NO130928B - - Google Patents
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- Publication number
- NO130928B NO130928B NO00170356A NO17035667A NO130928B NO 130928 B NO130928 B NO 130928B NO 00170356 A NO00170356 A NO 00170356A NO 17035667 A NO17035667 A NO 17035667A NO 130928 B NO130928 B NO 130928B
- Authority
- NO
- Norway
- Prior art keywords
- parts
- pentaerythritol
- temperature
- acetaldehyde
- azo
- Prior art date
Links
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 46
- IKHGUXGNUITLKF-UHFFFAOYSA-N Acetaldehyde Chemical compound CC=O IKHGUXGNUITLKF-UHFFFAOYSA-N 0.000 claims description 42
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 claims description 27
- 238000006243 chemical reaction Methods 0.000 claims description 21
- 239000003054 catalyst Substances 0.000 claims description 16
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 15
- 238000000034 method Methods 0.000 claims description 15
- 239000000203 mixture Substances 0.000 claims description 15
- OZAIFHULBGXAKX-UHFFFAOYSA-N 2-(2-cyanopropan-2-yldiazenyl)-2-methylpropanenitrile Chemical compound N#CC(C)(C)N=NC(C)(C)C#N OZAIFHULBGXAKX-UHFFFAOYSA-N 0.000 claims description 14
- 239000012429 reaction media Substances 0.000 claims description 12
- 239000003795 chemical substances by application Substances 0.000 claims description 10
- 239000007788 liquid Substances 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims description 7
- 239000000920 calcium hydroxide Substances 0.000 claims description 7
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 7
- QSJXEFYPDANLFS-UHFFFAOYSA-N Diacetyl Chemical compound CC(=O)C(C)=O QSJXEFYPDANLFS-UHFFFAOYSA-N 0.000 claims description 6
- 229930040373 Paraformaldehyde Natural products 0.000 claims description 5
- 150000001299 aldehydes Chemical class 0.000 claims description 5
- 238000009833 condensation Methods 0.000 claims description 4
- 230000005494 condensation Effects 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 229920002866 paraformaldehyde Polymers 0.000 claims description 4
- 238000010561 standard procedure Methods 0.000 claims description 4
- KYIKRXIYLAGAKQ-UHFFFAOYSA-N abcn Chemical compound C1CCCCC1(C#N)N=NC1(C#N)CCCCC1 KYIKRXIYLAGAKQ-UHFFFAOYSA-N 0.000 claims description 3
- 238000007792 addition Methods 0.000 claims description 3
- 239000011541 reaction mixture Substances 0.000 claims description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 2
- 150000002432 hydroperoxides Chemical class 0.000 claims description 2
- 229910052708 sodium Inorganic materials 0.000 claims description 2
- 239000011734 sodium Substances 0.000 claims description 2
- 239000004342 Benzoyl peroxide Substances 0.000 claims 2
- OMPJBNCRMGITSC-UHFFFAOYSA-N Benzoylperoxide Chemical compound C=1C=CC=CC=1C(=O)OOC(=O)C1=CC=CC=C1 OMPJBNCRMGITSC-UHFFFAOYSA-N 0.000 claims 2
- 235000019400 benzoyl peroxide Nutrition 0.000 claims 2
- 238000010438 heat treatment Methods 0.000 claims 1
- LRDFRRGEGBBSRN-UHFFFAOYSA-N isobutyronitrile Chemical compound CC(C)C#N LRDFRRGEGBBSRN-UHFFFAOYSA-N 0.000 claims 1
- 239000000243 solution Substances 0.000 description 6
- 239000007864 aqueous solution Substances 0.000 description 5
- 238000002425 crystallisation Methods 0.000 description 5
- 230000008025 crystallization Effects 0.000 description 5
