PL3916B3 - Method of extending the catalytic action of mercury compounds. - Google Patents

Method of extending the catalytic action of mercury compounds. Download PDF

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Publication number
PL3916B3
PL3916B3 PL3916A PL391621A PL3916B3 PL 3916 B3 PL3916 B3 PL 3916B3 PL 3916 A PL3916 A PL 3916A PL 391621 A PL391621 A PL 391621A PL 3916 B3 PL3916 B3 PL 3916B3
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PL
Poland
Prior art keywords
extending
catalytic action
mercury compounds
mercury
current
Prior art date
Application number
PL3916A
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Polish (pl)
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Application filed filed Critical
Publication of PL3916B3 publication Critical patent/PL3916B3/en

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Najdluzszy czas trwania patentu do 9 sierpnia 1939 r.W patencie Nr 418 opisany byl sposób przeprowadzania w postac czynna zuzy¬ tych katalizatorów rteciowych, jakie znaj¬ duja np. zastosowanie przy osadzaniu sie acetylenu, zapomeca utleniania anodowego.Jednoczesnie podany byl juz sposób zasto¬ sowania rteci metalicznej jako katody/ Znaleziono dalej, ze przy zastosowaniu rteci metalicznej jako anody, czy tez kato¬ dy, mozna pracowac nietylko z pradem sta¬ lym, ale i ze zmiennym przez co* uwydat¬ niaja sie szczególne korzysci, wzglednie u- proszczenia. Postepuje sie albo w ten spo¬ sób, ze pozwala sie nagromadzac wodorowi w krazacym pradzie gazów, lub tez stosuje sie specjalne urzadzenia, np. kanaly odpro^ wadzajace gazy, przeprowadzone poprzez elektrody i siegajace az do elektrolitów, które umozliwiaja odprowadzenie wodoru, wzglednie oddzielenie od przestrzeni zawie¬ rajacej acetylen. Diafragma jest pr zytem zbyteczna.Przyklad. Do aparatu mieszajacego, na dnie którego znajduja sie dwa wglebienia, przystosowane do umieszczenia elektrod skladajacych sie w danym przypadku z rte¬ ci metalicznej, wprowadza sie 11 mniej wie¬ cej 10% kwasu siarkowego. Wtedy wytwa¬ rza sie dostateczna ilosc soli rteciowe j przez przepuszczenie pradu zmiennego i wpu-szcza sie do ogrzanego do 70°—80^ C ply¬ nu reakcyjnego, mieszajac nadmiar acety¬ lenu, który przeprowadza sie w znany spo¬ sób w obieg kolowy, przyczem odbiera sie od pradu gazów utworzony aldehyd octowy w znany sposób. Jednoczesnie przepuszcza sie prad elektryczny o mniej wiecej 1 A. Od czasu do czasu wydala sie wodór, jaki stopniowo nagromadza sie w krazacym pra¬ dzie gazów, i napelnia aparat czystym ace¬ tylenem. PLThe longest term of the patent until August 9, 1939. Patent No. 418 describes a method of carrying out in active form used mercury catalysts, which are used, for example, in the deposition of acetylene, and which prevent anodic oxidation. At the same time, the method of using mercury was already given. metal as a cathode. It was further found that when using metallic mercury as an anode or also a cathode, it is possible to work not only with a direct current, but also with a variable current, which gives particular advantages, or simplification. This is either done in such a way that the hydrogen is allowed to accumulate in the circulating gas current, or special devices are used, e.g. gas discharge channels that pass through the electrodes and extend to the electrolytes, which allow the hydrogen to be withdrawn or to separate from the acetylene space. The diaphragm is not needed. Example. Into the mixing apparatus, at the bottom of which there are two cavities adapted to receive the electrodes consisting, in the case of metallic mercury, of approximately 10% sulfuric acid. A sufficient amount of mercury salt is then produced by passing an alternating current and released into the heated to 70 ° -80 ° C reaction fluid, mixing the excess acetylene, which is circulated in a known manner. whereby the acetaldehyde formed is removed from the gas current in a known manner. At the same time, an electric current of about 1 A is passed through. From time to time, hydrogen is released, which gradually builds up in the circulating gas stream, and the apparatus is filled with pure acetylene. PL

Claims (1)

1. Zastrzezenie patentowe. Sposób przedluzania katalitycznego dzialania zwiazków rteciowych wedlug pa¬ tentu Nr 418, znamienny tern, ze przy uzy¬ ciu rteci metalicznej jako anody i jako ka¬ tody, stosuje sie prad zmienny zamiast sta¬ lego. Chemische Fabrik Griesheim-Elektron. Zastepca: Cz, Raczynski, rzecznik patentowy. Druk L Roguslawskieao, Warszawa. PL1. Patent claim. The method of extending the catalytic action of mercury compounds according to the patent No. 418, characterized by the fact that when using metallic mercury as an anode and as a cathode, an alternating current is used instead of a constant one. Chemische Fabrik Griesheim-Elektron. Deputy: Cz, Raczynski, patent attorney. Printing L Roguslawskieao, Warsaw. PL
PL3916A 1921-03-22 Method of extending the catalytic action of mercury compounds. PL3916B3 (en)

Publications (1)

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PL3916B3 true PL3916B3 (en) 1926-03-31

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