NO139660B - SEILING AID. - Google Patents
SEILING AID. Download PDFInfo
- Publication number
- NO139660B NO139660B NO750724A NO750724A NO139660B NO 139660 B NO139660 B NO 139660B NO 750724 A NO750724 A NO 750724A NO 750724 A NO750724 A NO 750724A NO 139660 B NO139660 B NO 139660B
- Authority
- NO
- Norway
- Prior art keywords
- addition
- propylene glycol
- group
- weight
- samples
- Prior art date
Links
- 239000004460 silage Substances 0.000 claims description 13
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 claims description 12
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical group CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 11
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical group O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 6
- 235000019260 propionic acid Nutrition 0.000 claims description 6
- KFNABOVSAPCOCY-UHFFFAOYSA-N 1-propanoyloxypropan-2-yl propanoate Chemical compound CCC(=O)OCC(C)OC(=O)CC KFNABOVSAPCOCY-UHFFFAOYSA-N 0.000 claims description 3
- 240000004658 Medicago sativa Species 0.000 claims description 2
- 239000004480 active ingredient Substances 0.000 claims description 2
- RLUCXJBHKHIDSP-UHFFFAOYSA-N propane-1,2-diol;propanoic acid Chemical class CCC(O)=O.CC(O)CO RLUCXJBHKHIDSP-UHFFFAOYSA-N 0.000 claims description 2
- 235000010624 Medicago sativa Nutrition 0.000 claims 1
- 238000007792 addition Methods 0.000 description 14
- 150000002148 esters Chemical class 0.000 description 12
- 238000000855 fermentation Methods 0.000 description 9
- 230000004151 fermentation Effects 0.000 description 9
- FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Chemical compound CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 description 8
- 239000002253 acid Substances 0.000 description 8
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 8
- 150000007513 acids Chemical class 0.000 description 6
- 230000015572 biosynthetic process Effects 0.000 description 6
- 230000000694 effects Effects 0.000 description 6
- 239000000126 substance Substances 0.000 description 6
- 239000000654 additive Substances 0.000 description 4
- 239000004310 lactic acid Substances 0.000 description 4
- 235000014655 lactic acid Nutrition 0.000 description 4
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 4
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 240000008042 Zea mays Species 0.000 description 2
- 235000016383 Zea mays subsp huehuetenangensis Nutrition 0.000 description 2
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 2
- 235000019253 formic acid Nutrition 0.000 description 2
- 235000009973 maize Nutrition 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- SZLBUGKDPCQASQ-UHFFFAOYSA-N 1-hydroxypropan-2-yl propanoate Chemical compound CCC(=O)OC(C)CO SZLBUGKDPCQASQ-UHFFFAOYSA-N 0.000 description 1
- AAMWEWAFFUFOJV-UHFFFAOYSA-N 2-hydroxypropyl propanoate Chemical compound CCC(=O)OCC(C)O AAMWEWAFFUFOJV-UHFFFAOYSA-N 0.000 description 1
- 235000016068 Berberis vulgaris Nutrition 0.000 description 1
- 241000335053 Beta vulgaris Species 0.000 description 1
- BCZXFFBUYPCTSJ-UHFFFAOYSA-L Calcium propionate Chemical compound [Ca+2].CCC([O-])=O.CCC([O-])=O BCZXFFBUYPCTSJ-UHFFFAOYSA-L 0.000 description 1
- 244000025254 Cannabis sativa Species 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 241000209082 Lolium Species 0.000 description 1
- 235000017587 Medicago sativa ssp. sativa Nutrition 0.000 description 1
- -1 NaH^(PO^)^.NaHSO^ Chemical class 0.000 description 1
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 1
- 244000061456 Solanum tuberosum Species 0.000 description 1
- 235000002595 Solanum tuberosum Nutrition 0.000 description 1
- 241000219793 Trifolium Species 0.000 description 1
- 241000219873 Vicia Species 0.000 description 1
- 239000002250 absorbent Substances 0.000 description 1
- 230000002745 absorbent Effects 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 150000001447 alkali salts Chemical class 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 235000010331 calcium propionate Nutrition 0.000 description 1
