PT90794A - METHOD FOR THE MANUFACTURE OF CRYSTALS OF BARIUM AND / OR STRONIUM TITANATE - Google Patents
METHOD FOR THE MANUFACTURE OF CRYSTALS OF BARIUM AND / OR STRONIUM TITANATEInfo
- Publication number
- PT90794A PT90794A PT90794A PT9079489A PT90794A PT 90794 A PT90794 A PT 90794A PT 90794 A PT90794 A PT 90794A PT 9079489 A PT9079489 A PT 9079489A PT 90794 A PT90794 A PT 90794A
- Authority
- PT
- Portugal
- Prior art keywords
- barium
- oxide
- alcoholate
- crystals
- strontium
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/003—Titanates
- C01G23/006—Alkaline earth titanates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/02—Amorphous compounds
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Compositions Of Oxide Ceramics (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
Abstract
An amorphous powder of titanium oxide and of barium and/or strontium oxide is precipitated by the hydrolysis of titanium alcoholate in the presence of barium oxide, hydroxide or alcoholate or strontium oxide, hydroxide or alcoholate and an acid organic compound containing more than 6 carbon atoms, and the amorphous powder is heated while being treated with a stream of gas containing water vapour, ammonia or CO2, to crystallize the barium or strontium titanate and distill off the acid organic compound. The barium or strontium titanate crystals are less than one micron in size and have an irregular, angular morphology.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
BE8800674A BE1001780A4 (en) | 1988-06-13 | 1988-06-13 | Method for barium titanate crystal manufacturing and / or strontium and barium titanate crystals and / or strontium. |
Publications (2)
Publication Number | Publication Date |
---|---|
PT90794A true PT90794A (en) | 1989-12-29 |
PT90794B PT90794B (en) | 1994-10-31 |
Family
ID=3883464
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PT90794A PT90794B (en) | 1988-06-13 | 1989-06-09 | METHOD FOR THE MANUFACTURE OF CRYSTALS OF BARIUM AND / OR STRONIUM TITANATE |
Country Status (13)
Country | Link |
---|---|
US (1) | US5032375A (en) |
EP (1) | EP0346962B1 (en) |
JP (1) | JPH0280321A (en) |
KR (1) | KR900000296A (en) |
CN (1) | CN1039396A (en) |
AT (1) | ATE89241T1 (en) |
AU (1) | AU621375B2 (en) |
BE (1) | BE1001780A4 (en) |
CA (1) | CA1322099C (en) |
DE (1) | DE68906463D1 (en) |
DK (1) | DK285689A (en) |
NO (1) | NO892396L (en) |
PT (1) | PT90794B (en) |
Families Citing this family (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
IT1270828B (en) * | 1993-09-03 | 1997-05-13 | Chon Int Co Ltd | PROCESS FOR THE SYNTHESIS OF CRYSTAL CERAMIC POWDERS OF PEROVSKITE COMPOUNDS |
CN1063732C (en) * | 1994-05-06 | 2001-03-28 | 清华大学 | Method for making strontium titanate base grain-boundary layer capacitor material |
US5814272A (en) * | 1996-02-21 | 1998-09-29 | Millipore Corporation | Method for forming dendritic metal particles |
WO1999059918A1 (en) * | 1998-05-20 | 1999-11-25 | Toho Titanium Co., Ltd. | Barium titanate powder |
CN1082491C (en) * | 1998-06-12 | 2002-04-10 | 中国科学院青海盐湖研究所 | Process for preparing nm-class strontium titanate |
KR100630285B1 (en) * | 1998-08-19 | 2006-09-29 | 쇼와 덴코 가부시키가이샤 | Finely particulate titanium-containing substance, coating fluid containing the same, processes for producing these, and molded article having thin film comprising the substance |
US6613303B1 (en) * | 1998-10-13 | 2003-09-02 | Eurotope Entwicklungsgesellschaft für Isotopentechnologien mbh | Highly radioactive miniaturized ceremic strontium 90 radiation sources and method for the production thereof |
MXPA02001885A (en) * | 1999-08-23 | 2002-11-04 | Cabot Corp | Silicate based sintering aid and method. |
JP3735686B2 (en) * | 2001-10-30 | 2006-01-18 | 独立行政法人理化学研究所 | Method for producing metal oxide ferroelectric particle crystal |
KR100633723B1 (en) * | 2005-08-04 | 2006-10-13 | 한화석유화학 주식회사 | Process for preparing barium titanate |
JP5119008B2 (en) * | 2008-03-04 | 2013-01-16 | 日本化学工業株式会社 | Method for producing perovskite-type barium titanate powder |
