NO166609B - DEVICE FOR TESTING THE FUNCTIONALITY OF AN EMERGENCY LIGHTING DEVICE. - Google Patents
DEVICE FOR TESTING THE FUNCTIONALITY OF AN EMERGENCY LIGHTING DEVICE. Download PDFInfo
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- NO166609B NO166609B NO852842A NO852842A NO166609B NO 166609 B NO166609 B NO 166609B NO 852842 A NO852842 A NO 852842A NO 852842 A NO852842 A NO 852842A NO 166609 B NO166609 B NO 166609B
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- circuit
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- power supply
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- soil
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- NVBFHJWHLNUMCV-UHFFFAOYSA-N sulfamide Chemical class NS(N)(=O)=O NVBFHJWHLNUMCV-UHFFFAOYSA-N 0.000 claims description 9
- -1 dichlorofluoromethylmercapto Chemical class 0.000 claims description 4
- 230000002464 fungitoxic effect Effects 0.000 claims description 4
- 125000003342 alkenyl group Chemical group 0.000 claims description 3
- 125000000217 alkyl group Chemical group 0.000 claims description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 2
- 229910052739 hydrogen Inorganic materials 0.000 claims description 2
- 239000001257 hydrogen Substances 0.000 claims description 2
- 238000004088 simulation Methods 0.000 abstract 1
- 230000001960 triggered effect Effects 0.000 abstract 1
- 239000013543 active substance Substances 0.000 description 30
- 241000196324 Embryophyta Species 0.000 description 18
- 239000002689 soil Substances 0.000 description 18
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 12
- 238000002360 preparation method Methods 0.000 description 11
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 9
- 241000233866 Fungi Species 0.000 description 5
- 244000223014 Syzygium aromaticum Species 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- KDRSHFSCTSFYGH-UHFFFAOYSA-N [dichloro(fluoro)methyl] thiohypochlorite Chemical compound FC(Cl)(Cl)SCl KDRSHFSCTSFYGH-UHFFFAOYSA-N 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 3
- 235000016639 Syzygium aromaticum Nutrition 0.000 description 3
- 241000209140 Triticum Species 0.000 description 3
- 235000021307 Triticum Nutrition 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 239000011230 binding agent Substances 0.000 description 3
- 230000000855 fungicidal effect Effects 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 239000000454 talc Substances 0.000 description 3
- 229910052623 talc Inorganic materials 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- 241000223218 Fusarium Species 0.000 description 2
- 241000222831 Phialophora <Chaetothyriales> Species 0.000 description 2
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 2
- 239000006004 Quartz sand Substances 0.000 description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
- 241000722093 Tilletia caries Species 0.000 description 2
- 125000004432 carbon atom Chemical group C* 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 239000002361 compost Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000005520 cutting process Methods 0.000 description 2
- 201000010099 disease Diseases 0.000 description 2
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 2
- 230000002538 fungal effect Effects 0.000 description 2
- 239000000417 fungicide Substances 0.000 description 2
- 230000035784 germination Effects 0.000 description 2
- 238000011081 inoculation Methods 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 238000005554 pickling Methods 0.000 description 2
- 238000009331 sowing Methods 0.000 description 2
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 description 1
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 description 1
- 206010017533 Fungal infection Diseases 0.000 description 1
- 239000005909 Kieselgur Substances 0.000 description 1
- 208000031888 Mycoses Diseases 0.000 description 1
- 241000308483 Phialophora cinerescens Species 0.000 description 1
- 241000233639 Pythium Species 0.000 description 1
- 241001361634 Rhizoctonia Species 0.000 description 1
- 241000865903 Thielaviopsis Species 0.000 description 1
- 241000082085 Verticillium <Phyllachorales> Species 0.000 description 1
- 240000008042 Zea mays Species 0.000 description 1
- 235000016383 Zea mays subsp huehuetenangensis Nutrition 0.000 description 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 1
