PE20231381A1 - PROCESS FOR THE PREPARATION OF ANTHRANILAMIDES - Google Patents
PROCESS FOR THE PREPARATION OF ANTHRANILAMIDESInfo
- Publication number
- PE20231381A1 PE20231381A1 PE2022002880A PE2022002880A PE20231381A1 PE 20231381 A1 PE20231381 A1 PE 20231381A1 PE 2022002880 A PE2022002880 A PE 2022002880A PE 2022002880 A PE2022002880 A PE 2022002880A PE 20231381 A1 PE20231381 A1 PE 20231381A1
- Authority
- PE
- Peru
- Prior art keywords
- anthranilamides
- carried out
- preparation
- reaction
- arthropocidal
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 4
- PXBFMLJZNCDSMP-UHFFFAOYSA-N 2-Aminobenzamide Chemical class NC(=O)C1=CC=CC=C1N PXBFMLJZNCDSMP-UHFFFAOYSA-N 0.000 abstract 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 1
- 150000001263 acyl chlorides Chemical class 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D401/00—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom
- C07D401/02—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings
- C07D401/04—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings directly linked by a ring-member-to-ring-member bond
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
- A01N43/56—1,2-Diazoles; Hydrogenated 1,2-diazoles
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01P—BIOCIDAL, PEST REPELLANT, PEST ATTRACTANT OR PLANT GROWTH REGULATORY ACTIVITY OF CHEMICAL COMPOUNDS OR PREPARATIONS
- A01P7/00—Arthropodicides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B2200/00—Indexing scheme relating to specific properties of organic compounds
- C07B2200/13—Crystalline forms, e.g. polymorphs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Wood Science & Technology (AREA)
- Engineering & Computer Science (AREA)
- Environmental Sciences (AREA)
- Zoology (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- General Health & Medical Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Health & Medical Sciences (AREA)
- Dentistry (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Insects & Arthropods (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Plural Heterocyclic Compounds (AREA)
- Saccharide Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Pyrrole Compounds (AREA)
Abstract
El objeto de la presente invencion consiste en proporcionar un proceso novedoso y ventajoso para la preparacion comercial de antranilamidas artropocidas de formula (Ia) y (Ib) mediante reaccion de cloruro de acilo y las correspondientes amidas de acido antranilico, en donde el proceso se lleva a cabo en ausencia de depurador de acido y el acido clorhidrico formado se destila de la mezcla de la reaccion durante el proceso.The object of the present invention is to provide a novel and advantageous process for the commercial preparation of arthropocidal anthranilamides of formula (Ia) and (Ib) by reaction of acyl chloride and the corresponding anthranilic acid amides, where the process is carried out carried out in the absence of acid scrubber and the hydrochloric acid formed is distilled from the reaction mixture during the process.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US202063035865P | 2020-06-08 | 2020-06-08 | |
PCT/CN2021/098904 WO2021249396A1 (en) | 2020-06-08 | 2021-06-08 | The process of preparation of anthranilamides |
Publications (1)
Publication Number | Publication Date |
---|---|
PE20231381A1 true PE20231381A1 (en) | 2023-09-07 |
Family
ID=78845357
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PE2022002884A PE20231426A1 (en) | 2020-06-08 | 2021-06-08 | SOLID STATE FORMS OF CYANTRANILIPROL |
