PL49230B1 - - Google Patents
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- Publication number
- PL49230B1 PL49230B1 PL100095A PL10009562A PL49230B1 PL 49230 B1 PL49230 B1 PL 49230B1 PL 100095 A PL100095 A PL 100095A PL 10009562 A PL10009562 A PL 10009562A PL 49230 B1 PL49230 B1 PL 49230B1
- Authority
- PL
- Poland
- Prior art keywords
- formula
- hal
- lower alkyl
- chlorine
- acyl residue
- Prior art date
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- RWRDLPDLKQPQOW-UHFFFAOYSA-N Pyrrolidine Chemical compound C1CCNC1 RWRDLPDLKQPQOW-UHFFFAOYSA-N 0.000 claims 3
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims 2
- NQRYJNQNLNOLGT-UHFFFAOYSA-N Piperidine Chemical compound C1CCNCC1 NQRYJNQNLNOLGT-UHFFFAOYSA-N 0.000 claims 2
- 125000002252 acyl group Chemical group 0.000 claims 2
- 125000000217 alkyl group Chemical group 0.000 claims 2
- 239000000460 chlorine Substances 0.000 claims 2
- 229910052801 chlorine Inorganic materials 0.000 claims 2
- CHRAJVQLWOMYQI-SCZZXKLOSA-N (1s,5r)-5,8,8-trimethyl-3-azabicyclo[3.2.1]octane Chemical group C1NC[C@H]2CC[C@]1(C)C2(C)C CHRAJVQLWOMYQI-SCZZXKLOSA-N 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 125000004442 acylamino group Chemical group 0.000 claims 1
- 150000001412 amines Chemical class 0.000 claims 1
- 125000003710 aryl alkyl group Chemical group 0.000 claims 1
- 125000003118 aryl group Chemical group 0.000 claims 1
- NHOWLEZFTHYCTP-UHFFFAOYSA-N benzylhydrazine Chemical class NNCC1=CC=CC=C1 NHOWLEZFTHYCTP-UHFFFAOYSA-N 0.000 claims 1
- 239000011230 binding agent Substances 0.000 claims 1
- 125000001246 bromo group Chemical group Br* 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 claims 1
- 125000000753 cycloalkyl group Chemical group 0.000 claims 1
- 239000012433 hydrogen halide Substances 0.000 claims 1
- 229910000039 hydrogen halide Inorganic materials 0.000 claims 1
- 238000000034 method Methods 0.000 claims 1
- 229910052757 nitrogen Inorganic materials 0.000 claims 1
- 125000004433 nitrogen atom Chemical group N* 0.000 claims 1
- 239000003960 organic solvent Substances 0.000 claims 1
- 150000003839 salts Chemical class 0.000 claims 1
- 229920006395 saturated elastomer Polymers 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
Claims (1)
1. Zastrzezenie p a t entowe Sposób wytwarzania nowych dwuchlorowcoamd- nobenzyloamin o wzorze 1, w którym Hal ozna¬ cza atom chloru lub wod^a^symbole R i R' sa takie same lub rózne i oznaczaja nizsze reszty alkilowe, nasycone lub nienasycone, o lancuchu prostym lub rozgalezionym, reszty cykloalkilo- we, aralkilowe lub arylowe, albo razem z ato¬ mem azotu oznaczaja pierscienie pirolidynowy, piperydynowy lub kamfidynowy, ewentualnie podstawione nizszymi resztami alkilowymi zna¬ mienny tym, ze aminobenzyloaminy o wzorze 2, w którym R i R' maja wyzej podane znaczenie chloruje sie lub bromuje w obecnosci obojetne¬ go organicznego rozpuszczalnika, lub acyloami- nodwuchlorowcobenzyloaminy o wzorze 3, w którym grupy oznaczone symbolem Hal sa takie same lub rózne i oznaczaja atomy chloru lub bromu, a Ac oznacza dowolna reszte acylowa, poddaje sie reakcji z aminami o wzorze 4, w któ¬ rym R i R' maja wyzej podane znaczenie, w obecnosci srodka wiazacego chlorowcowodór, a nastepnie odszczepia sie reszte acylowa, lub dwuchlorowconitrobenzyloaminy o wzorze 5, w którym Hal, RiR' maja wyzej podane znacze¬ nie redukuje sie, a otrzymane zwiazki ewentual¬ nie przeprowadza sie w sole addycyjne z kwa¬ sami.49230 R /VCH- h/zóff H2N CH2-N< R' Wzór. Z CH2 —Hal Ac-HN / R HN Wzór 4 R R Ha{ Y^NH2 Hal Nzór6 -N R Ri Ha£ Yl~CH; —N / R H.N I 2 Hal A/zdf 749230 - A/zórS 2 \ /CH2 -CH2-CH-CH3 ca -CH2-CH-CH3 Wzó* 10 -CH2-CH2 -CHZ-CH, Wzór 11 Cli -CH« CH- HjC-C-CWj —CH. -CH-CH^ 2 ~'2^CH. -CH2-CH2 2 /•zd*« Wzóf # PL
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PL49230B1 true PL49230B1 (pl) | 1965-02-15 |
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