- QMHAHUAQAJVBIW-UHFFFAOYSA-N [methyl(sulfamoyl)amino]methane Chemical compound CN(C)S(N)(=O)=O QMHAHUAQAJVBIW-UHFFFAOYSA-N 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910001854 alkali hydroxide Inorganic materials 0.000 description 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 description 1
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid group Chemical group C(C1=CC=CC=C1)(=O)O WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 208000024386 fungal infectious disease Diseases 0.000 description 1
- 231100000162 fungitoxic Toxicity 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 150000007529 inorganic bases Chemical class 0.000 description 1
- 235000009973 maize Nutrition 0.000 description 1
- 239000002362 mulch Substances 0.000 description 1
- RSLUZFWSJKMVME-UHFFFAOYSA-N n-(methylsulfamoyl)butan-1-amine Chemical compound CCCCNS(=O)(=O)NC RSLUZFWSJKMVME-UHFFFAOYSA-N 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000006072 paste Substances 0.000 description 1
- 229920000151 polyglycol Polymers 0.000 description 1
- 239000010695 polyglycol Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 150000003141 primary amines Chemical class 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- YBBRCQOCSYXUOC-UHFFFAOYSA-N sulfuryl dichloride Chemical compound ClS(Cl)(=O)=O YBBRCQOCSYXUOC-UHFFFAOYSA-N 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 150000003512 tertiary amines Chemical class 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- ILWRPSCZWQJDMK-UHFFFAOYSA-N triethylazanium;chloride Chemical compound Cl.CCN(CC)CC ILWRPSCZWQJDMK-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
- G01R19/00—Arrangements for measuring currents or voltages or for indicating presence or sign thereof
- G01R19/165—Indicating that current or voltage is either above or below a predetermined value or within or outside a predetermined range of values
- G01R19/16533—Indicating that current or voltage is either above or below a predetermined value or within or outside a predetermined range of values characterised by the application
- G01R19/16538—Indicating that current or voltage is either above or below a predetermined value or within or outside a predetermined range of values characterised by the application in AC or DC supplies
- G01R19/16542—Indicating that current or voltage is either above or below a predetermined value or within or outside a predetermined range of values characterised by the application in AC or DC supplies for batteries
-
- H—ELECTRICITY
- H02—GENERATION; CONVERSION OR DISTRIBUTION OF ELECTRIC POWER
- H02J—CIRCUIT ARRANGEMENTS OR SYSTEMS FOR SUPPLYING OR DISTRIBUTING ELECTRIC POWER; SYSTEMS FOR STORING ELECTRIC ENERGY
- H02J9/00—Circuit arrangements for emergency or stand-by power supply, e.g. for emergency lighting
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- Power Engineering (AREA)
- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Business, Economics & Management (AREA)
- Emergency Management (AREA)
- Circuit Arrangement For Electric Light Sources In General (AREA)
- Stand-By Power Supply Arrangements (AREA)
- Indicating And Signalling Devices For Elevators (AREA)
- Circuit Arrangements For Discharge Lamps (AREA)
- Selective Calling Equipment (AREA)
- Waste-Gas Treatment And Other Accessory Devices For Furnaces (AREA)
- Investigating Strength Of Materials By Application Of Mechanical Stress (AREA)
- Eye Examination Apparatus (AREA)
Abstract
Description
Sulfamidderivater med fungitoksisk virkning. Sulfamide derivatives with fungitoxic effect.
Det er allerede kjent at man som fungiside virksomme stoffer kan anvende forbindelser som inneholder en triklormerkapto-gruppe eller en diklorfluormetylmerkaptogruppe. Noen av disse virksomme stoffer har i' praksis fått en meget stor betydning (sammenlign tysk patent nr. 921.290 og tysk utlegningsskrift 1.193.498)'It is already known that compounds containing a trichloromercapto group or a dichlorofluoromethylmercapto group can be used as fungicide active substances. Some of these active substances have in practice become very important (compare German patent no. 921,290 and German explanatory document 1,193,498)'
Det er nå funnet at de nye sulfamidderivater med den generelle formel It has now been found that the new sulfamide derivatives with the general formula
hvori in which
R og R' betyr alkyl eller alkenyl og R and R' mean alkyl or alkenyl and
Z betyr hydrogen eller diklorfluorraetylmerkapto, Z means hydrogen or dichlorofluoroethyl mercapto,
har sterke fungitoksiske egenskaper. has strong fungitoxic properties.
