PL416745A1 - Method for densification of solutions and the device for densification - Google Patents
Method for densification of solutions and the device for densificationInfo
- Publication number
- PL416745A1 PL416745A1 PL416745A PL41674516A PL416745A1 PL 416745 A1 PL416745 A1 PL 416745A1 PL 416745 A PL416745 A PL 416745A PL 41674516 A PL41674516 A PL 41674516A PL 416745 A1 PL416745 A1 PL 416745A1
- Authority
- PL
- Poland
- Prior art keywords
- concentrated solution
- solution
- evaporative
- evaporation
- outlets
- Prior art date
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/0088—Cascade evaporators
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/22—Evaporating by bringing a thin layer of the liquid into contact with a heated surface
- B01D1/222—In rotating vessels; vessels with movable parts
- B01D1/223—In rotating vessels; vessels with movable parts containing a rotor
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/26—Multiple-effect evaporating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/06—Flash distillation
- B01D3/065—Multiple-effect flash distillation (more than two traps)
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/10—Vacuum distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
- B01D3/146—Multiple effect distillation
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
Przedmiotem wynalazku jest sposób uzyskania bardzo wysokiego stopnia wykorzystania pary zasilającej w procesie zagęszczania roztworów, w wyparkach, składających się z wielu stożkowych wirujących zespołów wyparnych i urządzenie do takiego zagęszczania. W sposobie zagęszczany roztwór rozprowadzany jest na sześć lub więcej stożkowych powierzchni odparowania, zespolonych kaskadowym oddawaniem ciepła, przy czym z wybranych stopni wyparnych koncentrat odbierany jest osobno i łączony z roztworem pierwotnym podawanym do urządzenia. Ponadto roztwór u nasady stożków odparowania wypływa prostopadle do promienia ich obrotu powodując wir w przestrzeni rozprowadzania. Urządzenie wyparne składa się z jednego lub kilku wirujących wielostopniowych zespołów wyparnych, o kształcie odwróconych ściętych stożków, obwodowo zamkniętych monolitycznymi ścianami (6), a przyosiowo krawędziami trwale zespojonych z cylindrami (7), o średnicy znacznie większej niż wał (15), posiadającymi otwory (8) zasilania zagęszczanym roztworem, każdej stożkowej powierzchni odparowania i osadzonych kształtkami (9) skrajnymi, szczelnie, na elemencie (16) nośnym wydrążonego wału (15), z bocznymi otworami, połączonego z jednej strony z głowicą zasilającą w zagęszczany roztwór, z drugiej z głowicą parową. W zamkniętej przestrzeni pomiędzy wałem (15) i cylindrami (7) osadzone są szczelnie z otworami (8) zasilania walce (22) zaworów. Ze ścian (6) wychodzą króćce wypływowe końcowo zagęszczonego roztworu, króćce wypływowe wstępnie zagęszczonego roztworu i króćce wypływowe skroplin. Ich skraje odpowiednio wchodzą w przestrzeń pionowych koryt przepływowych, z przelewami, zamocowanych do kolistych obrzeży elementów (16) nośnego i (19) górnego. Zbiorczo dla każdego ciągu króćców uzyskuje się efekt U-rurki. Przelewy w odśrodkowych dnach koryt posiadają otwory wypływowe wstępnie i końcowo zagęszczonego roztworu na odpowiednich wysokościach tak, że wstępnie zagęszczony roztwór wyłapywany jest przez cylinder (33), a końcowo zagęszczony roztwór wyrzucany jest na ścianę (49) obudowy bocznej komory oparów. Zastosowane rozwiązania dają możliwość konstruowania urządzeń o zwiększonej ilości stopni wyparnych z zachowaniem efektywności ekonomicznej, ponieważ wszystkie stopnie wyparne posiadają taki sam, bardzo wysoki współczynnik przenikania ciepła. Konstrukcje posiadają bardzo szerokie spektrum zastosowań ze względu na sekundowy czas zagęszczania i pokonanie ograniczeń, wynikających z wysokiej lepkości koncentratu.The subject of the invention is a method of obtaining a very high degree of use of feed steam in the concentration of solutions, in evaporators, consisting of many conical rotating evaporative assemblies and a device for such concentration. In the method, the concentrated solution is distributed to six or more conical evaporation surfaces, combined with cascade heat release, with