PE20090270A1 - PROCESS AND APPARATUS FOR MIXING GASES - Google Patents

PROCESS AND APPARATUS FOR MIXING GASES

Info

Publication number
PE20090270A1
PE20090270A1 PE2008000998A PE2008000998A PE20090270A1 PE 20090270 A1 PE20090270 A1 PE 20090270A1 PE 2008000998 A PE2008000998 A PE 2008000998A PE 2008000998 A PE2008000998 A PE 2008000998A PE 20090270 A1 PE20090270 A1 PE 20090270A1
Authority
PE
Peru
Prior art keywords
converter
gas
gas flow
heat exchanger
gases
Prior art date
Application number
PE2008000998A
Other languages
Spanish (es)
Inventor
Karl-Heinz Daum
Wolfram Schalk
Ventosa David Cachero
Original Assignee
Outotec Oyj
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Outotec Oyj filed Critical Outotec Oyj
Publication of PE20090270A1 publication Critical patent/PE20090270A1/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00Sulfur; Compounds thereof
    • C01B17/69Sulfur trioxide; Sulfuric acid
    • C01B17/74Preparation
    • C01B17/76Preparation by contact processes
    • C01B17/80Apparatus
    • C01B17/803Converters
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/10Mixing gases with gases
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/30Injector mixers
    • B01F25/31Injector mixers in conduits or tubes through which the main component flows
    • B01F25/313Injector mixers in conduits or tubes through which the main component flows wherein additional components are introduced in the centre of the conduit
    • B01F25/3132Injector mixers in conduits or tubes through which the main component flows wherein additional components are introduced in the centre of the conduit by using two or more injector devices
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0446Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
    • B01J8/0461Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical annular shaped beds
    • B01J8/0469Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical annular shaped beds the beds being superimposed one above the other
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0492Feeding reactive fluids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0496Heating or cooling the reactor
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00Sulfur; Compounds thereof
    • C01B17/69Sulfur trioxide; Sulfuric acid
    • C01B17/74Preparation
    • C01B17/76Preparation by contact processes
    • C01B17/765Multi-stage SO3-conversion
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00017Controlling the temperature
    • B01J2208/00106Controlling the temperature by indirect heat exchange
    • B01J2208/00168Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00194Tubes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)

Abstract

SE REFIERE A UN PROCESO PARA MEZCLAR DOS GASES DE DIFERENTES TEMPERATURAS Y/O COMPOSICIONES EN UN CONVERTIDOR PARA PRODUCIR SO3 A PARTIR DE UN GAS QUE TIENE SO2, CARACTERIZADO PORQUE: A) UN PRIMER FLUJO DE GAS QUE CONTIENE SO2 ES INTRODUCIDO EN EL CONVERTIDOR A TRAVES DE UNA TUBERIA DE SUMINISTRO CENTRAL Y PASADO A TRAVES DE UN INTERCAMBIADOR DE CALOR INTEGRADO, DICHO PRIMER FLUJO DE GAS CONTIENE MAS DE UN 13% EN VOLUMEN DE SO2; B) EL SEGUNDO FLUJO DE GAS ES SUMISTRADO VIA UN CONDUCTO DE ANILLO COLOCADO EN EL CONVERTIDOR DIRECTAMENTE ANTES O DESPUES DEL INTERCAMBIADOR DE CALOR INTEGRADO, DESDE EL CUAL EL SEGUNDO FLUJO DE GAS ES DESCARGADO A TRAVES DE UNA PLURALIDAD DE ABERTURAS Y ES ALIMENTADO DENTRO DEL PRIMER FLUJO DE GAS, DE TAL FORMA QUE SE MEZCLE CON EL MISMO, EL MENCIONADO SEGUNDO FLUJO DE GAS CONTIENE DE UN 5 A UN 25% EN VOLUMEN DE SO3; Y C) LA MEZCLA DE GAS OBTENIDA ES LUEGO SUMINISTRADA A UNA ETAPA DE CONTACTO DEL CONVERTIDOR, EN LA CUAL EL SO2 ES AL MENOS PARCIALMENTE CONVERTIDO A SO3 SOBRE UN CATALIZADOR. SE REFIERE ADEMAS, A UN APARATO PARA MEZCLAR DOS GASES EN UN CONVERTIDOR PARA PRODUCIR SO3 QUE COMPRENDE: i) UN CONDUCTO DE SUMINISTRO PARA UN PRIMER GAS, ii) UN CONVERTIDOR, iii) UN INTERCAMBIADOR DE CALOR, Y iv) UNA CAMARA DE MEZCLADOREFERS TO A PROCESS TO MIX TWO GASES OF DIFFERENT TEMPERATURES AND / OR COMPOSITIONS IN A CONVERTER TO PRODUCE SO3 FROM A GAS THAT HAS SO2, CHARACTERIZED BECAUSE: A) A FIRST FLOW OF GAS CONTAINING SO2 IN THE CONVERTER IS INTRODUCED THROUGH A CENTRAL SUPPLY PIPE AND PASSED THROUGH AN INTEGRATED HEAT EXCHANGER, SAID FIRST GAS FLOW CONTAINS MORE THAN 13% BY VOLUME OF SO2; B) THE SECOND GAS FLOW IS SUPPLIED VIA A RING DUCT PLACED IN THE CONVERTER DIRECTLY BEFORE OR AFTER THE INTEGRATED HEAT EXCHANGER, FROM WHICH THE SECOND GAS FLOW IS DISCHARGED THROUGH A PLURALITY OF THE OPENING AND IS INTO THE OPENING. FIRST GAS FLOW, IN SUCH A WAY THAT IT IS MIXED WITH IT, THE MENTIONED SECOND GAS FLOW CONTAINS FROM 5 TO 25% BY VOLUME OF SO3; AND C) THE GAS MIXTURE OBTAINED IS THEN SUPPLIED TO A CONTACT STAGE OF THE CONVERTER, IN WHICH SO2 IS AT LEAST PARTIALLY CONVERTED TO SO3 OVER A CATALYST. IT ALSO REFERS TO AN APPARATUS FOR MIXING TWO GASES IN A CONVERTER TO PRODUCE SO3, INCLUDING: i) A SUPPLY PIPE FOR A FIRST GAS, ii) A CONVERTER, iii) A HEAT EXCHANGER, AND iv) A MIXING CHAMBER

