NO161615B - DEVICE FOR SUPPLY AND DISPOSAL OF ETSNATRON Melt. - Google Patents

DEVICE FOR SUPPLY AND DISPOSAL OF ETSNATRON Melt. Download PDF

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Publication number
NO161615B
NO161615B NO831837A NO831837A NO161615B NO 161615 B NO161615 B NO 161615B NO 831837 A NO831837 A NO 831837A NO 831837 A NO831837 A NO 831837A NO 161615 B NO161615 B NO 161615B
Authority
NO
Norway
Prior art keywords
caustic soda
melt
etsnatron
disposal
supply
Prior art date
Application number
NO831837A
Other languages
Norwegian (no)
Other versions
NO161615C (en
NO831837L (en
Inventor
Kurt Hennesen
Fritz Krahl
Heinz Steinroetter
Siegfried Benninger
Original Assignee
Hoechst Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hoechst Ag filed Critical Hoechst Ag
Publication of NO831837L publication Critical patent/NO831837L/en
Publication of NO161615B publication Critical patent/NO161615B/en
Publication of NO161615C publication Critical patent/NO161615C/en

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05BSPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
    • B05B3/00Spraying or sprinkling apparatus with moving outlet elements or moving deflecting elements
    • B05B3/02Spraying or sprinkling apparatus with moving outlet elements or moving deflecting elements with rotating elements
    • B05B3/10Spraying or sprinkling apparatus with moving outlet elements or moving deflecting elements with rotating elements discharging over substantially the whole periphery of the rotating member, i.e. the spraying being effected by centrifugal forces
    • B05B3/1057Spraying or sprinkling apparatus with moving outlet elements or moving deflecting elements with rotating elements discharging over substantially the whole periphery of the rotating member, i.e. the spraying being effected by centrifugal forces with at least two outlets, other than gas and cleaning fluid outlets, for discharging, selectively or not, different or identical liquids or other fluent materials on the rotating element
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/02Apparatus characterised by being constructed of material selected for its chemically-resistant properties
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • B01J2/02Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops
    • B01J2/04Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops in a gaseous medium
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05BSPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
    • B05B1/00Nozzles, spray heads or other outlets, with or without auxiliary devices such as valves, heating means
    • B05B1/14Nozzles, spray heads or other outlets, with or without auxiliary devices such as valves, heating means with multiple outlet openings; with strainers in or outside the outlet opening
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05BSPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
    • B05B3/00Spraying or sprinkling apparatus with moving outlet elements or moving deflecting elements
    • B05B3/02Spraying or sprinkling apparatus with moving outlet elements or moving deflecting elements with rotating elements
    • B05B3/10Spraying or sprinkling apparatus with moving outlet elements or moving deflecting elements with rotating elements discharging over substantially the whole periphery of the rotating member, i.e. the spraying being effected by centrifugal forces
    • B05B3/1007Spraying or sprinkling apparatus with moving outlet elements or moving deflecting elements with rotating elements discharging over substantially the whole periphery of the rotating member, i.e. the spraying being effected by centrifugal forces characterised by the rotating member
    • B05B3/1021Spraying or sprinkling apparatus with moving outlet elements or moving deflecting elements with rotating elements discharging over substantially the whole periphery of the rotating member, i.e. the spraying being effected by centrifugal forces characterised by the rotating member with individual passages at its periphery
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D1/00Oxides or hydroxides of sodium, potassium or alkali metals in general
    • C01D1/04Hydroxides
    • C01D1/42Concentration; Dehydration
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/02Apparatus characterised by their chemically-resistant properties
    • B01J2219/0204Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/02Apparatus characterised by their chemically-resistant properties
    • B01J2219/0204Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components
    • B01J2219/0227Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components of graphite

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Structures Of Non-Positive Displacement Pumps (AREA)
  • Processing Of Solid Wastes (AREA)
  • Detergent Compositions (AREA)
  • Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)
  • Breeding Of Plants And Reproduction By Means Of Culturing (AREA)
  • Micro-Organisms Or Cultivation Processes Thereof (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)
  • Coating By Spraying Or Casting (AREA)
  • Nozzles (AREA)
  • Glanulating (AREA)
  • Furnace Housings, Linings, Walls, And Ceilings (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)

Abstract

1. A device for feeding and spraying molten caustic soda which substantially consists of lye pump and spray head, wherein those parts of the device being in direct contact with the molten caustic soda are coated with glassy carbon.

Description

Oppfinnelsens gjenstand er en innretning til tilførsel og utslynging av etsnatronsmelte som i det vesentlige består av lutpumpe og slyngekurv. The object of the invention is a device for supplying and ejecting caustic soda melt which essentially consists of a lye pump and a sling basket.