Sulfamidderivatene med formel (I) får man når.man omsetter disubstituerte sulfamider med formel The sulfamide derivatives of formula (I) are obtained when disubstituted sulfamides of formula are reacted
hvori in which
R og R' har den ovenfor angitte betydning i molforhold på ca. 1 1 eller ca. 1 : 2 med fluordiklormetansulfenylklorid i nærvær av et syrebindende middel. R and R' have the meaning stated above in a molar ratio of approx. 1 1 or approx. 1:2 with fluorodichloromethanesulfenyl chloride in the presence of an acid-binding agent.
Det må anses som meget overraskende at de virksomme stoffer ifølge oppfinnelsen har en bedre fungisidvirkning enn de fra teknikkens stand kjente kjemisk tilsvarende oppbyggede fungisider. It must be regarded as very surprising that the active substances according to the invention have a better fungicidal effect than the chemically similarly constructed fungicides known from the state of the art.
De virksomme stoffer ifølge oppfinnelsen medfører derfor en berikelse av teknikken. The active substances according to the invention therefore lead to an enrichment of the technique.
Reaksjonsforløpet av fremgangsmåten kan gjengis ved føl-gende formelskjerna, idet dimetylsulfamid er anvendt som utgangsstoff. The course of the reaction of the method can be reproduced by the following formula core, dimethylsulfamide being used as starting material.
Utgangsforbindelsen er prinsippielt kjent. De ennå ikke kjente sulfamider fremstilles på samme måte som de allerede kjente sulfamider, nemlig ved omsetning av de tilsvarende primære aminer med sulfurylklorid. The output connection is known in principle. The not yet known sulfamides are prepared in the same way as the already known sulfamides, namely by reacting the corresponding primary amines with sulfuryl chloride.
Sulfamidene er entydig karakterisert med formel II. I denne formel betyr R og R' fortrinnsvis alkyl med 1 - '4 C-atomer såvel som alkenyl med 3 ~ 4 C-atomer, altså allyl. The sulfamides are uniquely characterized by formula II. In this formula, R and R' preferably mean alkyl with 1-4 C atoms as well as alkenyl with 3-4 C atoms, i.e. allyl.
Omsetningen kan foretas i nærvær av inert, organisk opp-løsningsmiddel. Hertil hører f.eks. hydrokarboner som benzol, eter som dietyleter og dioksan. Det kan imidlertid også arbeides i nærvær av vann. The reaction can be carried out in the presence of an inert, organic solvent. This includes e.g. hydrocarbons such as benzene, ethers such as diethyl ether and dioxane. However, it can also be worked in the presence of water.
Som syrebindemiddel kan det anvendes de vanlige syre-bindere, altså tertiære aminer som trietylamin og pyridin, såvel som også uorganiske baser som alkalikarbonater og alkalihydroksyder. The usual acid binders can be used as acid binders, i.e. tertiary amines such as triethylamine and pyridine, as well as inorganic bases such as alkali carbonates and alkali hydroxides.
Reaksjonstemperaturene kan varieres i et større område. The reaction temperatures can be varied over a larger range.
Vanligvis arbeider man mellom 0 og 80°C, fortrinnsvis mellom 20 og 50°C. Usually one works between 0 and 80°C, preferably between 20 and 50°C.
Ved gjennomføringen av fremgangsmåten anvender man alt etter det ønskede sluttprodukt enten 1 eller 2.mol fluordiklormetansulfenylklorid på 1 mol sulfamid. Mest hensiktsmessig arbeider man i nærvær av et fortynningsmiddel. Reaksjonsproduktets opparbeidelse foregår på vanlig måte. When carrying out the method, depending on the desired end product, either 1 or 2 mol of fluorodichloromethanesulfenyl chloride is used on 1 mol of sulfamide. It is most appropriate to work in the presence of a diluent. The preparation of the reaction product takes place in the usual way.