PE2008000998A 2007-06-13 2008-06-11 PROCESS AND APPARATUS FOR MIXING GASES PE20090270A1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE102007027881A DE102007027881B4 (en) 2007-06-13 2007-06-13 Method and apparatus for mixing gases

Publications (1)

Publication Number Publication Date
PE20090270A1 true PE20090270A1 (en) 2009-03-19

Family

ID=39827729

Family Applications (1)

Application Number Title Priority Date Filing Date
PE2008000998A PE20090270A1 (en) 2007-06-13 2008-06-11 PROCESS AND APPARATUS FOR MIXING GASES

Country Status (7)

Country Link
CN (1) CN101679037B (en)
AU (1) AU2008261290B2 (en)
CL (1) CL2008001718A1 (en)
DE (1) DE102007027881B4 (en)
MX (1) MX340510B (en)
PE (1) PE20090270A1 (en)
WO (1) WO2008151758A2 (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102745654A (en) * 2012-07-31 2012-10-24 阳谷祥光铜业有限公司 Conversion device for acid-making with smoke, system and method for heating conversion device for acid-making with smoke
CN108046221B (en) * 2017-12-12 2020-10-02 中国恩菲工程技术有限公司 Method for preparing acid by smelting flue gas

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2104858A (en) * 1935-01-23 1938-01-11 Gen Chemical Corp Manufacture of sulphuric acid
NL205521A (en) * 1951-10-10
DE1151341B (en) * 1961-03-21 1963-07-11 Schmidt Sche Heissdampf Installation of additional firing systems for introducing and mixing the fresh heating gas into exhaust gas ducts through which low-temperature exhaust gases flow
DE1926239U (en) * 1964-01-31 1965-11-04 Uhde Gmbh Friedrich DEVICE FOR MIXING GASES OF DIFFERENT DENSITY.
US3661165A (en) * 1970-07-21 1972-05-09 Nat Distillers Chem Corp System for mixing gases and sparger valve for accomplishing same
DE7242602U (en) * 1972-11-20 1976-04-29 Hoogovens Ijmuiden B.V., Ijmuiden (Niederlande)
US4152407A (en) * 1977-02-02 1979-05-01 Warren Fuchs Process and apparatus for exothermic reactions
CA1159229A (en) * 1980-09-19 1983-12-27 John Mcfarland Converter
US5480620A (en) * 1994-08-17 1996-01-02 Cameron; Gordon M. Catalytic converter
DE19800800C2 (en) 1998-01-13 2001-05-23 Metallgesellschaft Ag Process for the production of sulfuric acid
DE10023178A1 (en) 2000-05-11 2001-11-15 Mg Technologies Ag Two-stage catalytic production of sulfur trioxide gas with low sulfur dioxide content from high sulfur dioxide-content gas comprises use of two catalyst layers with temperature at each layer controlled
DE10249782A1 (en) 2002-10-24 2004-05-06 Outokumpu Oyj Process and plant for the production of sulfuric acid from sulfur dioxide-rich gases
DE10359744A1 (en) * 2003-12-19 2005-07-14 Uhde Gmbh Method and device for injecting oxygen into a synthesis reactor

Also Published As

Publication number Publication date
DE102007027881A1 (en) 2008-12-18
AU2008261290B2 (en) 2013-07-04
MX340510B (en) 2016-07-11
WO2008151758A3 (en) 2009-06-11
DE102007027881B4 (en) 2012-02-16
AU2008261290A1 (en) 2008-12-18
WO2008151758A2 (en) 2008-12-18
CN101679037B (en) 2015-03-04
CL2008001718A1 (en) 2008-08-01
CN101679037A (en) 2010-03-24
MX2009013478A (en) 2010-01-18

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