PL134938B1 - Lubricating casting powder for continuous casting of steel - Google Patents

Lubricating casting powder for continuous casting of steel Download PDF

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Publication number
PL134938B1
PL134938B1 PL23834982A PL23834982A PL134938B1 PL 134938 B1 PL134938 B1 PL 134938B1 PL 23834982 A PL23834982 A PL 23834982A PL 23834982 A PL23834982 A PL 23834982A PL 134938 B1 PL134938 B1 PL 134938B1
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PL
Poland
Prior art keywords
steel
casting
lubricating
powder
dust
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PL23834982A
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Polish (pl)
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PL238349A1 (en
Inventor
Ireneusz Szlenk
Jozef Magiera
Cecylia Ciemciok
Krystyna Gorzel
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Przed Dostaw Materialow Odlewn
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Priority to PL23834982A priority Critical patent/PL134938B1/en
Publication of PL238349A1 publication Critical patent/PL238349A1/en
Publication of PL134938B1 publication Critical patent/PL134938B1/en

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Description

Przedmiotem wynalazku jest zasypka smarujaca przeznaczona do smarowania krystalizatora w prooesie ciaglego odlewania stali* Znana zasypka smarujaca stosowana do tego celu stanowi sypka mieszanine zawierajaca wa- , gowo 10% wapniokrzemut 35% fluorytu, 10% kredy mielonej lub wapna palonego, 40% szkla mielo-* nego 1 5% metakrzemianu sodu* Zasypka ta wykazuje zbyt wysoka temperature topnienia oraz niestabilnosc skladu chemicznego ze wzgledu na duzy udzial wagowy odpadowego produktu jakim jest szklo mielone* Ponadto zawiera w stosunkowo duzych ilosciach fluoryt, rozkladajaoy sie podczas stosowania zasypki z wydzieleniem trujacego fluoru* Powyzszych wad nie wykazuje zasypka smarujaca wedlug wynalazku zawierajaca wagowo od 5 do 10% tlenku glinu, od 25, do 35% tlenku wapnia, od 25 do 35% krzemionki w postaol maozki kwarcowej, od 5 do 15% tlenków zelaza w postaol zmielonej zendry lub rudy hematytowej lub pylu magnetytowego, od 6 do 8% kriolitu, od 12 do 18% sody bezwodnej, od 2 do 10% wegla w postaci sadzy, lub pylu koksowego, lub weglowego, lub grafitu i do 2% srodka odpowietrza¬ jacego w postaci mocznika i jego pochodnych, zwiazków azowych, zwiazków N-nitrozowych lub Innych znany oh zwiazków gazotwórozyoh nalezacych do grupy poroforów organicznych* Przykladowy0sklad wagowy zasypki smarujaoej wedlug wynalazku przedstawiono ponizej w przykladzies Przyklad* Tlenek glinu - 7%, tlenek wapnia - 28%, maozka kwarcowa - 30%, zendra mielona - 8%, kriolit - 7%, soda bezwodna - 15%, grafit Eg - 4%, Poreks [dwunitrozopieoio- metylenoozteroamina] - 1%* Zasypke smarujaca wedlug wynalazku sporzadza sie przez staranne wymieszanie skladników w mieszarce przeznaczonej do mieszania materialów sypkich* Zasypke transportuje sie w workach polietylenowych chronia o ja przed zawilgoceniem* Zasypke smarujaca wedlug wynalazku, w ilosci 0,5 do 1 kg na tone stali, wprowadza sie porcjami lub w sposób ciagly na powierzchnie cieklej stali w krystalizatorze uzywanym w pro-2 134 938 ceeie ciaglego odlewania stali. W momencie zetkniecia aie zasypki z ciekla stala obecny w zasypce srodek gazotwórozy rozklada sie z wydzieleniem azotu lub innego gazu obojetnego, który usuwa powietrze z przestrzeni miedzyziarnowej zasypki, nie dopuszczajac do kontaktów cieklej stali z tlenem powietrza.Nastepnie pod wplywem wysokiej temperatury, zapala sie obeony w zasypce wegiel, który wydziela tlenek wegla tworzacy ochronna, redukoyjna warstwe gazowa nie dopuszczajaca do utleniania sie stali. Z chwila osiagniecia temperatury 1373 £ zasypka smarujaca wedlug wy¬ nalazku topi aie tworzao rzadkoplynne szkliwo ceramiczne stanowiace pod wzgledem ohemicz- nym glinokrzemian typu CaO .AlpOJSlOp* Glinokrzamian ten powstaje w wyniku reakoji zacno- dzaoej w wysokiej temperaturze pomiedzy zawartym w zasypce wapnem palonym, tlenkiem glinu i krzemionka w postaci maczki kwarcowej* Kriolit i soda bezwodna stanowia topniki obnizajace temperature topnienia zasypki sma¬ rujacej wedlug wynalazku* Natomiast tlenki zelaza dzialaja uplynniajaoo, przeciwdzialaja niebezpieczenstwu naweglania stali weglem obeonym w zasypce, co noze miec miejsce podczas jej stosowania w oiaglym odlewaniu stali niskoweglowyoh i nierdzewnyoh* Powstale niskolep- kie szkliwo glinokrzemianowe splywa z powierzohni oieklej stali w przestrzen pomiedzy krzep¬ nacy wlewek a wewnetrzna powierzchnie krystalizatora, spelniajac role smaru zapewniajacego wlasciwy i prawidlowy przebieg procesu ciaglego odlewania stali* Ciekla warstwa smaru, z uwagi na niska zawartosc tlenku glinu wykazuje silna tendencje do absorpcji i uplynniania z oieklej stali niemetalicznych zanieozyszozen, jak na przyklad ozastki szamoty pochodzace z erozji wymurówki, ukladu technologicznego ciaglego odlewania stali* Zasypka smarujaca wedlug wynalazku przeoiwdziala utlenianiu sie stali, wypromieniowaniu ciepla z górnej powierzohni stali w krystalizatorze oraz skutecznie przeciwdziala tworzeniu sie typowych wad powierzchniowych w postaol nakluc i porowatosci w przypowierzchniowej war¬ stwie odlewanego wlewka* Zasypka smarujaca wedlug wynalazku jest bezpieczna w stosowaniu, gdyz zawiera topnik fluorkowy, kriolit w stosunkowo niewielkiej ilosci* W poblizu stanowiska pracy, jak wykazaly przeprowadzone badania, ilosc fluoru wydzielanego z zasypki jest kilka¬ krotnie nizsza od wartosci dopuszczonej norma* Zastrzezenie patentowe Zasypka smarujaca do ciaglego odlewania stali, znamienna tym, ze zawiera wagowo od 5 do 10% tlenku glinu, od 25 do 