PL3101011T3 - Method for preparing lactames, comprising a photonitrosation step, followed by a beckmann rearrangement step - Google Patents

Method for preparing lactames, comprising a photonitrosation step, followed by a beckmann rearrangement step

Info

Publication number
PL3101011T3
PL3101011T3 PL16176645T PL16176645T PL3101011T3 PL 3101011 T3 PL3101011 T3 PL 3101011T3 PL 16176645 T PL16176645 T PL 16176645T PL 16176645 T PL16176645 T PL 16176645T PL 3101011 T3 PL3101011 T3 PL 3101011T3
Authority
PL
Poland
Prior art keywords
lactames
followed
preparing
photonitrosation
beckmann rearrangement
Prior art date
Application number
PL16176645T
Other languages
Polish (pl)
Inventor
Thierry Aubert
Original Assignee
Arkema France
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Arkema France filed Critical Arkema France
Publication of PL3101011T3 publication Critical patent/PL3101011T3/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/02—Preparation of lactams
    • C07D201/04—Preparation of lactams from or via oximes by Beckmann rearrangement
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/02—Preparation of lactams
    • C07D201/10—Preparation of lactams from cycloaliphatic compounds by simultaneous nitrosylation and rearrangement
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • C07C249/06—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by nitrosation of hydrocarbons or substituted hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D225/00—Heterocyclic compounds containing rings of more than seven members having one nitrogen atom as the only ring hetero atom
    • C07D225/02—Heterocyclic compounds containing rings of more than seven members having one nitrogen atom as the only ring hetero atom not condensed with other rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D227/00—Heterocyclic compounds containing rings having one nitrogen atom as the only ring hetero atom, according to more than one of groups C07D203/00 - C07D225/00
    • C07D227/02—Heterocyclic compounds containing rings having one nitrogen atom as the only ring hetero atom, according to more than one of groups C07D203/00 - C07D225/00 with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D227/06—Heterocyclic compounds containing rings having one nitrogen atom as the only ring hetero atom, according to more than one of groups C07D203/00 - C07D225/00 with only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D227/08—Oxygen atoms
    • C07D227/087—One doubly-bound oxygen atom in position 2, e.g. lactams
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/18—Systems containing only non-condensed rings with a ring being at least seven-membered
    • C07C2601/20—Systems containing only non-condensed rings with a ring being at least seven-membered the ring being twelve-membered

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Other In-Based Heterocyclic Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
PL16176645T 2008-05-26 2009-05-14 Method for preparing lactames, comprising a photonitrosation step, followed by a beckmann rearrangement step PL3101011T3 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR0853419A FR2931478B1 (en) 2008-05-26 2008-05-26 PRODUCT FOR PREPARING LACTAMS COMPRISING A PHOTONITROSATION STEP FOLLOWED BY A BECKMANN TRANSPOSITION STEP
EP09766032.8A EP2291357B1 (en) 2008-05-26 2009-05-14 Method for preparing lactames, comprising a photonitrosation step, followed by a beckmann transposition step
EP16176645.6A EP3101011B1 (en) 2008-05-26 2009-05-14 Method for preparing lactames, comprising a photonitrosation step, followed by a beckmann rearrangement step

Publications (1)

Publication Number Publication Date
PL3101011T3 true PL3101011T3 (en) 2018-09-28

Family

ID=40134955

Family Applications (2)

Application Number Title Priority Date Filing Date
PL09766032.8T PL2291357T3 (en) 2008-05-26 2009-05-14 Method for preparing lactames, comprising a photonitrosation step, followed by a beckmann transposition step
PL16176645T PL3101011T3 (en) 2008-05-26 2009-05-14 Method for preparing lactames, comprising a photonitrosation step, followed by a beckmann rearrangement step

Family Applications Before (1)

Application Number Title Priority Date Filing Date
PL09766032.8T PL2291357T3 (en) 2008-05-26 2009-05-14 Method for preparing lactames, comprising a photonitrosation step, followed by a beckmann transposition step

Country Status (7)

Country Link
US (2) US20110137027A1 (en)
EP (2) EP3101011B1 (en)
JP (5) JP6235769B2 (en)
CN (2) CN102046604B (en)
FR (1) FR2931478B1 (en)
PL (2) PL2291357T3 (en)
WO (1) WO2009153470A1 (en)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2931478B1 (en) * 2008-05-26 2012-08-03 Arkema France PRODUCT FOR PREPARING LACTAMS COMPRISING A PHOTONITROSATION STEP FOLLOWED BY A BECKMANN TRANSPOSITION STEP
JP5359063B2 (en) * 2008-06-30 2013-12-04 東レ株式会社 Method for producing cycloalkanone oxime
JP5359064B2 (en) * 2008-06-30 2013-12-04 東レ株式会社 Method for producing cycloalkanone oxime and photochemical reaction apparatus
JP5821623B2 (en) * 2010-12-28 2015-11-24 東レ株式会社 Method for producing cycloalkanone oxime and method for producing lactam
ES2526796T3 (en) 2012-06-26 2015-01-15 Toray Industries, Inc. Cycloalcanone oxime production method
US9932296B2 (en) 2012-06-27 2018-04-03 Toray Industries, Inc. Method of producing cycloalkanone oxime
CN107073433B (en) * 2014-10-09 2020-01-31 东丽株式会社 Photochemical reaction device and photochemical reaction method using same
CN107438594B (en) 2015-04-02 2020-11-06 安西娅芳香剂私人有限公司 Effective process for synthesizing cyclic amide
WO2017133995A1 (en) 2016-02-01 2017-08-10 Basf Se Method for producing c4-c15 lactams
CN108409646B (en) * 2018-01-19 2020-05-19 南京红太阳生物化学有限责任公司 Synthetic method of nicotinamide
FR3107612B1 (en) 2020-02-20 2022-03-04 Arkema France Lamp for photochemical reactor based on light-emitting diodes
CN115260073B (en) * 2022-08-31 2024-09-20 中国天辰工程有限公司 Method for preparing laurinlactam by using ammonium sulfate-free byproduct rearrangement process