- 239000004330 calcium propionate Substances 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 235000012015 potatoes Nutrition 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- JXKPEJDQGNYQSM-UHFFFAOYSA-M sodium propionate Chemical compound [Na+].CCC([O-])=O JXKPEJDQGNYQSM-UHFFFAOYSA-M 0.000 description 1
- 235000010334 sodium propionate Nutrition 0.000 description 1
- 239000004324 sodium propionate Substances 0.000 description 1
- 229960003212 sodium propionate Drugs 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K30/00—Processes specially adapted for preservation of materials in order to produce animal feeding-stuffs
- A23K30/10—Processes specially adapted for preservation of materials in order to produce animal feeding-stuffs of green fodder
- A23K30/15—Processes specially adapted for preservation of materials in order to produce animal feeding-stuffs of green fodder using chemicals or microorganisms for ensilaging
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Polymers & Plastics (AREA)
- Zoology (AREA)
- Microbiology (AREA)
- Animal Husbandry (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Fodder In General (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Food Preservation Except Freezing, Refrigeration, And Drying (AREA)
Description
Oppfinnelsen vedrører sileringshjelpemiddel. Ved sileringen, fremstillingen av gjæringsf6r, er dannelsen av melkesyre vesentlig. Det er i mange tilfeller hensiktsmessig eller nødvendig å påvirke gjæringen ved tilblanding av tilsetningsstoffer, for å befordre veksten av melkesyrebakterier og samtidig å hemme uønskede gjæringsprosesser, spesielt å undertrykke vekst av de mikro-organismer som bevirker dannelsen av smørsyre. Ut-slagsgivende for kvaliteten av silof6ret er spesielt gjæringsfor-løpet under de første dager. The invention relates to a silage aid. During silage, the production of fermentation broth, the formation of lactic acid is essential. In many cases, it is appropriate or necessary to influence the fermentation by adding additives, in order to promote the growth of lactic acid bacteria and at the same time to inhibit unwanted fermentation processes, in particular to suppress the growth of the micro-organisms that cause the formation of butyric acid. Decisive for the quality of the silage is especially the fermentation process during the first days.
Det er kjent at ved en pH-verdi på ca. 4 er omtrent utelukkende melkesyrebakterier levedyktige, og man benytter derfor som tilsetningsstoffer for silering, syrer som er egnet til inn-stilling av en tilsvarende-pH-verdi. Det anvendes eksempelvis maursyre, propionsyre eller blandinger av slatsyre med svovelsyre eller fosforsyre. Ved syretilsetningen kan dannelsen av smørsyre hemmes virksomt fra begynnelsen. Det er også kjent å anvende saltene av de nevnte syrer. Hvis det dreier seg om de sure alkali-salter av mineralsyrer som eksempelvis NaH^(PO^)^.NaHSO^, tilsvarer virkningen sterkt virkningen av de frie syrer. Anvendes imidlertid nøytrale salter, som eksempelvis natriumpropionat eller kal-siumpropionat, så er virkningen langsommere og mindre enn ved de frie syrer. Spesielt hemmes dannelsen av smørsyre i den av-gjørende begynnelsesfase av gjæringen bare utilstrekkelig. It is known that at a pH value of approx. 4, almost exclusively lactic acid bacteria are viable, and acids which are suitable for setting a corresponding pH value are therefore used as additives for silage. For example, formic acid, propionic acid or mixtures of formic acid with sulfuric acid or phosphoric acid are used. With the addition of acid, the formation of butyric acid can be effectively inhibited from the beginning. It is also known to use the salts of the aforementioned acids. If it concerns the acid alkali salts of mineral acids such as NaH^(PO^)^.NaHSO^, the effect strongly corresponds to the effect of the free acids. However, if neutral salts are used, such as sodium propionate or calcium propionate, the effect is slower and less than with the free acids. In particular, the formation of butyric acid in the decisive initial phase of the fermentation is inhibited only insufficiently.
