PL416571A1 - Method for oxidation of limonene - Google Patents
Method for oxidation of limoneneInfo
- Publication number
- PL416571A1 PL416571A1 PL416571A PL41657116A PL416571A1 PL 416571 A1 PL416571 A1 PL 416571A1 PL 416571 A PL416571 A PL 416571A PL 41657116 A PL41657116 A PL 41657116A PL 416571 A1 PL416571 A1 PL 416571A1
- Authority
- PL
- Poland
- Prior art keywords
- limonene
- oxidation
- methanol
- catalyst
- iron
- Prior art date
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
Abstract
Przedmiotem zgłoszenia jest sposób utleniania limonenu za pomocą 60% roztworu wodnego nadtlenku wodoru lub 6M roztworu wodoronadtlenku t-butylu w dekanie, w obecności katalizatora i metanolu jako rozpuszczalnika. Sposób ten charakteryzuje się tym, że jako katalizator stosuje się mezoporowate materiały węglowe impregnowane żelazem o zawartości żelaza od 0,1 do 10% masowych, zaś utlenianie prowadzi się w temperaturach 100 - 140°C, w czasie od 6 h do 24 h, przy czym w mieszanie reakcyjnej metanol stosuje się w stężeniu wynoszącym 63 - 69% wagowych.The subject of the application is a method of oxidizing limonene with a 60% aqueous solution of hydrogen peroxide or a 6M solution of t-butyl hydroperoxide in decane, in the presence of a catalyst and methanol as a solvent. This method is characterized by the fact that as a catalyst, mesoporous carbon materials impregnated with iron with an iron content of 0.1 to 10% by mass are used, while oxidation is carried out at temperatures of 100 - 140 ° C, during 6 to 24 hours, at methanol is used in the reaction mixture at a concentration of 63-69% by weight.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
PL416571A PL231515B1 (en) | 2016-03-22 | 2016-03-22 | Method for oxidation of limonene |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
PL416571A PL231515B1 (en) | 2016-03-22 | 2016-03-22 | Method for oxidation of limonene |
Publications (2)
Publication Number | Publication Date |
---|---|
PL416571A1 true PL416571A1 (en) | 2017-09-25 |
PL231515B1 PL231515B1 (en) | 2019-03-29 |
Family
ID=59897566
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PL416571A PL231515B1 (en) | 2016-03-22 | 2016-03-22 | Method for oxidation of limonene |
Country Status (1)
Country | Link |
---|---|
PL (1) | PL231515B1 (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
PL423547A1 (en) * | 2017-11-23 | 2019-06-03 | Zachodniopomorski Univ Technologiczny W Szczecinie | Method for oxidation of limonene |
-
2016
- 2016-03-22 PL PL416571A patent/PL231515B1/en unknown
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
PL423547A1 (en) * | 2017-11-23 | 2019-06-03 | Zachodniopomorski Univ Technologiczny W Szczecinie | Method for oxidation of limonene |
Also Published As
Publication number | Publication date |
---|---|
PL231515B1 (en) | 2019-03-29 |
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