по п.12, отличающийся тем, что полимерное продукт реакции включает нейлон 6,6 и нейлоновый сополимер.13. The polymer composition according to item 12, wherein the polymer reaction product includes nylon 6.6 and a nylon copolymer. 14. Состав по п.12, отличающийся тем, что добавка содержит олигомер, включающий14. The composition according to p. 12, characterized in that the additive contains an oligomer, including
Figure 00000001
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 15. Фильтрующая среда, содержащая тонкое волокно, причем это тонкое волокно имеет размер приблизительно от 0,01 до 0,5 мкм и после выдержки на воздухе при 140°F(60°C) и относительной влажности 100% в течение от 1 до 16 ч, по меньшей мере, 50% волокна остается, в основном, неизменным.15. The filter medium containing a thin fiber, and this fine fiber has a size of from about 0.01 to 0.5 μm and after exposure to air at 140 ° F (60 ° C) and a relative humidity of 100% for 1 to 16 h, at least 50% of the fiber remains essentially unchanged. 16. Среда по п.15, отличающаяся тем, что слой тонкого волокна может быть подвергнут действию спиртового растворителя при температуре 70°F(21°C), и в которой после 5 мин остается, по меньшей мере, 50% волокна.16. The environment of claim 15, wherein the thin fiber layer can be exposed to an alcohol solvent at a temperature of 70 ° F (21 ° C), and in which at least 50% of the fiber remains after 5 minutes. 17. Среда по п.15, отличающаяся тем, что фильтрующая среда также включает тканую или нетканую подложку.17. The medium according to item 15, wherein the filter medium also includes a woven or non-woven substrate. 18. Среда по п.15, отличающаяся тем, что подложка включает электростатически спряденную полимерную нетканую ткань.18. The environment of claim 15, wherein the substrate comprises electrostatically spun polymer nonwoven fabric. 19. Среда по п.15, отличающаяся тем, что тонкое волокно включает микроволокно, имеющее диаметр приблизительно от 0,1 до 0,5 мкм.19. The medium according to item 15, wherein the thin fiber includes a microfiber having a diameter of from about 0.1 to 0.5 microns. 20. Среда по п.19, отличающаяся тем, что включает подложку и слой тонкого волокна.20. The medium according to claim 19, characterized in that it includes a substrate and a layer of thin fiber. 21. Способ изготовления материала из тонкого волокна, включающего волокна, имеющие диаметр приблизительно от 0,01 до 0,5 мкм, и поверхностное покрытие, имеющее толщину менее чем приблизительно 100 А; причем способ включает формирование раствора, содержащего низший спирт, воду или их смеси и приблизительно от 3 до приблизительно 30 вес.% полимерного состава, отличающегося от сополимера, сформированного из циклического лактама и мономера диамина С6-10 или двухкислотного мономера С6-10 и приблизительно от 2 до 25 вес.% добавки, на основе полимера; указанная добавка включает смолистый материал, имеющий молекулярный вес приблизительно от 500 до приблизительно 3000 и ароматическую природу, в котором добавка смешивается в полимере, при этом раствор полимера подвергается действию электрического поля с потенциалом более чем 10х103 вольт, в результате чего в растворе формируются ускоренные пряди раствора, которые при испарении растворителя образуют тонкое волокно, собирая тонкое волокно на подложке и подвергая тонкое волокно и подложку термической обработке, при этом термическая обработка повышает температуру тонкого волокна до температуры, не превышающей точки плавления полимера.21. A method of manufacturing a material of thin fiber, including fibers having a diameter of from about 0.01 to 0.5 microns, and a surface coating having a thickness of less than about 100 A; wherein the method comprises forming a solution containing a lower alcohol, water or mixtures thereof and from about 3 to about 30 wt.% of the polymeric composition, different from the copolymer formed from a cyclic lactam and a C 6-10 diamine monomer or a C6-10 diacid monomer and from about 2 to 25% by weight of a polymer based additive; said additive includes a resinous material having a molecular weight of from about 500 to about 3000 and an aromatic nature in which the additive is mixed in the polymer, wherein the polymer solution is exposed to an electric field with a potential of more than 10x10 3 volts, resulting in the formation of accelerated strands in the solution solution, which upon evaporation of the solvent form a thin fiber, collecting the thin fiber on the substrate and subjecting the thin fiber and the substrate to heat treatment, while heat treatment It increases the fine fiber temperature to a temperature not exceeding the polymer melting point. 22. Способ по п.21, отличающийся тем, что полимер содержит полимер присоединения.22. The method according to item 21, wherein the polymer contains an addition polymer. 23. Способ по п.21, отличающийся тем, что полимер содержит смесь нейлонового гомополимера и нейлонового сополимера, включающего структурные единицы, производные от циклического лактама, мономера диамина С6-10 и двухкислотного мономера С6-10.23. The method according to claim 21, characterized in that the polymer mixture comprises a nylon homopolymer and a nylon copolymer comprising structural units derived from a cyclic lactam, a C 6-10 diamine monomer and a diacid monomer C 6-10. 24. Способ создания тонковолоконного материала, содержащего волокна, имеющие диаметр приблизительно от 0,01 до 2 мкм, при этом волокно включает линейное волокно, формирующее полимер и катализатор; указанный способ включает формирование раствора, включающего низший спирт, воду или их смеси и приблизительно от 3 до 30 вес.% полимерного состава, при этом полимерный раствор подвергается воздействию электрического поля потенциалом более порогового потенциала в вольтах, при котором в растворе формируются ускоренные пряди раствора, которые высушивают до тонкого волокна, собирая тонкое волокно на подложке и подвергая тонкое волокно термической обработке, при этом термическая обработка повышает температуру тонкого волокна до температуре, не превышающей точки плавления полимера, формирующего волокно.24. A method of creating a thin fiber material containing fibers having a diameter of from about 0.01 to 2 μm, the fiber comprising a linear fiber forming a polymer and a catalyst; said method includes forming a solution comprising lower alcohol, water or mixtures thereof and from about 3 to 30 wt.% polymer composition, wherein the polymer solution is exposed to an electric field with a potential of more than a threshold potential in volts, in which accelerated strands of the solution are formed in the solution, which are dried to a thin fiber, collecting the thin fiber on the substrate and subjecting the thin fiber to heat treatment, while the heat treatment raises the temperature of the thin fiber to a temperature not exceeding the melting point of the fiber-forming polymer.
RU2003107850/04A 2001-05-31 2001-08-09 Fine fiber compositions, methods for preparation thereof, and a method of manufacturing fine-fiber material RU2300543C2 (en)

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