Oppfinnelsen vedrører sileringshjelpemiddel som er karakterisert ved at det som virksomt stoff inneholder propylenglykolestrene av propionsyre. Enskjønt.det ved estrene dreier seg om nøytralt reagerende stoffer, inntrer virkningen hurtigere og ster-kere enn ved syrer. Det hindrer ikke bare den uønskede gjæringspro-sess med dannelse av smørsyre på utmerket måte, men det befordrer dessuten dannelsen av melkesyre. Virkningen av esteren over-treffer virkningen av propionsyre enskjønt esterens alkoholkom-ponent, 1,2-propylenglykol anvendt alene viser seg som stoff som ugunstig påvirker gjæringen. The invention relates to a silage aid which is characterized in that it contains the propylene glycol esters of propionic acid as an active ingredient. Although the esters are neutrally reactive substances, the effect occurs faster and stronger than with acids. It not only prevents the undesirable fermentation process with the formation of butyric acid in an excellent way, but it also promotes the formation of lactic acid. The effect of the ester exceeds that of propionic acid, although the ester's alcohol component, 1,2-propylene glycol used alone, appears to be a substance that adversely affects the fermentation.
Som .tilsetningsstoff ifølge oppfinnelsen kommer det på tale samtlige 1,2-propylenglykolestere av propionsyre, nemlig propylenglykol-l-monopropionat, propylenglykol-2-monopropionat og propylenglykol-1,2-dipropionat. Det kan i samme grad anvendes de enkelte estere eller blandinger av estere. Additives according to the invention include all 1,2-propylene glycol esters of propionic acid, namely propylene glycol-1-monopropionate, propylene glycol-2-monopropionate and propylene glycol-1,2-dipropionate. The individual esters or mixtures of esters can be used to the same extent.
Konsentrasjonen av esteren i sileringen kan velges innen vide grenser og retter seg i en viss grad etter typen av siloen og sileringsbetingelsene. Vanligvis er det hensiktsmessig til stoffene som skal sileres å sette minst 0,01 til 1,0 The concentration of the ester in the silage can be chosen within wide limits and depends to a certain extent on the type of silo and the silage conditions. Generally, it is appropriate for the substances to be sieved to set at least 0.01 to 1.0
vekt% ester. Større tilsetninger, f.eks. på 2 eller 5 vekt% er bare sjelden av betydning. Fortrinnsvis utgjør estertilsetningen 0,1 til 0,5 vekt%. wt% ester. Larger additions, e.g. of 2 or 5% by weight is only rarely of importance. Preferably, the ester addition amounts to 0.1 to 0.5% by weight.
Estrene anvendes spesielt som sådanne. De kan imidlertid også anvendes i blanding med andre stoffer. Herved kan det dreie seg om stoffer som på sin side har en virkning som tilsetningsstoff for sileringen eller som konserveringsstoffer eller om stoffer, som er inaktive. En sammenblanding av estrene med høy-dispers silisiumdioksyd eller andre absorbtivt virkende faststoffer kan eventuelt tjene til å overføre estrene, hvor det dreier seg om med vann lite blandbare væsker i et risledyktig faststoff. The esters are used in particular as such. However, they can also be used in a mixture with other substances. This may refer to substances which in turn have an effect as an additive for silage or as preservatives or to substances which are inactive. A mixture of the esters with highly-dispersed silicon dioxide or other absorbent solids can possibly serve to transfer the esters, where it is a question of liquids that are not very miscible with water in a solid that can drip.