the concentrate selected from the evaporative stages separately and combined with the original solution fed to the device. In addition, the solution at the base of the evaporation cones flows perpendicular to the radius of their rotation, causing a vortex in the distribution space. The evaporation device consists of one or several rotating multi-stage evaporative assemblies, in the shape of inverted truncated cones, circumferentially closed with monolithic walls (6), and axially joined edges permanently connected to cylinders (7), with a diameter much larger than the shaft (15), having holes (8) supplying the thickened solution, each conical evaporation surface and the molded (9) outermost, tightly, on the supporting element (16) of the hollow shaft (15), with lateral openings, connected on one side with the supply head to the concentrated solution, on the other with a steam head. In the closed space between the shaft (15) and the cylinders (7) they are sealed tightly with the holes (8) for supplying the rollers (22) to the valves. Outlets of the final thickened solution, outlets of the pre-concentrated solution and condensate outlets exit from the walls (6). Their edges respectively enter the space of vertical flow troughs, with overflows, attached to the circular edges of the (16) support and (19) upper elements. Collectively, a U-tube effect is obtained for each string of connections. Overflows in the centrifugal bottoms of the troughs have outlet holes of the pre-concentrated and finally concentrated solution at appropriate heights, such that the pre-concentrated solution is captured by the cylinder (33), and the finally concentrated solution is thrown onto the wall (49) of the side vapor chamber housing. The applied solutions make it possible to construct devices with an increased number of evaporative stages while maintaining economic efficiency, because all evaporative stages have the same, very high heat transfer coefficient. The constructions have a very wide spectrum of applications due to the second compaction time and overcoming the limitations resulting from the high viscosity of the concentrate.
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
PL416745A PL416745A1 (en) | 2016-04-04 | 2016-04-04 | Method for densification of solutions and the device for densification |
PCT/PL2017/000036 WO2017176134A2 (en) | 2016-04-04 | 2017-04-04 | Method for concentrating solutions and a device for concentrating |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
PL416745A PL416745A1 (en) | 2016-04-04 | 2016-04-04 | Method for densification of solutions and the device for densification |
Publications (1)
Publication Number | Publication Date |
---|---|
PL416745A1 true PL416745A1 (en) | 2017-10-09 |
Family
ID=59227797
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PL416745A PL416745A1 (en) | 2016-04-04 | 2016-04-04 | Method for densification of solutions and the device for densification |
Country Status (2)
Country | Link |
---|---|
PL (1) | PL416745A1 (en) |
WO (1) | WO2017176134A2 (en) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108423728A (en) * | 2018-03-21 | 2018-08-21 | 国电山东电力有限公司 | A kind of thermal wastewater concentration systems that air Natural Circulation water is in line and method |
CN116492707B (en) * | 2023-06-26 | 2023-08-29 | 山东兴达化工有限公司 | Evaporation crystallization integrated equipment |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA696789A (en) * | 1964-10-27 | Aktiebolaget Separator | Method and apparatus for evaporating liquids | |
FR2540739A1 (en) * | 1983-02-11 | 1984-08-17 | Elf France | DEVICE AND FACILITIES FOR THIN-FILM EVAPORATION DISTILLATION, ESPECIALLY FOR HYDROCARBONS, AND METHOD OF IMPLEMENTING SAID DEVICE |
US5395483A (en) * | 1992-07-31 | 1995-03-07 | Al-Hawaj; Osamah M. | Rotary apparatus for combined multi flashing and boiling liquids |
-
2016
- 2016-04-04 PL PL416745A patent/PL416745A1/en unknown
-
2017
- 2017-04-04 WO PCT/PL2017/000036 patent/WO2017176134A2/en active Application Filing
Also Published As
Publication number | Publication date |
---|---|
WO2017176134A3 (en) | 2017-12-07 |
WO2017176134A2 (en) | 2017-10-12 |
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