De virksomme stoffer ifølge oppfinnelsen har en høy fungitoksisk virkningsgrad og en stor virkningsbredde og har en relativt liten varmblodsgiftighet, hvorved de er enkle å håndtere og kan i praksis anvendes til bekjempelse av uønsket soppvekst. Deres gode plantetålbarhet muliggjør også en anvendelse mot soppaktive plantesyk-dommer ved behandling av de .stående kulturplanter eller enkelte deler av dem eller frøgods eller også kulturjorden. De virksomme stoffer er spesielt virksomme mot tracheomycose-frembringende sopp som angriper plantene fra jorden, som Verticillium-arter, Fusarium-arter og Phialophora-arter. De virker imidlertid likeledes også meget godt mot frøoverførbar sopp som Tilletia tritici og mot jordboende'sopp som Rhizoctonia-art.er, Fusarium-arter, Pythium-arter og Thielaviopsis-arter. The active substances according to the invention have a high degree of fungitoxic effectiveness and a large range of action and have a relatively low warm-blood toxicity, whereby they are easy to handle and can be used in practice to combat unwanted fungal growth. Their good plant tolerance also makes it possible to use them against fungal active plant diseases when treating the standing cultivated plants or certain parts of them or seed material or also the cultivated soil. The active substances are particularly effective against tracheomycosis-producing fungi which attack the plants from the soil, such as Verticillium species, Fusarium species and Phialophora species. However, they also work very well against seed-borne fungi such as Tilletia tritici and against soil-dwelling fungi such as Rhizoctonia species, Fusarium species, Pythium species and Thielaviopsis species.
De virksomme stoffer ifølge oppfinnelsen kan overføres i de vanlige formuleringer som oppløsninger, emulsjoner, suspensjoner, pulvere, pastaer og granulater. The active substances according to the invention can be transferred in the usual formulations such as solutions, emulsions, suspensions, powders, pastes and granules.
Jordbehandlingsmiddelprøve/jordfødte mykoser. Soil treatment product test/soil-born mycoses.
Til fremstilling av en hensiktsmessig virksom stofftilberedning drøyer man det virksomme stoff med talkum til 5 % °g deretter med kvartssand til 0,5 % virksomt stoffinnhold. To prepare a suitable active substance preparation, the active substance is diluted with talc to 5% °g, then with quartz sand to 0.5% active substance content.
Den virksomme stofftilberedning sammenblander man jevnt med Fruhstorfer enhets jord som først steriliseres og deretter er blitt podet med renkulturer av prøvesoppen. Jorden fylles i potter og besåes med 5 x 10 frø av vertsplanten. Pottene oppstilles ved de angitte temperaturer i veksthus og holdes normalt fuktige. 3 uker etter såing bestemmer man antall sunne planter i prosent av utlagte frø. 0 % betyr at det ikke er vokset opp sunne planter, 100 % betyr at det fra alle frø er dannet sunne planter. The active substance preparation is evenly mixed with Fruhstorfer's unit soil, which is first sterilized and then inoculated with pure cultures of the test fungus. The soil is filled in pots and sown with 5 x 10 seeds of the host plant. The pots are set up at the specified temperatures in the greenhouse and kept normally moist. 3 weeks after sowing, the number of healthy plants is determined as a percentage of sown seeds. 0% means that no healthy plants have grown, 100% means that healthy plants have been formed from all seeds.
Virksomt stoff, virksom stoffkonsentrasjon i jorden, prøvesopp, vertsplante, veksthustemperaturer såvel som resultater fremgår av følgende tabell: Active substance, active substance concentration in the soil, test fungus, host plant, greenhouse temperatures as well as results appear in the following table:
Jordbehandlingsmiddel-prøve / pytium ultiraura Soil treatment agent sample / pytium ultiraura
For fremstilling av en hensiktsmessig virksom stofftilberedning drøyer man det virksomme stoff med talkum til 5 % °g deretter med kvartssand til 0,5 % virksomt stoffinnhold. To prepare a suitable active substance preparation, the active substance is diluted with talc to 5% °g, then with quartz sand to 0.5% active substance content.
