PE20231381A1 - PROCESS FOR THE PREPARATION OF ANTHRANILAMIDES - Google Patents

PROCESS FOR THE PREPARATION OF ANTHRANILAMIDES

Info

Publication number
PE20231381A1
PE20231381A1 PE2022002880A PE2022002880A PE20231381A1 PE 20231381 A1 PE20231381 A1 PE 20231381A1 PE 2022002880 A PE2022002880 A PE 2022002880A PE 2022002880 A PE2022002880 A PE 2022002880A PE 20231381 A1 PE20231381 A1 PE 20231381A1
Authority
PE
Peru
Prior art keywords
anthranilamides
carried out
preparation
reaction
arthropocidal
Prior art date
Application number
PE2022002880A
Other languages
Spanish (es)
Inventor
Gal Suez
Hagit Forckosh
Yanai Golub
Jie Lie
Bob Chen
Regev Parnes
Original Assignee
Adama Makhteshim Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Adama Makhteshim Ltd filed Critical Adama Makhteshim Ltd
Publication of PE20231381A1 publication Critical patent/PE20231381A1/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D401/00Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom
    • C07D401/02Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings
    • C07D401/04Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings directly linked by a ring-member-to-ring-member bond
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/48Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
    • A01N43/561,2-Diazoles; Hydrogenated 1,2-diazoles
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01PBIOCIDAL, PEST REPELLANT, PEST ATTRACTANT OR PLANT GROWTH REGULATORY ACTIVITY OF CHEMICAL COMPOUNDS OR PREPARATIONS
    • A01P7/00Arthropodicides
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07BGENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00Indexing scheme relating to specific properties of organic compounds
    • C07B2200/13Crystalline forms, e.g. polymorphs

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Wood Science & Technology (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental Sciences (AREA)
  • Zoology (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • General Health & Medical Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Health & Medical Sciences (AREA)
  • Dentistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Insects & Arthropods (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Saccharide Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Pyrrole Compounds (AREA)

Abstract

El objeto de la presente invencion consiste en proporcionar un proceso novedoso y ventajoso para la preparacion comercial de antranilamidas artropocidas de formula (Ia) y (Ib) mediante reaccion de cloruro de acilo y las correspondientes amidas de acido antranilico, en donde el proceso se lleva a cabo en ausencia de depurador de acido y el acido clorhidrico formado se destila de la mezcla de la reaccion durante el proceso.The object of the present invention is to provide a novel and advantageous process for the commercial preparation of arthropocidal anthranilamides of formula (Ia) and (Ib) by reaction of acyl chloride and the corresponding anthranilic acid amides, where the process is carried out carried out in the absence of acid scrubber and the hydrochloric acid formed is distilled from the reaction mixture during the process.

PE2022002880A 2020-06-08 2021-06-08 PROCESS FOR THE PREPARATION OF ANTHRANILAMIDES PE20231381A1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US202063035865P 2020-06-08 2020-06-08
PCT/CN2021/098904 WO2021249396A1 (en) 2020-06-08 2021-06-08 The process of preparation of anthranilamides

Publications (1)

Publication Number Publication Date
PE20231381A1 true PE20231381A1 (en) 2023-09-07

Family

ID=78845357

Family Applications (2)

Application Number Title Priority Date Filing Date
PE2022002884A PE20231426A1 (en) 2020-06-08 2021-06-08 SOLID STATE FORMS OF CYANTRANILIPROL
PE2022002880A PE20231381A1 (en) 2020-06-08 2021-06-08 PROCESS FOR THE PREPARATION OF ANTHRANILAMIDES

Family Applications Before (1)

Application Number Title Priority Date Filing Date
PE2022002884A PE20231426A1 (en) 2020-06-08 2021-06-08 SOLID STATE FORMS OF CYANTRANILIPROL

Country Status (12)

Country Link
US (2) US20230348414A1 (en)
EP (2) EP4165031A4 (en)
CN (2) CN116490492A (en)
AR (2) AR122563A1 (en)
AU (2) AU2021286610A1 (en)
BR (2) BR112022025068A2 (en)
CA (2) CA3181797A1 (en)
CO (2) CO2023000040A2 (en)
IL (2) IL298908A (en)
MX (2) MX2022015596A (en)
PE (2) PE20231426A1 (en)
WO (2) WO2021249395A1 (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113896714A (en) * 2021-11-23 2022-01-07 江西汇和化工有限公司 Method for synthesizing chlorantraniliprole
WO2024176261A1 (en) * 2023-02-21 2024-08-29 Upl Limited A process for preparation of anthranilamide compound and intermediate thereof

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2264022B1 (en) * 2003-01-28 2013-07-24 E. I. du Pont de Nemours and Company Cyano anthranilamide insecticides
MY140912A (en) * 2004-07-26 2010-01-29 Du Pont Mixtures of anthranilamide invertebrate pest control agents
TWI363756B (en) * 2004-12-07 2012-05-11 Du Pont Method for preparing n-phenylpyrazole-1-carboxamides
TWI395728B (en) * 2006-12-06 2013-05-11 Du Pont Process for preparing 2-amino-5-cyanobenzoic acid derivatives
US8212075B2 (en) * 2007-11-08 2012-07-03 E.I. Du Pont De Nemours And Company Process for preparing 2-amino-5-cyanobenzoic acid derivatives
CN101550130B (en) * 2008-04-01 2012-11-07 中国中化股份有限公司 Method for preparing 3-halo-1-(3-chloro -2-pyridyl)-1H-pyrazole-5-formyl halide
RS53150B (en) * 2008-11-14 2014-06-30 E. I. Du Pont De Nemours And Company Method for preparing a non-hydratable crystal form
CN102020633B (en) * 2009-09-21 2013-08-07 中国中化股份有限公司 Method for preparing 1-(3,5- dichloropyridine-2-yl)-pyrazolecarboxamide compounds
CN110028489B (en) * 2018-01-12 2021-08-06 沈阳中化农药化工研发有限公司 Method for preparing benzamide compound by pressure reduction method
WO2019207595A1 (en) * 2018-04-23 2019-10-31 Natco Pharma Limited An improved process for the preparation of anthranilamide derivatives
CN112552284B (en) * 2020-12-18 2022-08-12 重庆华歌生物化学有限公司 Preparation method of chlorantraniliprole

Also Published As

Publication number Publication date
AR122564A1 (en) 2022-09-21
PE20231426A1 (en) 2023-09-13
MX2022015597A (en) 2023-02-01
IL298905A (en) 2023-02-01
CN116490492A (en) 2023-07-25
WO2021249395A1 (en) 2021-12-16
CO2023000040A2 (en) 2023-03-27
AU2021287782A1 (en) 2023-02-02
EP4165030A1 (en) 2023-04-19
US20230348414A1 (en) 2023-11-02
EP4165030A4 (en) 2024-07-31
CA3181797A1 (en) 2021-12-16
EP4165031A1 (en) 2023-04-19
CO2023000039A2 (en) 2023-03-27
CN116490491A (en) 2023-07-25
AR122563A1 (en) 2022-09-21
MX2022015596A (en) 2023-02-01
BR112022025066A2 (en) 2023-03-07
EP4165031A4 (en) 2024-09-25
WO2021249396A1 (en) 2021-12-16
US20230312505A1 (en) 2023-10-05
IL298908A (en) 2023-02-01
AU2021286610A1 (en) 2023-01-19
CA3181785A1 (en) 2021-12-16
BR112022025068A2 (en) 2023-03-07

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