39% tlenku wapnia, od 25 do 30% krzemionki w po- staoi maozki kwarcowej, od 5 do 15% tlenków zelaza w postaci zmielonej zendry, lub rudy he- matyoznej, lub pylu magnetytowego, od 6 do 9 kriolitu, od 12 do 18% sody bezwodnej, od 2 do 10% wegla w postaoi sadzy, lub pylu koksowego, lub pylu weglowego, lub grafitu i do 2% srodka odpowietrzajacego * postaol mocznika i jego pochodnych, lub zwiazków azowych, lub zwiazków N-nitrozowyoh, lub innyoh znanych zwiazków gazo twórczy oh nalezaoych do grupy poro* forów organicznych* Pracownia Poligraficzna UP PRL. Naklad 100 egz.Cena 100 zl. PLThe subject of the invention is a lubricating powder intended to lubricate the crystallizer in the process of continuous casting of steel * The known lubricating powder used for this purpose is a free-flowing mixture containing by weight 10% calcium silicate, 35% fluorspar, 10% ground chalk or quicklime, 40% ground glass. * of 1 5% sodium metasilicate * This backfill has an excessively high melting point and instability of the chemical composition due to the large proportion by weight of the waste product which is ground glass * In addition, it contains relatively large amounts of fluorite, decomposing when using the backfill with the release of poisonous fluorine * The above-mentioned disadvantages do not show the lubricating powder according to the invention, containing by weight from 5 to 10% of alumina, from 25 to 35% of calcium oxide, from 25 to 35% of silica in the form of quartz moss, from 5 to 15% of iron oxides in the form of ground scale or hematite ore or magnetite dust, from 6 to 8% cryolite, from 12 to 18% anhydrous soda, from 2 to 10% carbon in residues of soot, coke or coal dust, or graphite, and up to 2% of a deaerator in the form of urea and its derivatives, azo compounds, N-nitroso compounds or other known gas-forming compounds belonging to the group of organic blowing agents * Example weight composition of grease backfill according to the invention, the following examples are presented: Example * Aluminum oxide - 7%, calcium oxide - 28%, quartz stone - 30%, ground scale - 8%, cryolite - 7%, anhydrous soda - 15%, graphite Eg - 4%, Porex [dinitrozeo-methylene etheramine] - 1% * The lubricating powder according to the invention is prepared by careful mixing of the ingredients in a mixer designed for mixing loose materials * The powder is transported in polyethylene bags to protect against moisture * Lubricating powder according to the invention, in the amount of 0.5 to the invention 1 kg per ton of steel, is introduced batchwise or continuously onto the surface of the liquid steel in the crystallizer used in the pro-2 134 938 continuous casting and steel. At the moment of contact of the backfill with the liquid solid, the gasoline agent present in the backfill decomposes with the release of nitrogen or other inert gas, which removes air from the intergranular space of the backfill, preventing the liquid steel from contacting the air oxygen. Then, under the influence of high temperature, the envelope ignites in the powder there is carbon which releases carbon monoxide, which creates a protective, reducing gas layer, preventing steel oxidation. Upon reaching the temperature of 1373 ° C, the lubricating powder, according to the invention, melts and forms a liquid ceramic glaze, which is chemically an aluminosilicate of the CaO type. AlpOJSlOp * This aluminosilicate is formed as a result of a fiery reaction in a high temperature burnt lime contained between aluminum and silica in the form of quartz flour * Cryolite and anhydrous soda are fluxes lowering the melting point of the lubricating powder according to the invention * On the other hand, iron oxides act to liquefy, counteract the danger of carbon contamination of the steel with carbon in the powder, which should be used when casting steel Low-carbon and stainless steel * The resulting low-viscosity aluminosilicate glaze flows down from the surface of the molten steel into the space between the solidifying ingot and the inner surface of the crystallizer, fulfilling the role of a lubricant ensuring the proper and correct course of the continuous casting process of grease, due to the low content of alumina, it shows a strong tendency to absorb and liquefy non-metallic debris from the liquid steel, such as, for example, chamotte chips resulting from the erosion of lining, technological system of continuous steel casting * Lubricating powder, according to the invention, resists oxidation of steel, the upper surface of the steel in the crystallizer and effectively counteracts the formation of typical surface defects in the form of pincers and porosity in the subsurface layer of the cast ingot * The lubricating powder according to the invention is safe to use, because it contains fluoride flux, cryolite in a relatively small amount * Near the workplace As the tests carried out have shown, the amount of fluoride released from the powder is several times lower than the value allowed by the standard * Patent claim Lubricating powder for continuous casting of steel, characterized by the fact that it contains from 5 to 10% of aluminum oxide by weight, from 25 to 39% calcium oxide, 25 to 30% of silica in the form of quartz sand, 5 to 15% of iron oxides in the form of ground scale, or hematose ore, or magnetite dust, 6 to 9 cryolite, 12 to 18% soda anhydrous, from 2 to 10% carbon in the form of soot or coke dust, or coal dust, or graphite and up to 2% deaerating agent * urea and its derivatives or azo compounds or N-nitroso compounds or other known gas compounds creative oh belonging to the group of organic poros * Pracownia Poligraficzna UP PRL. Mintage 100 copies Price PLN 100. PL