Den virksomme stofftilberedning sammenblander man jevnt med naturlig infisert kompostjord som ved innsåing av jordert erfa-ringsmessig fører til stort utfall under kimplantene ved hjelp av pytium ultimum. Jorden fylles i potter og såes med 5 x 10 frø av markert. Pottene oppstilles ved 15 - l8°C i veksthus og holdes normalt fuktige. 3 uker etter utsåing bestemmer man antallet av sunne planter i prosent av utlagte frø. 0 % betyr at det ikke er vokst opp sunne planter, 100 % betyr at av alle frø er det dannet sunne planter. The effective substance preparation is evenly mixed with naturally infected compost soil, which, when seeded with soil, leads to a large yield under the seedlings with the help of pytium ultimum. The soil is filled in pots and sown with 5 x 10 seeds of marked. The pots are placed at 15 - 18°C in a greenhouse and kept normally moist. 3 weeks after sowing, the number of healthy plants is determined as a percentage of sown seeds. 0% means that no healthy plants have grown, 100% means that healthy plants have been formed from all seeds.
Virksomme stoffer, virksomme stoffkonsentrasjoner i Active substances, active substance concentrations in
jorden og resultatene fremgår av følgende tabell: the soil and the results appear in the following table:
Frøgodsbeisemiddel-prøve / hvetesott (frøbåren mykose). Seed treatment sample / wheat blight (seed-borne mycosis).
For fremstilling av et hensiktsmessig tørrbeisemiddel drøyer man det virksomme stoff med en blanding av like vektsdeler talkum og kiselger til en finpulverisert blanding med den ønskede virksomme stoffkonsentrasjon. To produce a suitable dry mordant, the active substance is ground with a mixture of equal parts by weight of talc and diatomaceous earth to a finely powdered mixture with the desired active substance concentration.
Man kontaminerer hvetefrøgods med 5 g chlamydosporer av tilletia tritici pr. kg frøgods. For beising ryster man frøgodset med beisemidlet i en lukket glassflaske. Frøgodset utsettes på fuktig leire under et dekksjikt av et lag mull og 2 cm passelig fuktig kompostjord i 10 dager i et kjøleskap ved 10°C optimale kimingsbetin-gelser for sporene. Wheat seed material is contaminated with 5 g of chlamydospores of tilletia tritici per kg seed material. For pickling, the seeds are shaken with the pickling agent in a closed glass bottle. The seed material is placed on moist clay under a covering layer of a layer of mulch and 2 cm of suitably moist compost soil for 10 days in a refrigerator at 10°C, optimal germination conditions for the spores.
Deretter bestemmer man mikroskopisk sporenes kiming på hvetekornene som hver er angrepet med omtrent 100.000 sporer. Det virksomme stoffet er desto mer virksomt jo færre sporer som er kimet. The germination of the spores is then determined microscopically on the wheat grains, each of which is attacked with approximately 100,000 spores. The active substance is all the more effective the fewer spores that have germinated.
Virksomt stoff, virksom stoffkonsentrasjon i beisemiddel, beisemiddelanvendt mengde og kimprosent av sporer fremgår av følgende tabell: Active substance, active substance concentration in mordant, amount of mordant used and germ percentage of spores can be seen in the following table:
Visne-prøver / nelliker. Withered samples / cloves.
I den nedenfor omtalte prøve ble de virksomme stoffer (a), (b), (c) og (d) undersøkt på deres fungiside virkning mot phialophora. In the test described below, the active substances (a), (b), (c) and (d) were examined for their fungicidal activity against phialophora.
Ved prøvene ble godt rotdannede nellikstiklinger plantet At the tests, well-rooted clove cuttings were planted
i jorden, hvortil det var satt en med phialophora cinerescens bevokst maismel-sandblanding. Denne inokulasjon førte ved ikke-behandlede planter etter tre uker til de første sykdomssymptomer og etter 5-6 uker til total visning og utdøing av plantene. in the soil, to which a maize meal-sand mixture grown with phialophora cinerescens had been added. This inoculation led to untreated plants after three weeks to the first disease symptoms and after 5-6 weeks to total wilting and dying of the plants.