Estrene som ifølge oppfinnelsen anvendes som hjelpemiddel egner seg for alle typer sileringer, spesielt for silering av planter som gress, luzern, vikkekorn, kløver, grønn-mais, roer og poteter. The esters which, according to the invention, are used as aids are suitable for all types of silage, especially for silage of plants such as grass, alfalfa, vetch, clover, green maize, beets and potatoes.
Eksempel 1 Example 1
Det ble silert prøver på hver 650 g nymalt viegress. Samples of each 650 g of freshly ground rye grass were sieved.
Tilsammen ble det satt 56 prøver, nemlig i 7 grupper på hver 8 like prøver: A total of 56 samples were set, namely in 7 groups of 8 equal samples each:
Gruppe 1 uten enhver tilsetning Group 1 without any addition
Gruppe 2a med tilsetning av 0,2 vekt% propylenglykol Gruppe 2b med tilsetning av 0,4 vekt% propylenglykol Gruppe 3a med tilsetning av 0,2 vekt% propionsyre \ Gruppe 3b med tilsetning av 0,4 vekt% propionsyre Gruppe 4a med tilsetning av 0,2 vekt% propylenglykol-1 ,\-dipropionat Group 2a with the addition of 0.2% by weight propylene glycol Group 2b with the addition of 0.4% by weight propylene glycol Group 3a with the addition of 0.2% by weight propionic acid \ Group 3b with the addition of 0.4% by weight propionic acid Group 4a with the addition of 0.2% by weight propylene glycol-1,\-dipropionate
\ \
Gruppe 4b med tilsetning av 0,4 vekt% propylenglykol-1,2-dipropionat. Group 4b with the addition of 0.4% by weight of propylene glycol-1,2-dipropionate.
Prøvene ble oppbevart i gasstett lukkede kar på The samples were stored in gas-tight closed vessels on
1 liters rominnhold ved ytre temperaturer på 24°C i 90 dager. 1 liter room content at external temperatures of 24°C for 90 days.
For vurdering av sileringens kvalitet ble det som grad for tap av næringsstoffer under gjæringen fastslått gjærings-gasstap. Det ble videre bestemt kvaliteten av sileringen ifølge lukt, farve og struktur ifølge DLG-gjærf6rnøkkelen (Handbuch der Futtermittel, bind 1 (1969), Verlag Paul Parey, Hamburg og Berlin). Resultatene var følgende: To assess the quality of the silage, fermentation gas loss was determined as the degree of loss of nutrients during fermentation. The quality of the silage was further determined according to smell, color and structure according to the DLG yeast key (Handbuch der Futtermittel, volume 1 (1969), Verlag Paul Parey, Hamburg and Berlin). The results were as follows:
Eksempel 2 Example 2
Det ble gått frem ifølge Eksempel 1, imidlertid It was proceeded according to Example 1, however
ble det silert prøver på hver 820 g fuktig maiskorn, Tilsammen ble det satt 32 prøver, nemlig i fire grupper på hver 8 like prøver. samples of each 820 g of moist maize grain were sieved. A total of 32 samples were collected, namely in four groups of 8 equal samples each.
Gruppe 1 uten enhver tilsetning Group 1 without any addition
Gruppe 2 tilsetning av 0,4 vekt% propylenglykol Group 2 addition of 0.4% by weight propylene glycol
Gruppe 3 tilsetning av 0,4 vekt% propionsyre Gruppe 4 tilsetning av 0,4 vekt% av en blanding av de to propylenglykolmonopropionater. Group 3 addition of 0.4% by weight of propionic acid Group 4 addition of 0.4% by weight of a mixture of the two propylene glycol monopropionates.
