PL434616A1 - 7,4'-di-O-hexylnaringenin oxime and method of its preparation - Google Patents

7,4'-di-O-hexylnaringenin oxime and method of its preparation

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Publication number
PL434616A1
PL434616A1 PL434616A PL43461620A PL434616A1 PL 434616 A1 PL434616 A1 PL 434616A1 PL 434616 A PL434616 A PL 434616A PL 43461620 A PL43461620 A PL 43461620A PL 434616 A1 PL434616 A1 PL 434616A1
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PL
Poland
Prior art keywords
hexylnaringenin
oxime
preparation
formula
application
Prior art date
Application number
PL434616A
Other languages
Polish (pl)
Other versions
PL240960B1 (en
Inventor
Joanna Kozłowska
Original Assignee
Uniwersytet Przyrodniczy we Wrocławiu
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Uniwersytet Przyrodniczy we Wrocławiu filed Critical Uniwersytet Przyrodniczy we Wrocławiu
Priority to PL434616A priority Critical patent/PL240960B1/en
Publication of PL434616A1 publication Critical patent/PL434616A1/en
Publication of PL240960B1 publication Critical patent/PL240960B1/en

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  • Coloring (AREA)
  • Non-Silver Salt Photosensitive Materials And Non-Silver Salt Photography (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

Przedmiotem zgłoszenia jest związek o nazwie: Oksym 7,4'-di-O-heksylonaringeniny o wzorze 2 przedstawiony na rysunku. Zgłoszenie obejmuje także sposób otrzymywania oksymu 7,4'-di-O-heksylonaringeniny charakteryzujący się tym, że do substratu, którym jest 7,4'-di-O-heksylonaringenina o wzorze 1 dodaje się chlorowodorek hydroksyloaminy oraz bezwodny octan sodu w stosunku molowym co najmniej 1:1,5:1,5 oraz minimalną ilość alkoholu, co stanowi mieszaninę reakcyjną, którą pozostawia się w temperaturze od 30°C do 55°C na okres od 1 do 48 godzin przy ciągłym mieszaniu, po czym mieszaninę wylewa się do wody z lodem, wytrącony osad sączy się pod zmniejszonym ciśnieniem, a następnie otrzymany surowy produkt oczyszcza się.The subject of the application is the compound named: 7,4'-di-O-hexylnaringenin oxime of formula 2 shown in the figure. The application also covers the preparation of 7,4'-di-O-hexylnaringenin oxime, characterized in that hydroxylamine hydrochloride and anhydrous sodium acetate are added to the substrate, which is 7,4'-di-O-hexylnaringenin of the formula 1, in a molar ratio. at least 1: 1.5: 1.5 and the minimum amount of alcohol, which is the reaction mixture, which is left at a temperature of 30 ° C to 55 ° C for 1 to 48 hours with continuous stirring, after which the mixture is poured to ice-water, the precipitate formed is filtered off under reduced pressure, and then the obtained crude product is purified.

PL434616A 2020-07-10 2020-07-10 7,4'-di-O-hexylnaringenin oxime and method of its preparation PL240960B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL434616A PL240960B1 (en) 2020-07-10 2020-07-10 7,4'-di-O-hexylnaringenin oxime and method of its preparation

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL434616A PL240960B1 (en) 2020-07-10 2020-07-10 7,4'-di-O-hexylnaringenin oxime and method of its preparation

Publications (2)

Publication Number Publication Date
PL434616A1 true PL434616A1 (en) 2022-01-17
PL240960B1 PL240960B1 (en) 2022-07-04

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Family Applications (1)

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PL434616A PL240960B1 (en) 2020-07-10 2020-07-10 7,4'-di-O-hexylnaringenin oxime and method of its preparation

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PL (1) PL240960B1 (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
PL443473A1 (en) * 2023-01-13 2024-07-15 Uniwersytet Przyrodniczy we Wrocławiu 7,4'-di-O-heptylnaringenin oxime and method of obtaining 7,4'-di-O-heptylnaringenin oxime
PL443475A1 (en) * 2023-01-13 2024-07-15 Uniwersytet Przyrodniczy we Wrocławiu 7,4'-di-O-octylnaringenin oxime and method of obtaining 7,4'-di-O-octylnaringenin oxime
PL443474A1 (en) * 2023-01-13 2024-07-15 Uniwersytet Przyrodniczy we Wrocławiu 7,4'-di-O-nonylnaringenin oxime and method of obtaining 7,4'-di-O-nonylnaringenin oxime

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
PL443473A1 (en) * 2023-01-13 2024-07-15 Uniwersytet Przyrodniczy we Wrocławiu 7,4'-di-O-heptylnaringenin oxime and method of obtaining 7,4'-di-O-heptylnaringenin oxime
PL443475A1 (en) * 2023-01-13 2024-07-15 Uniwersytet Przyrodniczy we Wrocławiu 7,4'-di-O-octylnaringenin oxime and method of obtaining 7,4'-di-O-octylnaringenin oxime
PL443474A1 (en) * 2023-01-13 2024-07-15 Uniwersytet Przyrodniczy we Wrocławiu 7,4'-di-O-nonylnaringenin oxime and method of obtaining 7,4'-di-O-nonylnaringenin oxime

Also Published As

Publication number Publication date
PL240960B1 (en) 2022-07-04

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