En del av jorden ble før plantningen-med nellikstiklinger behandlet med tilberedninger av de nevnte virksomme stoffer. Disse virksomme stofftilberedninger ble fremstilt ved oppløsning av en bestemt mengde av det virksomme stoff i en blanding av 9 vektsdeler aceton og 1 vektsdel nonylfenol-polyglykolfeter og fortynning av dette konsentrat med vann. 250 ml av-denne tilberedning ble helt hver gang på 1000 ml jord. Tilberedningen inneholdt så meget virksomt stoff at det i jorden forelå en virksom stoffkonsentrasjon på 100 mg virksomt stoff pr. 1 liter jord. Planter som ble dyrket på således behandlet jord viste ingen eller bare meget lite angrep. Part of the soil was treated with preparations of the aforementioned active substances before planting with clove cuttings. These active substance preparations were prepared by dissolving a specific amount of the active substance in a mixture of 9 parts by weight of acetone and 1 part by weight of nonylphenol-polyglycol fat and diluting this concentrate with water. 250 ml of this preparation was poured each time onto 1000 ml of soil. The preparation contained so much active substance that there was a concentration of active substance in the soil of 100 mg of active substance per 1 liter of soil. Plants grown on soil thus treated showed no or only very little attack.
Ved en sammenligning av lengde og vekst av nellikplantene som hverken var infisert eller behandlet med preparater med slike nellikplanter, som såvel var inokulert som også behandlet med de nevnte preparater ved sprøyting, viste det seg at de behandlede planter i de fleste tilfeller såvel hadde en tilsvarende eller sogar høyere gjennomsnittlig lengde og en tilsvarende eller sogar høyere gjennomsnittlig vekt. Plantebestanden var altså ved inokulasjon nøyaktig så god som ved de ubehandlede ikke-infiserte kontrollplanter. In a comparison of the length and growth of the clove plants that were neither infected nor treated with preparations with such clove plants, which were both inoculated and also treated with the aforementioned preparations by spraying, it turned out that the treated plants in most cases also had a corresponding or even higher average length and a corresponding or even higher average weight. The plant population was therefore exactly as good at inoculation as at the untreated non-infected control plants.
Eksempel 1. Example 1.
8 g N-butyl-N'-metylsulfamid oppløses under tilsetning av 17 g fluordiklormetansulfenylklorid i 100 ml benzol og blandes ved værelsetemperatur med 11 g trietylamin. Herved øker temperaturen til ca. 35°G. Man frafiltrerer utfelt trietylaminhydroklorid, inn-damper den benzoliske oppløsning i vakuum og får som residum 13 g av den ovennevnte forbindelse i form av en seig olje. 8 g of N-butyl-N'-methylsulfamide are dissolved with the addition of 17 g of fluorodichloromethanesulphenyl chloride in 100 ml of benzene and mixed at room temperature with 11 g of triethylamine. This increases the temperature to approx. 35°G. Precipitated triethylamine hydrochloride is filtered off, the benzoic solution is evaporated in vacuo and 13 g of the above-mentioned compound are obtained as a residue in the form of a viscous oil.
Analyse: beregnet: S 22,2 Cl 32,9 Analysis: calculated: S 22.2 Cl 32.9
funnet: S 22,2 Cl 30,1 found: S 22.2 Cl 30.1
På samme måte får man: In the same way, you get:
Eksempel 2. Example 2.
Eksempel 3. Example 3.
9 g N,N'-diallylsulfamid oppløses under tilsetning av 9 g of N,N'-diallyl sulfamide are dissolved while adding
11 g trietylamin i 150 ml benzol og blandes ved værelsetemperatur dråpevis med 17 g fluordiklormetansulfenylklorid. Herved lar man temperaturen øke til 40°C. Man utryster reaksjonsoppløsningen med vann, tørker den benzoliske oppløsning over natriumsulfat og får etter benzolens avdampning 20 g av en seigtflytende olje av ovennevnte konstitusjon. 11 g of triethylamine in 150 ml of benzene and mixed at room temperature dropwise with 17 g of fluorodichloromethanesulphenyl chloride. This allows the temperature to rise to 40°C. The reaction solution is shaken with water, the benzolic solution is dried over sodium sulphate and, after the benzene has evaporated, 20 g of a viscous oil of the above-mentioned constitution are obtained.
ng<0>: 1,5301. ng<0>: 1.5301.
