RO97372B1 - Process for preparing 2-benzoyl 1,3,5-cyclohexanetrione - Google Patents
Process for preparing 2-benzoyl 1,3,5-cyclohexanetrioneInfo
- Publication number
- RO97372B1 RO97372B1 RO128501A RO12850187A RO97372B1 RO 97372 B1 RO97372 B1 RO 97372B1 RO 128501 A RO128501 A RO 128501A RO 12850187 A RO12850187 A RO 12850187A RO 97372 B1 RO97372 B1 RO 97372B1
- Authority
- RO
- Romania
- Prior art keywords
- benzoyl
- cyanide
- mol
- cyclohexanetrione
- preparing
- Prior art date
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Inventia se refera la un procedeu de preparare a unor derivati de 2-benzoil-1, 3, 5-ciclohexantrione prin reactia unei trione cu un compus benzoil substituit, în raport molar de 1 : 1, la 0...50 degree C, în mediu de dimetilformamida, esterul enolic format reactioneaza apoi cu 1...4 mol baza moderata aleasa dintre trialchilamine cu 1...6 atomi, pirida, carbonat sau fosfat de sodiu si cu 0,01...0,5 mol sursa de cianura aleasa dintre cianuri alcaline, cianhidrine, cianura de zinc sau acid cianhidric la 20...40 degree C.The invention relates to a process for the preparation of 2-benzoyl-1,3,5-cyclohexanetriones by reacting a trione with a substituted benzoyl compound in a molar ratio of 1: 1 to 0 ... 50 ° C, in the dimethylformamide medium, the enolic ester formed is then reacted with 1-4 mol of the moderate base chosen from 1 to 6 trialkylamines, pyridine, carbonate or sodium phosphate and from 0.01 to 0.5 mol of the source of the cyanide chosen from alkali cyanides, cyanohydrins, zinc cyanide or hydrogen cyanide at 20 ... 40 degrees C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| RO128501A RO97372B1 (en) | 1987-06-05 | 1987-06-05 | Process for preparing 2-benzoyl 1,3,5-cyclohexanetrione |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| RO128501A RO97372B1 (en) | 1987-06-05 | 1987-06-05 | Process for preparing 2-benzoyl 1,3,5-cyclohexanetrione |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| RO97372B1 true RO97372B1 (en) | 1989-08-02 |
Family
ID=40905607
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RO128501A RO97372B1 (en) | 1987-06-05 | 1987-06-05 | Process for preparing 2-benzoyl 1,3,5-cyclohexanetrione |
Country Status (1)
| Country | Link |
|---|---|
| RO (1) | RO97372B1 (en) |
-
1987
- 1987-06-05 RO RO128501A patent/RO97372B1/en unknown
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