NL2032363B1 - Spray drying method for preparing candidate of salt water reference material - Google Patents
Spray drying method for preparing candidate of salt water reference material Download PDFInfo
- Publication number
- NL2032363B1 NL2032363B1 NL2032363A NL2032363A NL2032363B1 NL 2032363 B1 NL2032363 B1 NL 2032363B1 NL 2032363 A NL2032363 A NL 2032363A NL 2032363 A NL2032363 A NL 2032363A NL 2032363 B1 NL2032363 B1 NL 2032363B1
- Authority
- NL
- Netherlands
- Prior art keywords
- spray dryer
- salt water
- spray
- turning
- sample
- Prior art date
Links
- 150000003839 salts Chemical class 0.000 title claims abstract description 27
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 25
- 238000000034 method Methods 0.000 title claims abstract description 17
- 239000012925 reference material Substances 0.000 title claims abstract description 13
- 238000001694 spray drying Methods 0.000 title claims abstract description 13
- 239000007921 spray Substances 0.000 claims abstract description 27
- 230000002572 peristaltic effect Effects 0.000 claims abstract description 6
- 238000004321 preservation Methods 0.000 claims abstract description 5
- 239000011521 glass Substances 0.000 claims abstract description 4
- 239000012528 membrane Substances 0.000 claims abstract description 4
- 239000010979 ruby Substances 0.000 claims abstract description 4
- 229910001750 ruby Inorganic materials 0.000 claims abstract description 4
- 238000007789 sealing Methods 0.000 claims abstract description 4
- 238000004140 cleaning Methods 0.000 claims abstract description 3
- 238000001914 filtration Methods 0.000 claims abstract description 3
- 230000006835 compression Effects 0.000 claims description 3
- 238000007906 compression Methods 0.000 claims description 3
- 239000000243 solution Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000002354 inductively-coupled plasma atomic emission spectroscopy Methods 0.000 description 1
- 229910052744 lithium Inorganic materials 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 229910052712 strontium Inorganic materials 0.000 description 1
- CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 description 1
- 238000004457 water analysis Methods 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N2001/2893—Preparing calibration standards
Landscapes
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
U I T T R E K S E L A spray drying method for preparing a candidate of a salt water reference material is provided, including the following steps: filtering salt water with a 25 um filter membrane, and accurately pipetting 50 nflJ of filtered salt water 11) a glass colorimetric 5 tube; turning on an air exhauster of a laboratory mini spray dryer, turning on a heater of the spray dryer, turning on a compressor and a peristaltic pump after the inlet temperature of the spray dryer reaches 125°C, and cleaning a nozzle, where outlet temperature of the spray dryer is 140°C when the inlet temperature 10 of the spray dryer reaches 125°C; drawing the filtered salt water sample into the spray dryer by using a ruby nozzle, and spray— drying the sample; and taking out the spray—dried, sample, and performing prompt sealing for preservation, to obtain a finished product. 15 (+ Fig. 1)
Description
P1443 /NLpd
SPRAY DRYING METHOD FOR PREPARING CANDIDATE OF SALT WATER
REFERENCE MATERIAL
The present disclosure belongs to the field of testing tech- nologies of geological experiments, and in particular, to a spray drying method for preparing a candidate of a salt water reference material.
A salt water reference material is prepared from natural salt water and used for monitoring and controlling in the process of salt water analysis. An existing process is sampling salt water and then performing sealed preservation. A salt water reference material prepared according to the existing process has poor sta- bility and is difficult to transport.
To overcome the above defects in the prior art, an objective of the present disclosure is to provide a spray drying method for preparing a candidate of a salt water reference material, which is easy to operate. A finished product prepared according to this method has high stability and is easy to preserve.
To achieve the above objective, the present disclosure adopts the following technical solution:
A spray drying method for preparing a candidate of a salt wa- ter reference material is provided, including the following steps: step 1: filtering salt water with a 25 um filter membrane, and accurately pipetting 50 mL of filtered salt water to a glass colorimetric tube; step 2: turning on an air exhauster of a laboratory mini spray dryer, setting power of the air exhauster to 90 3, setting inlet temperature of the spray dryer to 125°C, turning on a heater of the spray dryer, turning on a compressor and a peristaltic pump after the inlet temperature of the spray dryer reaches 125°C, and cleaning a drawing nozzle, where outlet temperature of the spray dryer is 140°C when the inlet temperature of the spray dryer reach- es 125°C; step 3: drawing the filtered salt water sample into the spray dryer by using a ruby drawing nozzle, and spray-drying the sample; and step 4: taking out the spray-dried sample, and performing prompt sealing for preservation, to obtain a finished product.
In step 2, a compression speed of the compressor is set to 400 L/h, and a working ratio of the peristaltic pump is set to 25%.