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3553091A (en) * 1966-08-17 1971-01-05 Fumio Nishikawa Method of photonitrosation of cycloalkanes
US3652552A (en) * 1966-12-16 1972-03-28 Stamicarbon Preparation of lactams from cycloalkanes
FR2417501A1 (en) * 1978-02-17 1979-09-14 Ato Chimie PROCESS FOR PREPARING MILK BY ISOMERIZATION OF OXIMES IN A SULFURIC MEDIUM
BE893651A (en) * 1982-06-25 1982-12-27 Desaar Rene POROUS NOSE FOR STEEL BALLING
US6197999B1 (en) * 1997-07-02 2001-03-06 Atofina Photonitrosation of cyclododecane in chloroform in quasi-anhydrous medium
FR2784103B1 (en) * 1998-09-21 2000-12-08 Atochem Elf Sa PROCESS FOR PREPARING LAURYLLACTAM BY PHOTONITROSATION OF CYCLODODECANE AND TRANSPOSITION OF BECKMANN IN THE PRESENCE OF METHANESULPHONIC ACID
JP2000164931A (en) 1998-11-27 2000-06-16 Sumitomo Electric Ind Ltd White color light source
JP2001002636A (en) * 1999-06-15 2001-01-09 Toray Ind Inc Production of lactam
DE10016106A1 (en) * 2000-03-31 2001-10-04 Merck Patent Gmbh Beckmann rearrangement of organic oxime, e.g. aromatic ketoxime, involves reaction with a suitable rearrangement reagent in the liquid state or in solution in a micro-reactor
JP4397394B2 (en) * 2003-01-24 2010-01-13 ディジタル・オプティクス・インターナショナル・コーポレイション High density lighting system
RU2007104173A (en) 2004-08-04 2008-08-10 Мацусита Электрик Индастриал Ко., Лтд. (Jp) RADIO COMMUNICATION DEVICE, RADIO COMMUNICATION SYSTEM AND RADIO COMMUNICATION METHOD
DE102005003966A1 (en) * 2005-01-27 2006-08-10 Ehrfeld Mikrotechnik Bts Gmbh Apparatus for the continuous implementation of photochemical processes with low optical layer thicknesses, narrow residence time distribution and high throughputs
FR2887250B1 (en) * 2005-06-21 2009-10-02 Arkema Sa PROCESS FOR THE SYNTHESIS OF LAURYLLACTAM (L12) BY CATALYTIC REARRANGEMENT IN THE GASEOUS PHASE OF CYCLODODECANONE OXIME
JP5110779B2 (en) * 2005-07-21 2012-12-26 日東電工株式会社 Method and apparatus for producing photoreaction product sheets
EP3540794B1 (en) * 2006-03-10 2022-03-30 Nichia Corporation Light-emitting device
JP2009539227A (en) * 2006-05-31 2009-11-12 クリー エル イー ディー ライティング ソリューションズ インコーポレイテッド Lighting device and lighting method
JP5030222B2 (en) 2006-09-08 2012-09-19 国立大学法人東京工業大学 Photocatalytic microreactor
JP2009235365A (en) 2008-03-28 2009-10-15 Toyota Motor Corp Polylactic acid composite molding, manufacturing method for polylactic acid composite molding, and surface member for automobile interior material
FR2931478B1 (en) * 2008-05-26 2012-08-03 Arkema France PRODUCT FOR PREPARING LACTAMS COMPRISING A PHOTONITROSATION STEP FOLLOWED BY A BECKMANN TRANSPOSITION STEP
JP5359063B2 (en) * 2008-06-30 2013-12-04 東レ株式会社 Method for producing cycloalkanone oxime
JP5359064B2 (en) * 2008-06-30 2013-12-04 東レ株式会社 Method for producing cycloalkanone oxime and photochemical reaction apparatus

Also Published As

Publication number Publication date
EP3101011B1 (en) 2018-06-20
EP3101011A1 (en) 2016-12-07
US20110137027A1 (en) 2011-06-09
JP2019055999A (en) 2019-04-11
JP2011521004A (en) 2011-07-21
PL2291357T3 (en) 2016-12-30
EP2291357B1 (en) 2016-07-13
US20140246303A1 (en) 2014-09-04
FR2931478B1 (en) 2012-08-03
US9499481B2 (en) 2016-11-22
WO2009153470A1 (en) 2009-12-23
JP2017081987A (en) 2017-05-18
CN102046604B (en) 2015-02-25
CN102046604A (en) 2011-05-04
EP2291357A1 (en) 2011-03-09
CN103588706B (en) 2016-08-24
JP2015157871A (en) 2015-09-03
FR2931478A1 (en) 2009-11-27
JP2017132797A (en) 2017-08-03
JP6567332B2 (en) 2019-08-28
JP6235769B2 (en) 2017-11-22
CN103588706A (en) 2014-02-19

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