CN103011807B (en) * | 2012-12-17 | 2014-04-02 | 内蒙古自治区冶金研究院 | Method for preparing strontium titanate powder |
CN103613125B (en) * | 2013-11-05 | 2015-10-28 | 清华大学 | A kind of Ultrafine titanate nano powder and preparation method thereof |
GB201405258D0 (en) * | 2014-03-24 | 2014-05-07 | Univ Birmingham | Controlled atom source |
CN113562743B (en) * | 2021-08-19 | 2022-10-18 | 上海大学(浙江·嘉兴)新兴产业研究院 | Ammonia gas concentration and recovery device, barium titanate production equipment and barium titanate production method |
Family Cites Families (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3331659A (en) * | 1964-03-31 | 1967-07-18 | Malloy Frank | Process for producing lead titanate powder |
US3647364A (en) * | 1970-01-06 | 1972-03-07 | Us Air Force | Process for producing high-purity submicron barium and strontium titanate powders |
US4061583A (en) * | 1974-03-13 | 1977-12-06 | Murata Manufacturing Co., Ltd. | Preparation of titanates |
US4487755A (en) * | 1982-07-01 | 1984-12-11 | General Electric Company | Preparation of large crystal sized barium and/or strontium titanate powder |
JPS5945928A (en) * | 1982-09-08 | 1984-03-15 | Sony Corp | Preparation of fine particle from strontium titanate |
US4534956A (en) * | 1983-07-08 | 1985-08-13 | General Electric Company | Molten salt synthesis of barium and/or strontium titanate powder |
EP0141551B1 (en) * | 1983-10-12 | 1988-02-03 | Asahi Kasei Kogyo Kabushiki Kaisha | Titanate powder and process for producing the same |
JPS6183603A (en) * | 1984-09-07 | 1986-04-28 | Agency Of Ind Science & Technol | Preparation of amorphous compound metal oxide |
FR2571713B1 (en) * | 1984-10-15 | 1990-03-23 | Centre Nat Rech Scient | PROCESS FOR THE PREPARATION OF TITANATES, ZIRCONATES AND STANNATES |
FR2593166A1 (en) * | 1986-01-20 | 1987-07-24 | Solvay | PROCESS FOR PRODUCING A METAL OXIDE POWDER FOR CERAMIC MATERIALS AND ZIRCONIA POWDER OBTAINED THEREBY |
BE1001832A4 (en) * | 1987-03-26 | 1990-03-20 | Solvay | Method for producing a powder mixed metal oxide and mixed metal oxide powder. |
FR2617151B1 (en) * | 1987-06-29 | 1990-10-12 | Solvay | PROCESS FOR THE MANUFACTURE OF MIXED METAL OXIDE POWDER, AND MIXED METAL OXIDE POWDERS |
-
1988
- 1988-06-13 BE BE8800674A patent/BE1001780A4/en not_active IP Right Cessation
-
1989
- 1989-05-23 US US07/356,502 patent/US5032375A/en not_active Expired - Fee Related
- 1989-06-01 DE DE8989201394T patent/DE68906463D1/en not_active Expired - Lifetime
- 1989-06-01 EP EP89201394A patent/EP0346962B1/en not_active Expired - Lifetime
- 1989-06-01 AT AT89201394T patent/ATE89241T1/en not_active IP Right Cessation
- 1989-06-02 KR KR1019890007615A patent/KR900000296A/en not_active Application Discontinuation
- 1989-06-09 PT PT90794A patent/PT90794B/en not_active IP Right Cessation
- 1989-06-12 DK DK285689A patent/DK285689A/en not_active Application Discontinuation
- 1989-06-12 CA CA000602427A patent/CA1322099C/en not_active Expired - Fee Related
- 1989-06-12 NO NO89892396A patent/NO892396L/en unknown
- 1989-06-13 AU AU36339/89A patent/AU621375B2/en not_active Ceased
- 1989-06-13 JP JP1152078A patent/JPH0280321A/en active Pending
- 1989-06-13 CN CN89104049A patent/CN1039396A/en active Pending
Also Published As
Publication number | Publication date |
---|---|
NO892396L (en) | 1989-12-14 |
EP0346962A1 (en) | 1989-12-20 |
US5032375A (en) | 1991-07-16 |
PT90794B (en) | 1994-10-31 |
EP0346962B1 (en) | 1993-05-12 |
BE1001780A4 (en) | 1990-03-06 |
DE68906463D1 (en) | 1993-06-17 |
DK285689A (en) | 1989-12-14 |
KR900000296A (en) | 1990-01-30 |
DK285689D0 (en) | 1989-06-12 |
CN1039396A (en) | 1990-02-07 |
AU621375B2 (en) | 1992-03-12 |
ATE89241T1 (en) | 1993-05-15 |
AU3633989A (en) | 1989-12-14 |
NO892396D0 (en) | 1989-06-12 |
JPH0280321A (en) | 1990-03-20 |
CA1322099C (en) | 1993-09-14 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FG3A | Patent granted, date of granting |
Effective date: 19940419 |
|
MM3A | Annulment or lapse |
Free format text: LAPSE DUE TO NON-PAYMENT OF FEES Effective date: 19951031 |