- RWGFKTVRMDUZSP-UHFFFAOYSA-N cumene Chemical compound CC(C)C1=CC=CC=C1 RWGFKTVRMDUZSP-UHFFFAOYSA-N 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- CXWXQJXEFPUFDZ-UHFFFAOYSA-N tetralin Chemical compound C1=CC=C2CCCCC2=C1 CXWXQJXEFPUFDZ-UHFFFAOYSA-N 0.000 description 3
- IKHGUXGNUITLKF-XPULMUKRSA-N acetaldehyde Chemical compound [14CH]([14CH3])=O IKHGUXGNUITLKF-XPULMUKRSA-N 0.000 description 2
- 239000002585 base Substances 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000005119 centrifugation Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 150000004679 hydroxides Chemical class 0.000 description 2
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 2
- 235000013379 molasses Nutrition 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- 150000001342 alkaline earth metals Chemical class 0.000 description 1
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 1
- 239000007900 aqueous suspension Substances 0.000 description 1
- 229910052788 barium Inorganic materials 0.000 description 1
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 1
- 239000004327 boric acid Substances 0.000 description 1
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- YQHLDYVWEZKEOX-UHFFFAOYSA-N cumene hydroperoxide Chemical compound OOC(C)(C)C1=CC=CC=C1 YQHLDYVWEZKEOX-UHFFFAOYSA-N 0.000 description 1
- 230000001934 delay Effects 0.000 description 1
- 230000008034 disappearance Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000002269 spontaneous effect Effects 0.000 description 1
- 150000003606 tin compounds Chemical class 0.000 description 1
- 238000004383 yellowing Methods 0.000 description 1
- 150000003752 zinc compounds Chemical class 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21D—WORKING OR PROCESSING OF SHEET METAL OR METAL TUBES, RODS OR PROFILES WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21D22/00—Shaping without cutting, by stamping, spinning, or deep-drawing
- B21D22/20—Deep-drawing
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Shaping Metal By Deep-Drawing, Or The Like (AREA)
- Press Drives And Press Lines (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US59214366A | 1966-11-04 | 1966-11-04 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| NO130928B true NO130928B (ru) | 1974-12-02 |
| NO130928C NO130928C (ru) | 1975-03-12 |
Family
ID=24369481
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO170356A NO130928C (ru) | 1966-11-04 | 1967-11-01 |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US3509785A (ru) |
| AT (1) | AT283854B (ru) |
| BE (1) | BE704780A (ru) |
| CH (1) | CH471608A (ru) |
| CS (1) | CS174104B2 (ru) |
| DE (1) | DE1299854B (ru) |
| ES (1) | ES347164A1 (ru) |
| GB (1) | GB1209930A (ru) |
| IL (1) | IL28859A (ru) |
| NL (1) | NL6714899A (ru) |
| NO (1) | NO130928C (ru) |
| SE (1) | SE316896B (ru) |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3668914A (en) * | 1969-12-31 | 1972-06-13 | Bogdan Vyacheslavovich Voitsek | Method of stamping metal convex articles from sheets |
| US3695087A (en) * | 1970-08-26 | 1972-10-03 | Arthur H Tuberman | Method and apparatus for pointing tubes |
| NO130553C (ru) * | 1973-01-25 | 1975-01-08 | Gunnar Vinje | |
| NL181914C (nl) * | 1977-07-05 | 1900-01-01 | Toyo Seikan Kaisha Ltd | Inrichting voor het vervaardigen van getrokken voorwerpen. |
| FR2448946A1 (fr) * | 1979-02-14 | 1980-09-12 | Cuq Pierre | Procede d'emboutissage, avec conformage centripete du flan |
