PL48686B1 - - Google Patents
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- Publication number
- PL48686B1 PL48686B1 PL101941A PL10194163A PL48686B1 PL 48686 B1 PL48686 B1 PL 48686B1 PL 101941 A PL101941 A PL 101941A PL 10194163 A PL10194163 A PL 10194163A PL 48686 B1 PL48686 B1 PL 48686B1
- Authority
- PL
- Poland
- Prior art keywords
- weight
- parts
- mixed
- dibutyl phthalate
- stearin
- Prior art date
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- DOIRQSBPFJWKBE-UHFFFAOYSA-N dibutyl phthalate Chemical compound CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 claims description 8
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 5
- 229920005989 resin Polymers 0.000 claims description 5
- 239000011347 resin Substances 0.000 claims description 5
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims description 4
- DCXXMTOCNZCJGO-UHFFFAOYSA-N Glycerol trioctadecanoate Natural products CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 claims description 4
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 claims description 3
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 claims description 3
- 239000004359 castor oil Substances 0.000 claims description 3
- 235000019438 castor oil Nutrition 0.000 claims description 3
- ZXJXZNDDNMQXFV-UHFFFAOYSA-M crystal violet Chemical compound [Cl-].C1=CC(N(C)C)=CC=C1[C+](C=1C=CC(=CC=1)N(C)C)C1=CC=C(N(C)C)C=C1 ZXJXZNDDNMQXFV-UHFFFAOYSA-M 0.000 claims description 3
- 235000011187 glycerol Nutrition 0.000 claims description 3
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims description 3
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 claims description 3
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 claims description 3
- 239000003921 oil Substances 0.000 claims description 2
- MILSYCKGLDDVLM-UHFFFAOYSA-N 2-phenylpropan-2-ylbenzene Chemical class C=1C=CC=CC=1C(C)(C)C1=CC=CC=C1 MILSYCKGLDDVLM-UHFFFAOYSA-N 0.000 claims 1
- 235000004443 Ricinus communis Nutrition 0.000 claims 1
- 210000002445 nipple Anatomy 0.000 claims 1
- 229920003002 synthetic resin Polymers 0.000 claims 1
- 239000000057 synthetic resin Substances 0.000 claims 1
- BUZMJVBOGDBMGI-UHFFFAOYSA-N 1-phenylpropylbenzene Chemical compound C=1C=CC=CC=1C(CC)C1=CC=CC=C1 BUZMJVBOGDBMGI-UHFFFAOYSA-N 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000002202 Polyethylene glycol Substances 0.000 description 1
- 229920000180 alkyd Polymers 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- XNGIFLGASWRNHJ-UHFFFAOYSA-L phthalate(2-) Chemical compound [O-]C(=O)C1=CC=CC=C1C([O-])=O XNGIFLGASWRNHJ-UHFFFAOYSA-L 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
Description
Opublikowano: 30.XI.1964 48686 KI. 22 g, UJA<£ MKP UKD |3IBL. '¦ Wspóltwórcy wynalazku: mgr Wiktor Klein, mgr inz. Teresa Siadak-Fal- kowska, Jadwiga Pietraszek, Ignacy Mirtynski, Stefan Laczny, Kazimierz Stokaluk, Stanislaw Sanak Wlasciciel patentu: Spóldzielnia Pracy Wytwórczosci Róznej „Impreg- nacja", Kraków(Polska) Sposób wytwarzania pasty do dlugopisów Przedmiotem wynalazku jest sposób wytwarza¬ nia pasty do dlugopisów, przy zastosowaniu kra¬ jowych surowców.Dotychczas stosowane pasty zawieraja miedzy innymi jako glówne skladniki: zywice abietofor- niofenolowa wzglednie zywice alkidowa modyfi¬ kowana olejem rycynowym, glikol polietylenowy, alkohol benzylowy i odpowiednie barwniki.Sposób wytwarzania pasty do dlugopisów wedlug wynalazku polega na zastosowaniu zywicy dwufe- nylopropanowej modyfikowanej kalafonia i estry¬ fikowanej gliceryna lub pentaerytrytem i odpo¬ wiednim polaczeniu w okreslonych warunkach temperatury z pozostalymi skladnikami: ftalanem dwubutylu, olejem rycynowym i stearyna.Pasta otrzymana tym sposobem jest produktem jednorodnym, bardzo dobrze splywa z kulki dlugo¬ pisu, jest malo wrazliwa na zmiany temperatury, a iprzy tym ma wszystkie cechy wymagane przy odbiorze technicznym tego rodzaju produktów.Sposób otrzymywania pasty polega na tym, ze rozdrobniona zywice dwufenylopropanowa modyfi¬ kowana kalafonia i estryfikowana gliceryna lub pentaerytrytem w ilosci 260 czesci wagowych mie¬ sza sie z 260 czesciami wagowymi oleju rycyno¬ wego, przy zachowaniu temperatury 180°C, po czym dodaje sie 292 czesci wagowe ftalanu dwubutylo- 10 15 20 25 2 wego i saczy sie ten roztwór przez nucze. Nastep¬ nie topi sie w drugim mieszalniku 104 czesci wa¬ gowe stearyny w temperaturze 57°C i dodaje fio¬ letu metylowego. Po rozpuszczeniu barwnika w cieklej stearynie przelewa sie te ciecz do poprzed¬ nio otrzymanego roztworu i miesza sie przy rów¬ noczesnym ogrzewaniu do temperatury 80°C. PLPublished: 30.XI.1964 48686 IC. 22 g, UJA <£ MKP UKD | 3IBL. '¦ Co-authors of the invention: mgr Wiktor Klein, mgr inz. Teresa Siadak-Falkowska, Jadwiga Pietraszek, Ignacy Mirtynski, Stefan Laczny, Kazimierz Stokaluk, Stanislaw Sanak The owner of the patent: Spółdzielnia Pracy Wytwórczosci Róznej "Impreg- nacja", Krakow (Poland) The method of producing pen paste The subject of the invention is a method of producing pen paste using domestic raw materials. Pastes used so far contain, among others, as the main components: abietophenol resins or alkyd resins modified with castor oil, polyethylene glycol, The method of producing the pen paste according to the invention is based on the use of a diphenylpropane resin modified with rosin and esterified with glycerin or pentaerythritol and appropriate combination, under certain temperature conditions, with the other components: dubicutyl phthalate and rearin oil. thus obtained is the product of one thing It is not very sensitive to temperature changes, and at the same time has all the features required for technical acceptance of this type of product. The method of obtaining the paste consists in the fact that fragmented diphenylpropane resin, modified rosin and esterified glycerin or pentaerythritol in an amount of 260 parts by weight is mixed with 260 parts by weight of castor oil, maintaining a temperature of 180 ° C, then 292 parts by weight of dibutyl phthalate are added and the solution is sucked by suction. . 104 parts by weight of stearin are then melted in a second mixer at 57 ° C. and methyl violet is added. After the dye is dissolved in the liquid stearin, the liquid is poured into the previously prepared solution and mixed while heating to 80 ° C. PL
Claims (1)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PL48686B1 true PL48686B1 (en) | 1964-10-15 |
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