PE2022002880A PE20231381A1 (en) | 2020-06-08 | 2021-06-08 | PROCESS FOR THE PREPARATION OF ANTHRANILAMIDES |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PE2022002884A PE20231426A1 (en) | 2020-06-08 | 2021-06-08 | SOLID STATE FORMS OF CYANTRANILIPROL |
Country Status (12)
Country | Link |
---|---|
US (2) | US20230348414A1 (en) |
EP (2) | EP4165031A4 (en) |
CN (2) | CN116490492A (en) |
AR (2) | AR122563A1 (en) |
AU (2) | AU2021286610A1 (en) |
BR (2) | BR112022025068A2 (en) |
CA (2) | CA3181797A1 (en) |
CO (2) | CO2023000040A2 (en) |
IL (2) | IL298908A (en) |
MX (2) | MX2022015596A (en) |
PE (2) | PE20231426A1 (en) |
WO (2) | WO2021249395A1 (en) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113896714A (en) * | 2021-11-23 | 2022-01-07 | 江西汇和化工有限公司 | Method for synthesizing chlorantraniliprole |
WO2024176261A1 (en) * | 2023-02-21 | 2024-08-29 | Upl Limited | A process for preparation of anthranilamide compound and intermediate thereof |
Family Cites Families (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2264022B1 (en) * | 2003-01-28 | 2013-07-24 | E. I. du Pont de Nemours and Company | Cyano anthranilamide insecticides |
MY140912A (en) * | 2004-07-26 | 2010-01-29 | Du Pont | Mixtures of anthranilamide invertebrate pest control agents |
TWI363756B (en) * | 2004-12-07 | 2012-05-11 | Du Pont | Method for preparing n-phenylpyrazole-1-carboxamides |
TWI395728B (en) * | 2006-12-06 | 2013-05-11 | Du Pont | Process for preparing 2-amino-5-cyanobenzoic acid derivatives |
US8212075B2 (en) * | 2007-11-08 | 2012-07-03 | E.I. Du Pont De Nemours And Company | Process for preparing 2-amino-5-cyanobenzoic acid derivatives |
CN101550130B (en) * | 2008-04-01 | 2012-11-07 | 中国中化股份有限公司 | Method for preparing 3-halo-1-(3-chloro -2-pyridyl)-1H-pyrazole-5-formyl halide |
RS53150B (en) * | 2008-11-14 | 2014-06-30 | E. I. Du Pont De Nemours And Company | Method for preparing a non-hydratable crystal form |
CN102020633B (en) * | 2009-09-21 | 2013-08-07 | 中国中化股份有限公司 | Method for preparing 1-(3,5- dichloropyridine-2-yl)-pyrazolecarboxamide compounds |
CN110028489B (en) * | 2018-01-12 | 2021-08-06 | 沈阳中化农药化工研发有限公司 | Method for preparing benzamide compound by pressure reduction method |
WO2019207595A1 (en) * | 2018-04-23 | 2019-10-31 | Natco Pharma Limited | An improved process for the preparation of anthranilamide derivatives |
CN112552284B (en) * | 2020-12-18 | 2022-08-12 | 重庆华歌生物化学有限公司 | Preparation method of chlorantraniliprole |
-
2021
- 2021-06-08 US US18/009,072 patent/US20230348414A1/en active Pending
- 2021-06-08 CN CN202180058429.4A patent/CN116490492A/en active Pending
- 2021-06-08 MX MX2022015596A patent/MX2022015596A/en unknown
- 2021-06-08 EP EP21821439.3A patent/EP4165031A4/en active Pending
- 2021-06-08 AR ARP210101554A patent/AR122563A1/en unknown
- 2021-06-08 IL IL298908A patent/IL298908A/en unknown
- 2021-06-08 US US18/009,066 patent/US20230312505A1/en active Pending
- 2021-06-08 AU AU2021286610A patent/AU2021286610A1/en active Pending
- 2021-06-08 CN CN202180058527.8A patent/CN116490491A/en active Pending
- 2021-06-08 CA CA3181797A patent/CA3181797A1/en active Pending
- 2021-06-08 MX MX2022015597A patent/MX2022015597A/en unknown
- 2021-06-08 WO PCT/CN2021/098903 patent/WO2021249395A1/en active Application Filing
- 2021-06-08 AR ARP210101555A patent/AR122564A1/en unknown
- 2021-06-08 BR BR112022025068A patent/BR112022025068A2/en unknown
- 2021-06-08 EP EP21820820.5A patent/EP4165030A4/en active Pending
- 2021-06-08 WO PCT/CN2021/098904 patent/WO2021249396A1/en active Application Filing
- 2021-06-08 AU AU2021287782A patent/AU2021287782A1/en active Pending
- 2021-06-08 PE PE2022002884A patent/PE20231426A1/en unknown