Claims (1)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR8411400A FR2568065B1 (en) | 1984-07-18 | 1984-07-18 | SELF-LIFE TEST DEVICE FOR SAFETY LIGHTING BLOCK |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| NO852842L NO852842L (en) | 1986-01-20 |
| NO166609B true NO166609B (en) | 1991-05-06 |
| NO166609C NO166609C (en) | 1991-08-14 |
Family
ID=9306251
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO852842A NO166609C (en) | 1984-07-18 | 1985-07-16 | DEVICE FOR TESTING THE FUNCTIONALITY OF AN EMERGENCY LIGHTING DEVICE. |
Country Status (5)
| Country | Link |
|---|---|
| EP (1) | EP0171629B1 (en) |
| AT (1) | ATE51328T1 (en) |
| DE (1) | DE3576770D1 (en) |
| FR (1) | FR2568065B1 (en) |
| NO (1) | NO166609C (en) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2197760A (en) * | 1986-10-31 | 1988-05-25 | Fano Int Ltd | Emergency lighting unit |
| FR2616929B1 (en) * | 1987-06-18 | 1989-12-15 | Impex Comptoir General | AUTONOMY TEST CONTROL DEVICE FOR A SET OF SAFETY LIGHTING BLOCKS |
| IT1213713B (en) * | 1987-10-29 | 1989-12-29 | Monteveglio Bo A | AUTONOMOUS EMERGENCY LIGHTING SYSTEM WITH PROGRAMMED, DISPLAYED AND EVENTUALLY CENTRALIZED SELF-DIAGNOSIS IN CONNECTION WITH THE POWER SUPPLY |
| FR2631754B1 (en) * | 1988-05-20 | 1993-07-30 | Accumulateurs Fixes | SELF-LIFE TEST APPARATUS FOR SAFETY LIGHTING BLOCK |
| CN104837259B (en) * | 2015-05-08 | 2018-05-29 | 申勇兵 | There is the on-off circuit of emergency starting power device |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2016223B (en) * | 1978-02-09 | 1982-11-03 | Maylectro Ltd | Emergency lighting |
| ZA782491B (en) * | 1978-05-01 | 1979-12-27 | Anglo Amer Corp South Africa | Battery testing |
| DE2851599C2 (en) * | 1978-11-29 | 1987-01-29 | Theo Benning Elektrotechnik Und Elektronik Gmbh & Co Kg, 4290 Bocholt | Device for automatic testing of battery capacity |
| DE3070600D1 (en) * | 1979-12-04 | 1985-06-05 | Emlux Ltd | Testing emergency battery equipment |
| FR2477282A1 (en) * | 1980-02-29 | 1981-09-04 | Sncf | Accumulator battery charge and discharge control monitor - uses transistor to maintain constant current charge and discharge and clock running only while current flows to show amount of use |
-
1984
- 1984-07-18 FR FR8411400A patent/FR2568065B1/en not_active Expired
-
1985
- 1985-07-16 AT AT85108873T patent/ATE51328T1/en not_active IP Right Cessation
- 1985-07-16 EP EP85108873A patent/EP0171629B1/en not_active Expired - Lifetime
- 1985-07-16 DE DE8585108873T patent/DE3576770D1/en not_active Expired - Fee Related
- 1985-07-16 NO NO852842A patent/NO166609C/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| EP0171629B1 (en) | 1990-03-21 |
| ATE51328T1 (en) | 1990-04-15 |
| EP0171629A1 (en) | 1986-02-19 |
| NO166609C (en) | 1991-08-14 |
| NO852842L (en) | 1986-01-20 |
| FR2568065B1 (en) | 1986-11-14 |
| FR2568065A1 (en) | 1986-01-24 |
| DE3576770D1 (en) | 1990-04-26 |
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