Compared with the prior art, in the present disclosure, a candidate of a salt water reference material is prepared by using the spray drying method, such that a process is easy to control, and a finished product is convenient to preserve.
FIG. 1 is a flowchart of a process according to the present disclosure.
The implementations of the present disclosure are described below in detail with reference to the accompanying drawings and examples.
A spray drying method for preparing a candidate of a salt wa- ter reference material is provided. Referring to FIG. 1, the meth- od includes the following steps:
Step 1: Filter salt water with a 25 pm filter membrane, and accurately pipette 50 mL of filtered salt water to a glass colori- metric tube.
Step 2: Turn on an air exhauster of a laboratory mini spray dryer, set power of the air exhauster to 90 %, set inlet tempera- ture of the spray dryer to 125°C, turn on a heater of the spray dryer, turn on a compressor (whose compression speed is set to 400
L/h) and a peristaltic pump (whose working ratio is set to 25%) after the inlet temperature of the spray dryer reaches 125°C, and clean a nozzle, where outlet temperature of the spray dryer is 140°C when the inlet temperature of the spray dryer reaches 125°C.
Step 3: Draw the filtered salt water sample into the spray dryer by using a ruby nozzle, and spray-dry the sample.
Step 4: Take out the spray-dried sample, and perform prompt sealing for preservation, to obtain a finished product.
Before use, the finished product of the candidate of the salt water reference material can be reduced to a twice diluted solu- tion of original salt water by opening a sealed packaging bag and quantitatively adding the finished product in 100 mL of distilled water for dissolution.
The following test data is obtained when the sample is de- tected according to an inductively coupled plasma atomic emission spectrometry and a volumetric method:
Concentration of lithium: 131 mg/mL
Concentration of strontium: 25 mg/mL.
Claims (2)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL2032363A NL2032363B1 (en) | 2022-07-04 | 2022-07-04 | Spray drying method for preparing candidate of salt water reference material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL2032363A NL2032363B1 (en) | 2022-07-04 | 2022-07-04 | Spray drying method for preparing candidate of salt water reference material |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| NL2032363B1 true NL2032363B1 (en) | 2024-01-19 |
Family
ID=89621196
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NL2032363A NL2032363B1 (en) | 2022-07-04 | 2022-07-04 | Spray drying method for preparing candidate of salt water reference material |
Country Status (1)
| Country | Link |
|---|---|
| NL (1) | NL2032363B1 (en) |
-
2022
- 2022-07-04 NL NL2032363A patent/NL2032363B1/en active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101324491B (en) | Smoking apparatus capable of implementing continuous one-time sampling of main fume gas phase object | |
| NL2032363B1 (en) | Spray drying method for preparing candidate of salt water reference material | |
| CN209878413U (en) | Atmospheric aerosol on-line trapping and chemical component detection device | |
| AU2020102406A4 (en) | Method for detecting pesticide residues in agricultural products | |
| US10976228B2 (en) | Extraction of materials from liquids | |
| CN103357268A (en) | Biochemical sample filtering system and filtering method | |
| US20200246755A1 (en) | Self-preserving biodegradable environmental dna filter | |
| CN203664304U (en) | Cuvette washing device | |
| CN104777018A (en) | Automatic pretreatment device for processing paralytic shellfish toxin samples | |
| CN207540870U (en) | A kind of automatic enriching apparatus in water sample scene | |
| CN108181151A (en) | Method for preparing brine standard substance candidate | |
| CN110501300A (en) | A kind of automobile exhaust gas checking apparatus and detection method | |
| CN108181150A (en) | Method for preparing potassium, sodium, calcium and magnesium element standard substance candidate in underground water | |
| CN210427152U (en) | Oil liquid pretreatment device for online oil quality analysis | |
| CN113804799A (en) | Pretreatment method and method for testing NMP content in lithium ion battery pole piece | |
| CN219848986U (en) | Ultrafiltration concentration and replacement device for liquid enzyme preparation | |
| CN111487094B (en) | SO in the flue gas is discharged 3 Detection pretreatment system and use method thereof | |
| CN207336192U (en) | A kind of vacuum concentrating apparatus for being used for 96 orifice plates | |
| CN112946057B (en) | Method for simultaneously detecting multiple volatile organic compounds in fermentation process | |
| CN209280694U (en) | A kind of milk melamine detection device | |
| CN208026525U (en) | A kind of fluid sample degassing system | |
| CN113740124A (en) | Gaseous organic amine collecting device and method thereof | |
| CN113295809A (en) | Analytical method for extracting ester compounds in white spirit based on pervaporation membrane | |
| CN208334313U (en) | A kind of Full-automatic pumping formula gas analyzing apparatus | |
| CN209085989U (en) | A kind of online sampling mechanism of alkyl chloride production |