MX2010011899A - Mixture and method for quantifying astaxanthin in residues of fermented shrimp using high-performance liquid chromatography (hplc). - Google Patents

Mixture and method for quantifying astaxanthin in residues of fermented shrimp using high-performance liquid chromatography (hplc).

Info

Publication number
MX2010011899A
MX2010011899A MX2010011899A MX2010011899A MX2010011899A MX 2010011899 A MX2010011899 A MX 2010011899A MX 2010011899 A MX2010011899 A MX 2010011899A MX 2010011899 A MX2010011899 A MX 2010011899A MX 2010011899 A MX2010011899 A MX 2010011899A
Authority
MX
Mexico
Prior art keywords
hplc
astaxanthin
quantifying
residues
mixture
Prior art date
Application number
MX2010011899A
Other languages
Spanish (es)
Inventor
Jaime Lopez Cervantes
Dalia Isabel Sanchez Machado
Karl Reiner Fick Rochin
Original Assignee
Bioderpac S A De C V
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bioderpac S A De C V filed Critical Bioderpac S A De C V
Priority to MX2010011899A priority Critical patent/MX2010011899A/en
Priority to PCT/MX2011/000015 priority patent/WO2012057596A1/en
Publication of MX2010011899A publication Critical patent/MX2010011899A/en

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/04—Preparation or injection of sample to be analysed
    • G01N30/06—Preparation
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L17/00—Food-from-the-sea products; Fish products; Fish meal; Fish-egg substitutes; Preparation or treatment thereof
    • A23L17/40—Shell-fish
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
    • A23L5/40—Colouring or decolouring of foods
    • A23L5/42—Addition of dyes or pigments, e.g. in combination with optical brighteners
    • A23L5/43—Addition of dyes or pigments, e.g. in combination with optical brighteners using naturally occurring organic dyes or pigments, their artificial duplicates or their derivatives
    • A23L5/44—Addition of dyes or pigments, e.g. in combination with optical brighteners using naturally occurring organic dyes or pigments, their artificial duplicates or their derivatives using carotenoids or xanthophylls
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/32—Bonded phase chromatography
    • B01D15/325—Reversed phase
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/04—Preparation or injection of sample to be analysed
    • G01N30/06—Preparation
    • G01N30/14—Preparation by elimination of some components
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P21/00—Preparation of peptides or proteins
    • C12P21/06—Preparation of peptides or proteins produced by the hydrolysis of a peptide bond, e.g. hydrolysate products
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/04—Preparation or injection of sample to be analysed
    • G01N30/06—Preparation
    • G01N2030/062—Preparation extracting sample from raw material
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/04—Preparation or injection of sample to be analysed
    • G01N30/06—Preparation
    • G01N2030/067—Preparation by reaction, e.g. derivatising the sample
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/04—Preparation or injection of sample to be analysed
    • G01N30/06—Preparation
    • G01N30/14—Preparation by elimination of some components
    • G01N2030/143—Preparation by elimination of some components selective absorption
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/04—Preparation or injection of sample to be analysed
    • G01N30/06—Preparation
    • G01N30/14—Preparation by elimination of some components
    • G01N2030/146—Preparation by elimination of some components using membranes
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/88—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86
    • G01N2030/8809—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample
    • G01N2030/8813—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample biological materials
    • G01N2030/8831—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample biological materials involving peptides or proteins
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/62—Detectors specially adapted therefor
    • G01N30/74—Optical detectors

Abstract

The present invention refers to a HPLC method for the quantification of astaxanthin derived from shrimp products. The method was used to quantify the amino acids present in the liquor obtained as final product in lactic fermentation. It was found that the linearity, precision and recovery of the method are suitable for the quantification of the amino acids selected, the analysed samples containing 20.40, 24.8 and 18.8 Ág/g of dry matter of alanine, valine and isoleucine, respectively.
MX2010011899A 2010-10-29 2010-10-29 Mixture and method for quantifying astaxanthin in residues of fermented shrimp using high-performance liquid chromatography (hplc). MX2010011899A (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
MX2010011899A MX2010011899A (en) 2010-10-29 2010-10-29 Mixture and method for quantifying astaxanthin in residues of fermented shrimp using high-performance liquid chromatography (hplc).
PCT/MX2011/000015 WO2012057596A1 (en) 2010-10-29 2011-02-04 Hplc method and mixture for quantifying astaxanthin in fermented shrimp waste

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
MX2010011899A MX2010011899A (en) 2010-10-29 2010-10-29 Mixture and method for quantifying astaxanthin in residues of fermented shrimp using high-performance liquid chromatography (hplc).

Publications (1)

Publication Number Publication Date
MX2010011899A true MX2010011899A (en) 2012-04-30

Family

ID=45994127

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2010011899A MX2010011899A (en) 2010-10-29 2010-10-29 Mixture and method for quantifying astaxanthin in residues of fermented shrimp using high-performance liquid chromatography (hplc).

Country Status (2)

Country Link
MX (1) MX2010011899A (en)
WO (1) WO2012057596A1 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109655422A (en) * 2018-10-30 2019-04-19 晨光生物科技集团股份有限公司 A kind of detection method of lycopene content

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103630626B (en) * 2013-11-27 2016-01-13 青岛旭能生物工程有限责任公司 A kind of extraction of thick-wall microalgae natural astaxanthin and content assaying method
CN105527362A (en) * 2015-12-17 2016-04-27 天津市天津医院 Analysis method of fingerprint spectrum of amino acids in granulation-promoting ointment
CN105695550B (en) * 2016-03-31 2019-12-17 广州元大生物科技发展有限公司 Method for producing astaxanthin by high-density culture of lactobacillus plantarum
CN106483241A (en) * 2016-10-28 2017-03-08 陕西科技大学 The Ultra Performance Liquid Chromatography level Four bar electrostatic field orbit ion trap mass spectrum screening method of pigment in wine
CN107102091B (en) * 2017-06-15 2020-11-13 秦皇岛惠恩生物技术有限公司 Method for quantitatively detecting astaxanthin in haematococcus pluvialis extract by using Asta-E-H lipase
CN110286179A (en) * 2019-08-08 2019-09-27 广西壮族自治区药用植物园 The quickly high performance liquid chromatography of detection Zeaxanthin cycle pigment
CN111346400A (en) * 2020-03-31 2020-06-30 河北医科大学 Liquid sample vortex differential centrifugal extraction device and extraction method
CN112946140B (en) * 2021-03-12 2023-03-21 广州市食品检验所（广州市酒类检测中心） Method for detecting water-soluble anion synthetic pigment in food
CN114487176B (en) * 2022-01-18 2023-06-16 大连海洋大学 Rapid screening method for dangerous substances in aquatic products

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2002000908A2 (en) * 2000-09-25 2002-01-03 Novozymes A/S Methods for processing crustacean material
MXPA02012838A (en) * 2002-12-19 2004-04-27 Univ Autonoma Metropolitana Enzymatic process for obtaining astaxanthin and protein from fermented shrimp residues.

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109655422A (en) * 2018-10-30 2019-04-19 晨光生物科技集团股份有限公司 A kind of detection method of lycopene content

Also Published As

Publication number Publication date
WO2012057596A1 (en) 2012-05-03

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