| DE3042483A1 (de) * | 1980-11-11 | 1982-06-16 | Philips Patentverwaltung Gmbh, 2000 Hamburg | Verfahren und anordnung zur herstellung einer duesenplatte fuer tintenstrahlschreibwerke |
| US4644775A (en) * | 1985-06-14 | 1987-02-24 | Fuchs Jr Francis J | Shell forming apparatus and process |
| US5190770A (en) * | 1989-01-12 | 1993-03-02 | Rheon Automatic Machinery Co., Ltd. | Apparatus for cutting and shaping a spherical body |
| GB2240060B (en) * | 1990-01-18 | 1994-03-16 | Nam Lee Ind | Method of producing a main frame for a shipping container |
| JPH03285632A (ja) * | 1990-03-30 | 1991-12-16 | Rheon Autom Mach Co Ltd | 包被球断装置 |
| JP2916515B2 (ja) * | 1990-05-01 | 1999-07-05 | レオン自動機 株式会社 | 包被球断装置 |
| US5223277A (en) * | 1990-09-12 | 1993-06-29 | Rheon Automatic Machinery Co., Ltd. | Apparatus for cutting an enveloped body |
| US5406823A (en) * | 1991-01-18 | 1995-04-18 | Nam Lee Industries (Pte) Ltd. | Method of producing a main frame for a shipping container |
| US5295378A (en) * | 1992-08-05 | 1994-03-22 | Mark Industries | Method for making a precisely machined part |
| US7316150B1 (en) | 2006-11-07 | 2008-01-08 | Ford Motor Company | Impact reduction apparatus for stretch draw dies |
| CN101837407A (zh) * | 2010-04-15 | 2010-09-22 | 重庆理工大学 | 通过固体颗粒介质加径向推力的成形模具 |
| CN101869944A (zh) * | 2010-04-15 | 2010-10-27 | 重庆理工大学 | 通过固体颗粒介质加径向推力的可变形状凸模成形模具 |
| CN101862791A (zh) * | 2010-04-15 | 2010-10-20 | 重庆理工大学 | 带活动拉延筋加固体颗粒介质径向推力的成型模具 |
| US9848726B2 (en) * | 2013-09-16 | 2017-12-26 | Johnny Todd Harris | Vegetable peeler |
| CN106111814B (zh) * | 2016-08-09 | 2019-02-01 | 机械科学研究总院 | 拉延模具 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1530000A (en) * | 1924-03-27 | 1925-03-17 | John J Kauffman | Drawing die |
| US2847957A (en) * | 1955-12-20 | 1958-08-19 | Budd Co | Apparatus for rapidly forming deep draws in metal sheets |
| US3172928A (en) * | 1961-08-08 | 1965-03-09 | Raybestos Manhattan Inc | Method for deep forming fluorocarbon polymer sheet material |
| US3314275A (en) * | 1963-12-17 | 1967-04-18 | Mary E Mullen | Tooling for sheet material forming |
| US3303806A (en) * | 1965-05-17 | 1967-02-14 | Plastic Can Corp | Method for making metallic containers |
-
1966
- 1966-11-04 US US592143A patent/US3509785A/en not_active Expired - Lifetime
-
1967
- 1967-10-06 BE BE704780D patent/BE704780A/xx unknown
- 1967-10-28 DE DEP1704406.3A patent/DE1299854B/de active Pending
- 1967-10-30 IL IL28859A patent/IL28859A/en unknown
- 1967-10-31 AT AT985067A patent/AT283854B/de not_active IP Right Cessation
- 1967-10-31 GB GB49353/67A patent/GB1209930A/en not_active Expired
- 1967-11-01 NO NO170356A patent/NO130928C/no unknown
- 1967-11-02 CH CH1534767A patent/CH471608A/de not_active IP Right Cessation
- 1967-11-02 NL NL6714899A patent/NL6714899A/xx unknown
- 1967-11-03 SE SE15088/67A patent/SE316896B/xx unknown
- 1967-11-03 ES ES347164A patent/ES347164A1/es not_active Expired
- 1967-11-04 CS CS7829A patent/CS174104B2/cs unknown
Also Published As
| Publication number | Publication date |
|---|---|
| IL28859A (en) | 1971-04-28 |
| DE1299854B (de) | 1969-07-24 |
| SE316896B (ru) | 1969-11-03 |
| NL6714899A (ru) | 1968-05-06 |
| BE704780A (ru) | 1968-04-08 |
| AT283854B (de) | 1970-08-25 |
| CS174104B2 (ru) | 1977-03-31 |
| US3509785A (en) | 1970-05-05 |
| CH471608A (de) | 1969-04-30 |
| NO130928C (ru) | 1975-03-12 |
| ES347164A1 (es) | 1969-01-16 |
| GB1209930A (en) | 1970-10-21 |
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