PL6641B1 - A method of purifying carbonic acid from carbonic acid secretions. - Google Patents

A method of purifying carbonic acid from carbonic acid secretions. Download PDF

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Publication number
PL6641B1
PL6641B1 PL6641A PL664121A PL6641B1 PL 6641 B1 PL6641 B1 PL 6641B1 PL 6641 A PL6641 A PL 6641A PL 664121 A PL664121 A PL 664121A PL 6641 B1 PL6641 B1 PL 6641B1
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PL
Poland
Prior art keywords
carbonic acid
action
purifying
acid
secretions
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Application number
PL6641A
Other languages
Polish (pl)
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Publication date
Application filed filed Critical
Publication of PL6641B1 publication Critical patent/PL6641B1/en

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Description

Kwas weglowy, pochodzacy z wydziela¬ czy kwasu weglowego przy aparatach do wytwarzania amottijaku, a zawierajacy przecietnie 90% C02, jednak zanieczy¬ szczony siarkowodorem, fenolem,, naftalina, pirydyna, substancjami empireiimatyczne- mi, a nawet kwasem pruskim, musial wla¬ snie z powodu tych zanieczyszczen, które go dotad czynily niezdatnym do zadnego uzytku, uchodzic w powietrze, co znowu ze wzgledów higjenicznych nie bylo calkiem bez zarzutu* W mysl wynalazku zwalnia sie kwas ten, bardzo stezony, a tworzacy przy¬ kry produkt odpadkowy, od wsizelkich za¬ nieczyszczen przez metodyczne postepowa¬ nie, czyli przemienia ten kwas weglowy w wysokowartosciowy produkt, nadajacy sie znakomicie do zastosowania w przemysle chemicznym, a nawet do sporzadzania na¬ pojów. Niniejszy sposób polega na tern, ze kwas weglowy, pochodzacy z wydzielaczy kwasu weglowego, przechodzi pokolei przez wode, wadzian tlenku zelazowego, przez mase oczyszczajaca Lux'a, stezony kwas siarkowy, olej parafinowy lub miiine- ralny, a wreszcie przez wegiel kostny.Woda wyciaga z kwasu weglowego pew¬ na czesc wszystkich zanieczyszczen; masa oczyszczajaca Lux'a wydala siarkowodór i kwas pruski, a oczyszczania tego dokoncza koncentrowany kwas siarkowy, który nie- tylko osusza kwas weglowy i niszczy ostat¬ nie slady kwasu pruisjkiego, wzgledne je pochlania, lecz takze usuwa zasadowe za¬ nieczyszczenia kwasu weglowego, jak pi¬ rydyne oraz produkty empireumatyczne,których ostatnie slady wydala olej parafi¬ nowy lub mineralny, podczas gdy przetlo- czenie kwasu weglowego przez wegiel kost¬ ny czyni kwas weglowy zupelnie bezwon- nym. Oczyszczony w ten spoteób calkowicie kwas weglowy mozna uzyc takze do skra¬ plania i d)o innyh celów, gdzie rozchodzi sie w wysokim stopniu o czystosc i silne stezenie kwasu weglowego. PLCarbonic acid, derived from the release of carbonic acid in the amothijac apparatus, and containing an average of 90% CO2, but contaminated with hydrogen sulphide, phenol, naphthaline, pyridine, empireimatic substances, and even prussian acid, must have poured in. because of these impurities, which so far made it unusable, it could escape into the air, which again, for hygienic reasons, was not completely flawless. * According to the invention, this acid, very concentrated, and an odorous waste product, is released from all It is contaminated by a methodical procedure, that is, it transforms this carbonic acid into a high-quality product, perfectly suited for use in the chemical industry and even for making drinks. The present method is based on the fact that carbonic acid, which is derived from carbonic acid extractors, passes through water, ferric oxide hydrate, through Lux cleansing mass, concentrated sulfuric acid, paraffinic or mineral oil, and finally through bone carbon. extracts some of all impurities from carbonic acid; Lux's cleansing mass expels hydrogen sulfide and prussic acid, and this purification is accomplished by concentrated sulfuric acid, which not only dries the carbonic acid and destroys the last traces of Prusic acid, or absorbs them, but also removes alkaline carbonic acid impurities, such as pyridines and empireumatic products, the last traces of which are released by paraffin or mineral oil, while transferring carbonic acid through bone carbon renders the carbonic acid completely odorless. The carbonic acid purified in this way can also be used for condensation and d) for other purposes, where it is largely pure and a strong concentration of carbonic acid. PL

Claims (1)

1. Zastrzezenie patentowe. Sposób oczyszczania kwasu weglowego, uchodzacego po dysocjacji zwiazków amc- njakowych z wydzielaczy kwasu weglowe¬ go, praktycznie biorac wolnego od amon ja¬ ku, lecz zanieczyszczonego siarkowodorem, zwiazkami cyjamowemi, fenolem, naftale¬ nem, pirydyna i substancjami enipiretuna- tyczinemi, znamienny tern, ze kwas weglo¬ wy poddaje isie najpierw dzialaniu zAmneij wody, nastepnie dzialaniu wódziami tlenku zelazowego i poteim dizialajniu kwasu siar¬ kowego 'stezonego, wreszcie dzialaniu oleju parafinowego lub mineralnego, a wkoncu poddaje sie go filtrowianiiu przez wegiel kostny. E r n si t K u b i n. Zajstepca: M. Brokman, rzecznik patentowy. Druk L. Boguslawskiego, Warsiawa. PL1. Patent claim. A method of purifying carbonic acid, escaping after the dissociation of ammonium compounds from carbonic acid separators, taking practically ammonium-free but contaminated with hydrogen sulfide, cyam compounds, phenol, naphthalene, pyridine and eniprethinemic substances, characterized by that the carbonic acid is first subjected to the action of mild water, then to the action of ferric oxide and then to the action of concentrated sulfuric acid, finally to the action of paraffin or mineral oil, and finally it is filtered by bone charcoal. E r n si t K u b i n. Zajstepca: M. Brokman, patent attorney. Printed by L. Boguslawski, Warsiawa. PL
PL6641A 1921-06-13 A method of purifying carbonic acid from carbonic acid secretions. PL6641B1 (en)

Publications (1)

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PL6641B1 true PL6641B1 (en) 1927-02-28

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