Claims (1)

1. Zastrzezenie patentowe Zasypka smarujaca do ciaglego odlewania stali, znamienna tym, ze zawiera wagowo od 5 do 10% tlenku glinu, od 25 do 39% tlenku wapnia, od 25 do 30% krzemionki w po- staoi maozki kwarcowej, od 5 do 15% tlenków zelaza w postaci zmielonej zendry, lub rudy he- matyoznej, lub pylu magnetytowego, od 6 do 9 kriolitu, od 12 do 18% sody bezwodnej, od 2 do 10% wegla w postaoi sadzy, lub pylu koksowego, lub pylu weglowego, lub grafitu i do 2% srodka odpowietrzajacego * postaol mocznika i jego pochodnych, lub zwiazków azowych, lub zwiazków N-nitrozowyoh, lub innyoh znanych zwiazków gazo twórczy oh nalezaoych do grupy poro* forów organicznych* Pracownia Poligraficzna UP PRL. Naklad 100 egz. Cena 100 zl. PL1. Patent claim Lubricating powder for continuous casting of steel, characterized in that it contains from 5 to 10% by weight of alumina, from 25 to 39% of calcium oxide, from 25 to 30% of silica in the form of silica, from 5 to 15 % of iron oxides in the form of ground scale, or hematose ore, or magnetite dust, 6 to 9 cryolite, 12 to 18% anhydrous soda, 2 to 10% carbon black, coke dust or coal dust, or graphite and up to 2% deaerating agent * urea and its derivatives, or azo compounds or N-nitroso compounds, or other known gas-forming compounds belonging to the group of organic blowing agents * Pracownia Poligraficzna UP PRL. Mintage 100 copies. Price PLN 100. PL
PL23834982A 1982-09-24 1982-09-24 Lubricating casting powder for continuous casting of steel PL134938B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL23834982A PL134938B1 (en) 1982-09-24 1982-09-24 Lubricating casting powder for continuous casting of steel

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL23834982A PL134938B1 (en) 1982-09-24 1982-09-24 Lubricating casting powder for continuous casting of steel

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PL238349A1 PL238349A1 (en) 1984-03-26
PL134938B1 true PL134938B1 (en) 1985-09-30

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