MXPA05013640A - Metodo para la elaboracion de caprolactama. - Google Patents
Metodo para la elaboracion de caprolactama.Info
- Publication number
- MXPA05013640A MXPA05013640A MXPA05013640A MXPA05013640A MXPA05013640A MX PA05013640 A MXPA05013640 A MX PA05013640A MX PA05013640 A MXPA05013640 A MX PA05013640A MX PA05013640 A MXPA05013640 A MX PA05013640A MX PA05013640 A MXPA05013640 A MX PA05013640A
- Authority
- MX
- Mexico
- Prior art keywords
- caprolactam
- making
- tha
- making caprolactam
- aminocapronitrile
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D223/00—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom
- C07D223/02—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings
- C07D223/04—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings with only hydrogen atoms, halogen atoms, hydrocarbon or substituted hydrocarbon radicals, directly attached to ring carbon atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Other In-Based Heterocyclic Compounds (AREA)
Abstract
La presente invencion describe un metodo para elaborar caprolactama a partir de 6-aminocapronitrilo que contiene mas de 500 ppm de tetrahidroazepina y sus derivados (THA) en el que el amoniaco y el agua se remueven de la caprolactama cruda en una sola etapa de separacion y despues la THA se remueve del fundido de la caprolactama resultante.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/464,175 US6716977B1 (en) | 2003-06-17 | 2003-06-17 | Method for making caprolactam from impure ACN wherein ammonia and water are removed from crude caprolactam in a simple separation step and then THA is removed from the resulting caprolactam melt |
PCT/US2004/019432 WO2004113288A1 (en) | 2003-06-17 | 2004-06-17 | Method for making caprolactam |
Publications (1)
Publication Number | Publication Date |
---|---|
MXPA05013640A true MXPA05013640A (es) | 2006-02-24 |
Family
ID=32031044
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MXPA05013640A MXPA05013640A (es) | 2003-06-17 | 2004-06-17 | Metodo para la elaboracion de caprolactama. |
Country Status (8)
Country | Link |
---|---|
US (1) | US6716977B1 (es) |
EP (1) | EP1636178B1 (es) |
JP (1) | JP4961208B2 (es) |
CN (1) | CN100368396C (es) |
DE (1) | DE602004003818T2 (es) |
MX (1) | MXPA05013640A (es) |
TW (1) | TW200517372A (es) |
WO (1) | WO2004113288A1 (es) |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE10253095A1 (de) * | 2002-11-13 | 2004-06-17 | Basf Ag | Verfahren zur Reinigung von Caprolactam |
US7390897B2 (en) * | 2005-03-18 | 2008-06-24 | Invista North America S.A.R.L. | Method for making caprolactam from impure 6-aminocapronitrile |
US7060820B1 (en) * | 2005-03-18 | 2006-06-13 | Invista North America S.A.R.L. | Process for making caprolactam |
CN102875469B (zh) * | 2011-07-14 | 2015-01-14 | 中国石油化工股份有限公司 | 采用径向移动床反应器制备己内酰胺的方法 |
CN102875468A (zh) * | 2011-07-14 | 2013-01-16 | 中国石油化工股份有限公司 | 一种环己酮肟气相重排生产己内酰胺的方法 |
Family Cites Families (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2301964A (en) | 1941-09-12 | 1942-11-17 | Du Pont | Method of preparing lactams |
US2357484A (en) | 1941-09-12 | 1944-09-05 | Du Pont | Process for producing compounds containing an n-substituted amide group |
FR2729949A1 (fr) * | 1995-01-27 | 1996-08-02 | Rhone Poulenc Chimie | Procede de preparation de lactame |
DE19517823A1 (de) * | 1995-05-18 | 1996-11-21 | Basf Ag | Verfahren zur Herstellung von Caprolactam |
FR2735471B1 (fr) * | 1995-06-16 | 1997-08-22 | Rhone Poulenc Chimie | Procede de preparation de lactames |
FR2755132B1 (fr) | 1996-10-24 | 1998-11-27 | Rhone Poulenc Fibres | Procede de traitement de lactames |
DE19704613A1 (de) * | 1997-02-07 | 1998-08-13 | Basf Ag | Verfahren zur Abtrennung von 6-Aminocapronsäurenitril aus Mischungen, die 6-Aminocapronsäurenitril und ein Imin enthalten |
DE10029187A1 (de) * | 2000-06-19 | 2001-12-20 | Basf Ag | Verfahren zur Abtrennung von 6-Aminocapronitril aus Gemischen, die 6-Aminocapronitril, Adipodinitril und Hexamethylendiamin enthalten |
-
2003
- 2003-06-17 US US10/464,175 patent/US6716977B1/en not_active Expired - Lifetime
-
2004
- 2004-06-17 MX MXPA05013640A patent/MXPA05013640A/es active IP Right Grant
- 2004-06-17 WO PCT/US2004/019432 patent/WO2004113288A1/en active IP Right Grant
- 2004-06-17 CN CNB2004800169495A patent/CN100368396C/zh not_active Expired - Fee Related
- 2004-06-17 DE DE602004003818T patent/DE602004003818T2/de not_active Expired - Lifetime
- 2004-06-17 JP JP2006517364A patent/JP4961208B2/ja not_active Expired - Fee Related
- 2004-06-17 TW TW093117500A patent/TW200517372A/zh unknown
- 2004-06-17 EP EP04755552A patent/EP1636178B1/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
JP4961208B2 (ja) | 2012-06-27 |
DE602004003818D1 (de) | 2007-02-01 |
EP1636178B1 (en) | 2006-12-20 |
EP1636178A1 (en) | 2006-03-22 |
JP2007521271A (ja) | 2007-08-02 |
CN1809532A (zh) | 2006-07-26 |
WO2004113288A1 (en) | 2004-12-29 |
DE602004003818T2 (de) | 2007-10-11 |
US6716977B1 (en) | 2004-04-06 |
CN100368396C (zh) | 2008-02-13 |
TW200517372A (en) | 2005-06-01 |
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Legal Events
Date | Code | Title | Description |
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FG | Grant or registration |