Resultatene var følgende: The results were as follows:
Claims (1)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2412834A DE2412834A1 (en) | 1974-03-16 | 1974-03-16 | SILAGE AIDS |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| NO750724L NO750724L (en) | 1975-09-17 |
| NO139660B true NO139660B (en) | 1979-01-15 |
| NO139660C NO139660C (en) | 1979-04-25 |
Family
ID=5910345
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO750724A NO139660C (en) | 1974-03-16 | 1975-03-04 | SEILING AID. |
Country Status (17)
| Country | Link |
|---|---|
| AT (1) | AT345653B (en) |
| BE (1) | BE826736A (en) |
| CA (1) | CA1047301A (en) |
| CH (1) | CH616567A5 (en) |
| CS (1) | CS182832B2 (en) |
| DD (1) | DD118521A5 (en) |
| DE (1) | DE2412834A1 (en) |
| DK (1) | DK104275A (en) |
| FI (1) | FI57047C (en) |
| FR (1) | FR2263702A1 (en) |
| GB (1) | GB1489320A (en) |
| HU (1) | HU169511B (en) |
| NL (1) | NL7502743A (en) |
| NO (1) | NO139660C (en) |
| PL (1) | PL92446B1 (en) |
| SE (1) | SE7502925L (en) |
| SU (1) | SU606530A3 (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3540771A1 (en) * | 1985-11-16 | 1987-05-21 | Basf Ag | USE OF PROPANDIOL FORMAT IN FEED OR DRINKING WATER FOR ANIMALS |
-
1974
- 1974-03-16 DE DE2412834A patent/DE2412834A1/en not_active Withdrawn
-
1975
- 1975-02-13 FI FI750395A patent/FI57047C/en not_active IP Right Cessation
- 1975-02-21 SU SU752107252A patent/SU606530A3/en active
- 1975-02-25 CS CS7500001242A patent/CS182832B2/en unknown
- 1975-03-04 NO NO750724A patent/NO139660C/en unknown
- 1975-03-07 NL NL7502743A patent/NL7502743A/en not_active Application Discontinuation
- 1975-03-10 GB GB9809/75A patent/GB1489320A/en not_active Expired
- 1975-03-14 AT AT196875A patent/AT345653B/en not_active IP Right Cessation
- 1975-03-14 BE BE6044954A patent/BE826736A/en unknown
- 1975-03-14 CA CA222,101A patent/CA1047301A/en not_active Expired
- 1975-03-14 HU HUDE883A patent/HU169511B/hu unknown
- 1975-03-14 DK DK104275A patent/DK104275A/da unknown
- 1975-03-14 SE SE7502925A patent/SE7502925L/xx unknown
- 1975-03-14 DD DD184785A patent/DD118521A5/xx unknown
- 1975-03-14 CH CH329675A patent/CH616567A5/en not_active IP Right Cessation
- 1975-03-15 PL PL1975178796A patent/PL92446B1/pl unknown
- 1975-03-17 FR FR7508275A patent/FR2263702A1/fr not_active Withdrawn
Also Published As
| Publication number | Publication date |
|---|---|
| GB1489320A (en) | 1977-10-19 |
| CA1047301A (en) | 1979-01-30 |
| DE2412834A1 (en) | 1975-09-18 |
| NO139660C (en) | 1979-04-25 |
| ATA196875A (en) | 1978-01-15 |
| FI750395A (en) | 1975-09-17 |
| FR2263702A1 (en) | 1975-10-10 |
| AT345653B (en) | 1978-09-25 |
| BE826736A (en) | 1975-09-15 |
| NO750724L (en) | 1975-09-17 |
| DK104275A (en) | 1975-09-17 |
| CH616567A5 (en) | 1980-04-15 |
| SE7502925L (en) | 1975-09-17 |
| DD118521A5 (en) | 1976-03-12 |
| FI57047C (en) | 1980-06-10 |
| SU606530A3 (en) | 1978-05-05 |
| NL7502743A (en) | 1975-09-18 |
| CS182832B2 (en) | 1978-05-31 |
| HU169511B (en) | 1976-12-28 |
| FI57047B (en) | 1980-02-29 |
| PL92446B1 (en) | 1977-04-30 |
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