Ved fremstilling av fast etsnatron eller Prill-fremgangsmåten tilføres etsnatronsmelte ved hjelp av en lutpumpe, f.eks. en dykkepumpe, til en slyngekurv hvormed den ved toppen av et Prill-tårn oppdeles i enkelte små dråper. Derved har det vist seg at innretningsdelene som spesielt kommer i berøring med den strømmengde etsnatronlut og evt. i tillegg med oksygen ligger under for en betraktelig slitasje enskjønt de er fremstilt av edelstål, nikkel, nikkellegeringer, sølv eller edelmetallegeringer. When producing solid caustic soda or the Prill method, caustic soda melt is added using a lye pump, e.g. a submersible pump, to a sling basket with which it is divided into individual small drops at the top of a Prill tower. Thereby, it has been shown that the equipment parts that come into contact with the flowing caustic soda and possibly also with oxygen are subject to considerable wear and tear, even though they are made of stainless steel, nickel, nickel alloys, silver or precious metal alloys.

Det besto følgelig den oppgave å tilveiebringe en innretning hvis deler som kommer i berøring med etsnatronsmelte er best mulig beskyttet mot slitasje. The task was therefore to provide a device whose parts that come into contact with caustic soda melt are as well protected against wear as possible.

Oppgaven løses Ifølge oppfinnelsen ved at Innretningens deler som kommer direkte i berøring med etsnatronsmelten består av glasskarbon eller er belagt med glasskarbon. According to the invention, the task is solved in that the parts of the Device that come into direct contact with the caustic soda melt consist of glassy carbon or are coated with glassy carbon.

Alle innretningens deler som deler av pumper, ventiler, rør rørbuer, armaturer, slyngekurver osv. som kommer i berøring med etsnatronsmelte kan bestå av glasskarbon respektiv belegges med glasskarbon. All parts of the device such as parts of pumps, valves, pipes, pipe bends, fittings, sling baskets etc. that come into contact with caustic soda melt can consist of glass carbon or be coated with glass carbon.

Oppfinnelsen skal forklares nærmere ved hjelp av to ek-sempler . The invention will be explained in more detail using two examples.

Fig. 1 viser en slyngekurv for etsnatronsmelte, og fig. 2 viser en dykkepumpe for etsnatronsmelte. Fig. 1 shows a sling basket for caustic soda melt, and fig. 2 shows a submersible pump for caustic soda melting.

Slyngekurven (fig. 1) består av en hylse 1 til opptak av drivaksen som Ikke er vist og bunndelen 2. På bunndelen 2 sitter mantelen 4 av kurven av glasskarbon med hullene 10 hvorigjennom etsnatronsmelten forstøves. Gjennom et dekke, en ring 3 og ankeret bestående av bolter 5, underlagsskiver 6 og muttere 7 holdes mantelen 4. Bunndelen 2 og hylsen 1 er beskyttet ved hjelp av en boks 8 og boltene 5 av hylser 9 av glasskarbon. 11 er tilførselsledninger for etsnatronsmelter som gjennom en ringspalte 12 rager inn i slyngekurven. The sling basket (fig. 1) consists of a sleeve 1 for receiving the drive shaft, which is not shown, and the bottom part 2. On the bottom part 2 sits the mantle 4 of the basket made of glass carbon with the holes 10 through which the caustic soda melt is atomized. Through a cover, a ring 3 and the anchor consisting of bolts 5, washers 6 and nuts 7, the mantle 4 is held. The bottom part 2 and the sleeve 1 are protected by means of a box 8 and the bolts 5 by sleeves 9 of glass carbon. 11 are supply lines for caustic soda melts that project through an annular gap 12 into the sling basket.

