PL443290A1 - Sposób wytwarzania destylatów wzbogaconych w α- i β-kwasy (humulony i lupulony) z surowego ekstraktu chmielowego - Google Patents

Sposób wytwarzania destylatów wzbogaconych w α- i β-kwasy (humulony i lupulony) z surowego ekstraktu chmielowego

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Publication number
PL443290A1
PL443290A1 PL443290A PL44329022A PL443290A1 PL 443290 A1 PL443290 A1 PL 443290A1 PL 443290 A PL443290 A PL 443290A PL 44329022 A PL44329022 A PL 44329022A PL 443290 A1 PL443290 A1 PL 443290A1
Authority
PL
Poland
Prior art keywords
sup
lupulones
humulones
enriched
acids
Prior art date
Application number
PL443290A
Other languages
English (en)
Other versions
PL247884B1 (pl
Inventor
Zygmunt Fekner
Edward Rój
Katarzyna Tyśkiewicz
Marcin Gruba
Agnieszka Dębczak
Marcin Konkol
Original Assignee
Sieć Badawcza Łukasiewicz - Instytut Nowych Syntez Chemicznych
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sieć Badawcza Łukasiewicz - Instytut Nowych Syntez Chemicznych filed Critical Sieć Badawcza Łukasiewicz - Instytut Nowych Syntez Chemicznych
Priority to PL443290A priority Critical patent/PL247884B1/pl
Publication of PL443290A1 publication Critical patent/PL443290A1/pl
Publication of PL247884B1 publication Critical patent/PL247884B1/pl

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12C—BEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
    • C12C3/00—Treatment of hops
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/12—Molecular distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/587—Unsaturated compounds containing a keto groups being part of a ring
    • C07C49/703—Unsaturated compounds containing a keto groups being part of a ring containing hydroxy groups
    • C07C49/743—Unsaturated compounds containing a keto groups being part of a ring containing hydroxy groups having unsaturation outside the rings, e.g. humulones, lupulones
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12C—BEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
    • C12C3/00—Treatment of hops
    • C12C3/04—Conserving; Storing; Packing
    • C12C3/08—Solvent extracts from hops
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12C—BEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
    • C12C3/00—Treatment of hops
    • C12C3/12—Isomerised products from hops

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Food Science & Technology (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Przedmiotem zgłoszenia jest sposób destylacji molekularnej ekstraktów chmielowych charakteryzujący się tym, że ekstrakt chmielowy po upłynnieniu w temperaturze 70°C poddaje się destylacji w temperaturze 115°C, ciśnieniu poniżej 10<sup>-1</sup> Pa, przepływie 75 ml dm<sup>-2</sup> h<sup>-1</sup>, w wyniku czego otrzymuje się strumień destylatu D1 i pozostałości R1. Pozostałość R1 poddaje się ponownej destylacji przy temperaturze 117°C, ciśnieniu poniżej 10<sup>-1</sup> Pa, przepływie 56 ml dm<sup>-2</sup> h<sup>-1</sup>, uzyskując strumień destylatu D2 i pozostałości R2. Korzystnie pozostałość R2 poddaje się kolejnej destylacji molekularnej przy temperaturze 119°C, ciśnieniu poniżej 10<sup>-1</sup> Pa, przepływie 47 ml dm<sup>-2</sup> h<sup>-1</sup>. Uzyskane destylaty D2 i D3 łączy  się i miesza w celu uzyskania finalnego destylatu.
PL443290A 2022-12-23 2022-12-23 Sposób wytwarzania destylatów wzbogaconych w α- i β-kwasy (humulony i lupulony) z surowego ekstraktu chmielowego PL247884B1 (pl)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL443290A PL247884B1 (pl) 2022-12-23 2022-12-23 Sposób wytwarzania destylatów wzbogaconych w α- i β-kwasy (humulony i lupulony) z surowego ekstraktu chmielowego

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL443290A PL247884B1 (pl) 2022-12-23 2022-12-23 Sposób wytwarzania destylatów wzbogaconych w α- i β-kwasy (humulony i lupulony) z surowego ekstraktu chmielowego

Publications (2)

Publication Number Publication Date
PL443290A1 true PL443290A1 (pl) 2024-06-24
PL247884B1 PL247884B1 (pl) 2025-09-15

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
PL443290A PL247884B1 (pl) 2022-12-23 2022-12-23 Sposób wytwarzania destylatów wzbogaconych w α- i β-kwasy (humulony i lupulony) z surowego ekstraktu chmielowego

Country Status (1)

Country Link
PL (1) PL247884B1 (pl)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1133515A (en) * 1966-09-01 1968-11-13 Alan Poyser Improvements relating to box-shaped containers suitable for growing plants
US4160787A (en) * 1975-04-02 1979-07-10 G.I.E. Tepral Process for extracting bitter flavoring principles from hops
US4918240A (en) * 1988-08-15 1990-04-17 Kalamazoo Holdings, Inc. Purification of beta acids for hydrogenolysis and such purified beta acids
CZ2011216A3 (cs) * 2011-04-14 2012-02-29 Chmelarský institut, s. r. o. Zpusob prípravy cistých beta kyselin chmele

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1133515A (en) * 1966-09-01 1968-11-13 Alan Poyser Improvements relating to box-shaped containers suitable for growing plants
US4160787A (en) * 1975-04-02 1979-07-10 G.I.E. Tepral Process for extracting bitter flavoring principles from hops
US4918240A (en) * 1988-08-15 1990-04-17 Kalamazoo Holdings, Inc. Purification of beta acids for hydrogenolysis and such purified beta acids
CZ2011216A3 (cs) * 2011-04-14 2012-02-29 Chmelarský institut, s. r. o. Zpusob prípravy cistých beta kyselin chmele

Also Published As

Publication number Publication date
PL247884B1 (pl) 2025-09-15

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