LT6185B - Recombined sterilized 3.5 percent milk and its production method - Google Patents

Abstract

The present invention relates to the production of dairy products, in particular to the production of recombined sterilized 3.5 percent fat milk. In the manufacture is used 10-45 percent of the natural skimmed milk, purified using the extremely small high-tech filters, to carry the process at low temperature in order to maintain undenatured proteins. Another component of the product - water, which is basis of chemical and microbiological processes of food, is also purified extremely by using the reverse osmosis method. By combining specially purified components can be obtained product having the desired properties. Advantage of this invention is that the skimmed milk has not been exposed higher than at 58 °C temperature and has preserved all milk constituents (undenatured proteins, vitamins, minerals, lactose), and combining with water and dry milk matter, allows to obtain high-quality milk product.

Description

The invention can be used in the dairy industry.

The presently known method of producing recombinant milk is described in Aloyz Gudonis' book "Dairy Product Technology", Vilnius, 2009. publishing house "Technology", section 6.13 "Technology for the production of regenerated milk".

Recombined milk is the milk product obtained by combining preserved milk fat and dry non-fat milk materials with the addition of water to obtain a milk product of appropriate composition. This method has the following disadvantages:

Using the technology described in Gudon's book, skimmed milk powder (or skimmed milk powder) is thickened in an evaporator and dried in a drying tower at temperatures between 80 and 120 ° C, which eliminates all vitamins and denaturates proteins.

Calcium salts are most affected by milk heating, and these changes are usually irreversible.

Calcium phosphate aggregates and precipitates in the form of colloidal calcium phosphate on casein powder. Such colloidal calcium phosphate blocks the active areas of the calcium micelle and prevents the rennet from attacking casein. Decreased ionic and molecular calcium levels in milk by 11-50% decrease the enzymatic properties of milk. Therefore, in the production of rennet cheeses and fermented products (yoghurts, yogurt products), soluble calcium salts (usually calcium chloride) are added to such milk to restore the salt balance.

The calcium phosphate portion of the heated milk settles on the surface of the heating unit and, together with the denatured whey proteins and other milk components, forms an insoluble precipitate (milk stone) .The composition of this precipitate (water 2.7-14%, protein 8-50%, fat 2-5 %, minerals 20-73%) depending on the composition of the milk being heated, the temperature and time of heating, the design of the unit and other factors.

Because of the disadvantages mentioned, the milk product produced in this way loses many good qualities and is not of sufficient quality.

Our invention-production method of recombinant dairy production technology allows to maintain the natural composition, taste and properties of dairy products.

This production method uses 10-40% natural skim milk, with special bacterial cleansing, low temperature, non-denatured proteins and other dry matter retained due to the special cleaning of skim milk from bacterial contamination and low pasteurization temperature.

The key idea behind this approach is that new nanotechnology is used to clean skim milk and the other ingredient of the product, water, from extremely inorganic impurities and bacteria.

The absorbed milk water is concentrated on the surface of the milk components (proteins, phospholipids, polysaccharides) in the colloidal state. Most of it consists of water attached to the hydrophilic groups of protein molecules. The most important hydrophilic groups of milk protein molecules are -NH2, -COOH, -OH, = NH, -CO-, - HS. Bound water accounts for 2.0 + 3.5% of total milk water. The aqueous medium is the basis of chemical and microbiological processes in food, and for this reason the water must be removed or combined, i.e. reduce the proportion of active water. Water forms a monomolecular layer on the inner surface of a foodstuff and is therefore immobile. As the amount of water in the food increases, the water accumulates in the microcapillary, where its mobility is limited. Still or immobile water is an unfavorable medium for chemical and enzymatic reactions. The mobility and absorption "a" of the water in the product determine the stability of the product. It is best when the value of "a" is between 0.2 and 0.4. In this case, chemical and enzymatic reactions are almost non-existent.

Applying this theory, mixing skim milk from 10 to 40%, and specially formulated membrane water, anhydrous milk fat, dry non-fat milk parts, we can produce many high quality recombinant milk products.

The advantage of these products is that skim milk has not been exposed to temperatures higher than 58 ° C and has retained all milk constituents (non-denatured proteins, vitamins, minerals, lactose) and by combining with water, milk solids that have retained adsorb water to obtain quality dairy products (drinking milk of different fat, yoghurts, fermented condensed milk products, etc.) Cow's milk delivered to the processing plant is processed in the usual way, which is chilled, stored, separated by separation of fat, skim milk and cream stored in intermediate containers.

Skim milk and water purification technology is outlined in Figures 1 and 2.

Skim milk cleaning technology is shown in Figure 1.