Pumpehuset av dykkepumpen (fig. 2) består av ledeinnretningen 13 og sugelokk 14. Navet av løpehjulet 15 rager gjennom ledeinnretningen 13 bestående av pumpehus 18, boks 17 og ledeskovler 19 og opptar drivakselen. Ledeinnretningen 13 har en boks 17 til beskyttelse av pumpehusdelen 18. Boksen 17 har ledeskovler 19. Likeledes er sugelokket 14 utstyrt med en boks 20 som beskytter lokket 14 og hvis stusser 21 tjener som sugerør for etsnatronsmelten. Sugelokk 14 og pumpehuset 18 begrenser en ringkanal 22 hvorover etsnatronsmelten tilføres til en utløpsstuss 23. I ringkanalen 22 er det anordnet en ledering 24. Boks 17 med ledeskovler 19, boks 20 med stusser 21 og pumpehjul er fremstilt av glasskarbon. Lederingen 24 kan likeledes bestå av glasskarbon. The pump housing of the submersible pump (fig. 2) consists of the guide device 13 and suction cap 14. The hub of the impeller 15 protrudes through the guide device 13 consisting of pump housing 18, box 17 and guide vanes 19 and occupies the drive shaft. The guide device 13 has a box 17 to protect the pump housing part 18. The box 17 has guide vanes 19. Likewise, the suction lid 14 is equipped with a box 20 which protects the lid 14 and whose nozzle 21 serves as a suction tube for the caustic soda melt. Suction cap 14 and pump housing 18 limit an annular channel 22 over which the caustic soda melt is supplied to an outlet nozzle 23. In the annular channel 22, a guide ring 24 is arranged. Box 17 with guide vanes 19, box 20 with nozzles 21 and impeller are made of carbon glass. The conductor ring 24 can likewise consist of glassy carbon.

Claims (1)

Innretning til tilførsel og utslyngning eller forstøvning av etsnatronsmelte og som i det vesentlige består av lutpumpe (fig. 2) og slyngekurv (fig. 1),karakterisert ved at innretningens deler som kommer direkte i berøring med etsnatronsmelten er belagt med glasskarbon eller består av glasskarbon.Device for supplying and ejecting or atomizing caustic soda melt and which essentially consists of a lye pump (fig. 2) and sling basket (fig. 1), characterized in that the parts of the device that come into direct contact with the caustic soda melt are coated with glass carbon or consist of glass carbon .
NO831837A 1982-05-25 1983-05-24 DEVICE FOR SUPPLY AND DISPOSAL OF ETSNATRON Melt. NO161615C (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19823219497 DE3219497A1 (en) 1982-05-25 1982-05-25 DEVICE FOR FEEDING AND SPRAYING MELTING MELT

Publications (3)

Publication Number Publication Date
NO831837L NO831837L (en) 1983-11-28
NO161615B true NO161615B (en) 1989-05-29
NO161615C NO161615C (en) 1989-09-06

Family

ID=6164373

Family Applications (1)

Application Number Title Priority Date Filing Date
NO831837A NO161615C (en) 1982-05-25 1983-05-24 DEVICE FOR SUPPLY AND DISPOSAL OF ETSNATRON Melt.

Country Status (8)

Country Link
EP (1) EP0095145B1 (en)
JP (1) JPS58208134A (en)
AT (1) ATE18513T1 (en)
CA (1) CA1197959A (en)
DE (2) DE3219497A1 (en)
FI (1) FI72901C (en)
NO (1) NO161615C (en)
ZA (1) ZA833722B (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3834151C1 (en) * 1988-10-07 1989-12-07 Benckiser-Knapsack Gmbh, 6802 Ladenburg, De
DE4439924A1 (en) * 1994-11-08 1996-05-09 Bayerische Motoren Werke Ag Carbon@ cladding layer for electrostatic spraying
DE19801700A1 (en) * 1998-01-17 1999-07-22 Cit Alcatel Fiber coating equipment, especially for optical glass fiber
DE19914165A1 (en) * 1999-03-29 2000-10-19 Bk Giulini Chem Gmbh & Co Ohg Device for the production of corrosive phosphate melts

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1475809A (en) * 1966-02-17 1967-04-07 Lorraine Carbone Application of vitreous carbon to the manufacture of dies, wire guides, wear parts
US3733151A (en) * 1972-03-01 1973-05-15 Dow Chemical Co Pump assembly for handling liquid materials
DE2451969C2 (en) * 1974-10-30 1976-11-08 Aerospace Corp PROCESS FOR GLAZING WORKPIECES MADE OF CERAMIC, CHARCOAL OR CARBON

Also Published As

Publication number Publication date
CA1197959A (en) 1985-12-17
FI831830L (en) 1983-11-26
FI72901B (en) 1987-04-30
DE3219497A1 (en) 1983-12-01
FI72901C (en) 1987-08-10
FI831830A0 (en) 1983-05-23
ZA833722B (en) 1985-01-30
DE3362521D1 (en) 1986-04-17
EP0095145A2 (en) 1983-11-30
EP0095145B1 (en) 1986-03-12
JPS58208134A (en) 1983-12-03
ATE18513T1 (en) 1986-03-15
NO161615C (en) 1989-09-06
NO831837L (en) 1983-11-28
EP0095145A3 (en) 1984-05-02

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