RU2001132860A - Pymetrosine Solvates - Google Patents

Pymetrosine Solvates

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Publication number
RU2001132860A
RU2001132860A RU2001132860/04A RU2001132860A RU2001132860A RU 2001132860 A RU2001132860 A RU 2001132860A RU 2001132860/04 A RU2001132860/04 A RU 2001132860/04A RU 2001132860 A RU2001132860 A RU 2001132860A RU 2001132860 A RU2001132860 A RU 2001132860A
Authority
RU
Russia
Prior art keywords
formula
pesticidal
tetra
compound
methyl
Prior art date
Application number
RU2001132860/04A
Other languages
Russian (ru)
Other versions
RU2238941C2 (en
Inventor
Стефан ГУТМАНН
Original Assignee
Зингента Партисипейшнс Аг
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Зингента Партисипейшнс Аг filed Critical Зингента Партисипейшнс Аг
Publication of RU2001132860A publication Critical patent/RU2001132860A/en
Application granted granted Critical
Publication of RU2238941C2 publication Critical patent/RU2238941C2/en

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Claims (8)

1. Соединения формулы1. Compounds of the formula
Figure 00000001
Figure 00000001
 где r и s независимо друг от друга обозначают любое число от 0,00 до 12,0; иwhere r and s independently from each other denote any number from 0.00 to 12.0; and L обозначает метанол, этанол, пропанол, изопропанол, бутанол, изобутанол, трет-бутанол, циклогексанол. тетрагидрофуриловый спирт, этиленгликоль, глицерин, метилацетат, этилацетат, этиллактат, бутиролактон, этиленкарбонат, пропиленкарбонат, ацетонитрил, диметилсульфоксид, диметилформамид, димстилацетамид, N-метил-2-пирролидон, N-октил-2-пирролидон, N-децил-2-нирролидон, ацетон, бутанон, метилизобутилкетон, метилпропилкетон, ацетофенон, циклогексанон, метиленхлорид, трихлорметан, трихлорэтан, тетрагидрофуран, диэтиловый эфир, 1,2-диметоксиэтан, диоксан, метил-трет-бутиловый эфир, этаноламин, пиридин, хлорбензол, толуол, ксилол или тетраметилмочевину; при условии, что r и s одновременно не равны 0, каждое в свободной форме или в форме соли, и их таутомеры, каждый в свободной форме или в форме соли.L is methanol, ethanol, propanol, isopropanol, butanol, isobutanol, tert-butanol, cyclohexanol. tetrahydrofuryl alcohol, ethylene glycol, glycerin, methyl acetate, ethyl acetate, ethyl lactate, butyrolactone, ethylene carbonate, propylene carbonate, acetonitrile, dimethyl sulfoxide, dimethylformamide, dimstylacetamide, N-methyl-2-pyrrolidone, N-octylidrolide, N-octylidrolidone , acetone, butanone, methyl isobutyl ketone, methylpropyl ketone, acetophenone, cyclohexanone, methylene chloride, trichloromethane, trichloroethane, tetrahydrofuran, diethyl ether, 1,2-dimethoxyethane, dioxane, methyl tert-butyl ether, ethanolamine, pyridyltetrachloro, tetra-chloro-tetra-chloro-tetra-chloro-tetra-methylbenzene, Evinu; provided that r and s are not simultaneously equal to 0, each in free or salt form, and their tautomers, each in free or salt form. 2. Соединения формулы (1) по п.1, где L. обозначает метанол.2. The compounds of formula (1) according to claim 1, where L. is methanol. 3. Соединения формулы (1) но п.1, где r равно 0 и s равно 2.3. The compounds of formula (1) but claim 1, where r is 0 and s is 2. 4. Пестицидная композиция, содержащая соединение формулы (I) но любому из пп.1-3 и один или несколько адъювантов.4. A pesticidal composition containing a compound of formula (I) but to any one of claims 1 to 3 and one or more adjuvants. 5. Способ борьбы с вредителями, предусматривающий нанесение действующего вещества формулы (1) по п.1 или композиции по п.4, содержащей это действующее вещество, в количестве, обладающем пестицидной активностью, на вредителей или место их обитания.5. A method of controlling pests, comprising applying the active substance of the formula (1) according to claim 1 or a composition according to claim 4, containing this active substance, in an amount having pesticidal activity, on the pests or their habitat. 6. Способ получения пестицидных композиций по п.4, предусматривающий приведение пестицидной смеси, включающей практически не содержащее растворитель соединение формулы (I), где r и s равны 0, в контакт с сольватирующим агентом.6. A method for producing pesticidal compositions according to claim 4, comprising bringing a pesticidal mixture comprising a practically solvent-free compound of formula (I), where r and s are 0, in contact with a solvating agent. 7. Способ получения соединения формулы (1) по п.1, согласно которому несольватированное обладающее пестицидной активностью соединение приводят в контакт с сольватирующим агентом.7. A method for producing a compound of formula (1) according to claim 1, wherein the unsolvated pesticidal compound is contacted with a solvating agent. 8. Пестицидная композиция но п.4, полученная способом, описанным в п.6.8. The pesticidal composition but in claim 4, obtained by the method described in claim 6. 7. Применение композиции по п.4 для борьбы с вредителями.7. The use of a composition according to claim 4 for pest control.
RU2001132860A 1999-05-12 2000-05-10 Pimetrozine dihydrate, method for its preparing, methods for preparing insecticide composition, insecticide composition RU2238941C2 (en)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
CH90599 1999-05-12
CH905/99 1999-05-12
CH1606/99 1999-09-03
CH160699 1999-09-03