- 2021-06-08 BR BR112022025066A patent/BR112022025066A2/en unknown
- 2021-06-08 PE PE2022002880A patent/PE20231381A1/en unknown
- 2021-06-08 IL IL298905A patent/IL298905A/en unknown
- 2021-06-08 CA CA3181785A patent/CA3181785A1/en active Pending
-
2023
- 2023-01-03 CO CONC2023/0000040A patent/CO2023000040A2/en unknown
- 2023-01-03 CO CONC2023/0000039A patent/CO2023000039A2/en unknown
Also Published As
Publication number | Publication date |
---|---|
AR122564A1 (en) | 2022-09-21 |
PE20231426A1 (en) | 2023-09-13 |
MX2022015597A (en) | 2023-02-01 |
IL298905A (en) | 2023-02-01 |
CN116490492A (en) | 2023-07-25 |
WO2021249395A1 (en) | 2021-12-16 |
CO2023000040A2 (en) | 2023-03-27 |
AU2021287782A1 (en) | 2023-02-02 |
EP4165030A1 (en) | 2023-04-19 |
US20230348414A1 (en) | 2023-11-02 |
EP4165030A4 (en) | 2024-07-31 |
CA3181797A1 (en) | 2021-12-16 |
EP4165031A1 (en) | 2023-04-19 |
CO2023000039A2 (en) | 2023-03-27 |
CN116490491A (en) | 2023-07-25 |
AR122563A1 (en) | 2022-09-21 |
MX2022015596A (en) | 2023-02-01 |
BR112022025066A2 (en) | 2023-03-07 |
EP4165031A4 (en) | 2024-09-25 |
WO2021249396A1 (en) | 2021-12-16 |
US20230312505A1 (en) | 2023-10-05 |
IL298908A (en) | 2023-02-01 |
AU2021286610A1 (en) | 2023-01-19 |
CA3181785A1 (en) | 2021-12-16 |
BR112022025068A2 (en) | 2023-03-07 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CO2023000040A2 (en) | Process for the preparation of anthranilamides | |
EA201591093A1 (en) | METHODS OF SYNTHESIS ANALOGUE OF PROSTACYCLINE | |
US9187407B2 (en) | Method to produce N-acyl amino acid surfactants using N-acyl amino acid surfactants or the corresponding anhydrides as catalysts | |
AR092278A1 (en) | PROCESS FOR OBTAINING N-ACILIC DERIVATIVES OF BIFENYL-ALANINE AND RELATED INTERMEDIARIES | |
MX2009002121A (en) | A process for the manufacture of snac (salcaprozate sodium). | |
AR083840A1 (en) | PROCESSES FOR THE PREPARATION OF N- [2- (7-METOXI-1-NAFTIL) ETIL] ACETAMIDE | |
AR077526A1 (en) | METHOD FOR THE SYNTHESIS OF (1S, 2R) - MILNACIPRAN | |
PE20140188A1 (en) | CO-CRYSTALS AND SALTS OF CCR3 INHIBITORS | |
MA35886B1 (en) | Benzylsulfanilamide derivatives used as -2 mogat inhibitors | |
PL416028A1 (en) | Method for production of high purity monochloroacetic acid | |
MX2018000196A (en) | Process for the preparation of a furfural derivative. | |
MX2020006837A (en) | Method for producing thiocarboxamidine salt compound. | |
MX2022006048A (en) | A continuous flow process for the synthesis of hydroxamic acid. | |
CY1112714T1 (en) | PROCEDURE FOR THE PRODUCTION OF HIGH-CLEANANCE OF MELOXICAM AND POTASSIUM SILVER | |
CN105061209A (en) | Synthetic method of 2-diester methylmalonate compounds | |
FR2976940B1 (en) | PROCESS FOR PREPARING ALPHA- AND BETA-AMINOPHOSPHORUS ACID AND DERIVATIVES THEREOF | |
RU2014111398A (en) | SUBSTITUTED DIPEPTIDES WITH NEUROPSYCHOTROPIC ACTIVITY | |
AR093245A1 (en) | PROCESSES FOR THE PREPARATION OF AGOMELATIN USING INTERMEDIARIES | |
AR059417A1 (en) | REPLACED QUINOLONES III, A METHOD FOR THEIR PREPARATION AND USE IN THE MANUFACTURE OF A MEDICINAL PRODUCT FOR THE TREATMENT OR PROFILAXIS OF AN INFECTION WITH THE HUMAN CITOMEGALOVIRUS (HCMV). | |
EP2814808B1 (en) | Process for preparing chloroamines | |
RU2015108347A (en) | METHOD AND INTERMEDIATE COMPOUNDS FOR THE PRODUCTION OF DAZATINIB | |
JP2008214225A (en) | Method for producing 5,5-disubstituted-3-pyrrolin-2-one derivative | |
JP5900993B2 (en) | New acid chloride | |
JP2016199489A (en) | Method for producing 2-amino-6-methylnicotinic acid ester | |
BR102012001156A2 (en) | process for the production of alkyl phosphates |