Publications (2)

Publication Number Publication Date
RU2001132860A true RU2001132860A (en) 2003-08-20
RU2238941C2 RU2238941C2 (en) 2004-10-27

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RU2001132860A RU2238941C2 (en) 1999-05-12 2000-05-10 Pimetrozine dihydrate, method for its preparing, methods for preparing insecticide composition, insecticide composition

Country Status (26)

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US (1) US6784176B2 (en)
EP (1) EP1177189B1 (en)
JP (1) JP4824172B2 (en)
KR (1) KR100736060B1 (en)
CN (1) CN1219779C (en)
AR (1) AR035908A1 (en)
AT (1) ATE312832T1 (en)
AU (1) AU764924B2 (en)
BR (1) BR0010501B1 (en)
CA (1) CA2372156C (en)
CO (1) CO5210907A1 (en)
CY (1) CY1105396T1 (en)
CZ (1) CZ303340B6 (en)
DE (1) DE60024807T2 (en)
DK (1) DK1177189T3 (en)
DZ (1) DZ3157A1 (en)
EG (1) EG22667A (en)
ES (1) ES2252021T3 (en)
HU (1) HU229398B1 (en)
IL (1) IL145831A0 (en)
NZ (1) NZ515025A (en)
PL (1) PL202065B1 (en)
RU (1) RU2238941C2 (en)
TR (1) TR200102931T2 (en)
TW (1) TW542830B (en)
WO (1) WO2000068222A2 (en)

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EA019843B1 (en) * 2004-07-01 2014-06-30 Е. И. Дюпон Де Немур Энд Компани Synergistic mixtures of anthranilamide invertebrate pest control agents

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TWI280128B (en) 2002-05-22 2007-05-01 Smithkline Beecham Corp 3'-[(2Z)-[1-(3,4- dimethylphenyl)-1,5-dihydro-3-methyl-5-oxo-4H-pyrazol-4-ylidene]hydrazino]-2'-hydroxy-[1,1'-biphenyl]-3-carboxylic acid bis-(monoethanolamine)
WO2007115967A1 (en) * 2006-04-12 2007-10-18 F. Hoffmann-La Roche Ag Crystalline isopropanol solvate of glucokinase activator
ECSP077628A (en) 2007-05-03 2008-12-30 Smithkline Beechman Corp NEW PHARMACEUTICAL COMPOSITION
EP2002722A1 (en) * 2007-06-15 2008-12-17 Syngeta Participations AG Methods of controlling insects
GB0811300D0 (en) * 2008-06-19 2008-07-30 Syngenta Participations Ag Methods of controlling neonicotinoid resistant insects
US8609693B2 (en) 2009-05-29 2013-12-17 Glaxosmithkline Llc Methods of administration of thrombopoietin agonist compounds
WO2011134816A1 (en) 2010-04-27 2011-11-03 Syngenta Participations Ag Methods of controlling neonicotinoid resistant aphids
EP2776381B1 (en) 2011-11-07 2016-06-01 3M Innovative Properties Company Method for selectively treating the surface of dental ceramic
US10028809B2 (en) 2012-10-17 2018-07-24 3M Innovative Properties Company Multi sectional dental zirconia milling block, process of production and use thereof
CN103098799B (en) * 2013-02-02 2016-08-03 广东中迅农科股份有限公司 Pymetrozine and azone suspended emulsion and preparation method thereof
WO2015096013A1 (en) 2013-12-23 2015-07-02 Dow Global Technologies Llc Pymetrozine formulations
MA41827A (en) * 2015-03-27 2018-01-30 Pharmacyclics Llc SOLVATED FORMS OF A BRUTON TYROSINE KINASE INHIBITOR
CN107935689A (en) * 2017-11-29 2018-04-20 章立功 A kind of disease-resistant pear tree fertilizer
CN112538070B (en) * 2020-12-02 2023-04-07 天津大学 Pymetrozine-p-hydroxybenzoic acid eutectic crystal and preparation method thereof

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DE3853662D1 (en) * 1987-10-16 1995-06-01 Ciba Geigy Ag Pesticides.
US5384403A (en) * 1993-03-31 1995-01-24 Ciba-Geigy Corporation Process for the preparation of aminotriazine derivatives

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EA019843B1 (en) * 2004-07-01 2014-06-30 Е. И. Дюпон Де Немур Энд Компани Synergistic mixtures of anthranilamide invertebrate pest control agents
EA019922B1 (en) * 2004-07-01 2014-07-30 Е.И. Дюпон Де Немур Энд Компани Synergistic mixtures of anthranilamide compounds for controlling invertebrate pests

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