Skim milk is pumped into a heat exchanger 2 where it is heated to 45-48 ° C and sent to a bactofuge 3, then skimmed milk is pumped into a MF (microfiltration unit) 5 using filters: The system is designed to reduce bacterial levels using M / F (microfiltration) method. The system yields 5000-20000 dm ³ / h, the process temperature is 25-52 ° C, the filtrate is directed to pasteurisation 6 where it is maintained at 56.5-58.5 ° C until the alkaline phosphatase sample is negative, cooled in heat exchanger tanks 8 for further production.

System parameters:

System purpose (microfiltration) method

Machine model:

Productivity:

Performance of concentrate:

Permeate consumption: Working temperature: Filters used:

Filtering area: Number of concentration loops:

up to 4-6 ° C and accumulates in the intermediate bacteria reduction using the M / F industrial system

000-20,000 dm ³ / h.

-100-1 000dm ³ / hr.

-19,000-19,900 dm ³ / h.

25-52 ° C, ceramic, 1.1-1.6 microns permeability

25 to 52 m ²

2-4.

The water purification technology is shown in Figure 2.

Water pump (for feeding water from well or nets) - 1, Reverse osmosis filter - 2, Heat exchanger water pasteurizer - 3, Water intermediate storage tanks - 4.

Water purification using reverse osmosis. Reverse osmosis membranes have the narrowest pores and are therefore most selective. They trap all bacteria and viruses, most of the dissolved salts and organic matter (including iron and humus compounds, which give the water its color and pathogenic substances). Reverse osmosis membranes hold an average of 97-99% of all dissolved substances. Such membranes are used in many industries that require high quality water (water supply, alcohol and non-alcoholic beverages, food, pharmaceutical, electronics, etc.). Reverse osmosis membranes are widely used in the home: Reverse osmosis systems provide access to the cleanest water that meets sanitary rules and regulations and European drinking water quality standards.

Model

Filters Used Number of Filters Filter Area Industrial System Reverse Osmosis Spiral 7.9

10-16 from 565 m ² .

V // 16 E - 4 membrane tubes // 10-16 filters.

table

Minimum water quality requirements

Type of contamination Impact Concentration Dust (> 10u) Membrane abrasion 1 mg / l Suspension / colloids of consistent materials Contamination of membranes 1 mg / l Iron, magnesium in the form of colloids Contamination of membranes 0.01 mg / l Iron Oxidation, formation of suspensions of basic iron compounds causing membrane contamination <0.02 mg / l Hardness 1. Basic cleaning products and the effectiveness of synthetic detergents decrease. 2. Basic cleaning agents cause precipitation of salts that increase hardness, which causes membrane contamination. 3. Hardness-increasing salts and protein compounds are deposited with each other, increasing membrane contamination. 4. Buffer effect that increases the amount of basic cleaning agents needed to maintain an appropriate pH. 20 mg / l (CaCOs) Alkalinity Buffer to increase the amount of acidic agents needed to maintain an appropriate pH 100 mg / l

effect. Biological oxygen need Membrane contamination as the filtrate contains colloids and / or bulkycellular compounds. Decrease in chlorine activity (inefficiency). Nutrient medium for microorganisms. 100 mg / l Colloidal silicon dioxide Membrane abrasion. 0.01 mg / l Soluble silica Membrane fouling due to the precipitation of calcium metasilicate and magnesium silicate as well as the sodium salt of silicon-aluminum acid. 10 mg / l High bacterial colonies Membrane fouling due to plaques. 1000/1 ml Koli-titre Membrane fouling due to bacteria. 0/100 ml

table

Degree of water purification due to membrane filtration

Type of contamination Degree of purification Mechanical impurities / turbidity > 99% Inorganic substances Sodium 90-95% I Calcium 93-98% Magnesium 93-98% Iron 93-98% Manganese 93-98% Copper 93-98% Nickel 93-98% Zinc 93-98% Lead: 93-98% Chlorides 90-95% Nitrates 60-90% Phosphates 93-98% Sulphates 93-98% Cyanides 90-95% Organic matter i Organic molecules of a weight of> 200 to> 99% Organic molecules of up to 200 up to 99% in

Product: Recombined, sterilized 3.5% fat milk

Stabilizer for combining anhydrous milk fat and dry milk solids up to 0.15% Anhydrous milk fat up to 3.45% Non-fat milk concentrates: protein, minerals, lactose up to 8.6% Fat-free milk 10-45% Water filtrate 65-90%

The dry matter content of sterilized milk with a fat content of 3.5%

Anhydrous milk fat 3.45-3.5% Proteins 3.15-3.20% Non-fat milk concentrates: protein, minerals, lactose 8.50-8.60% Stabilizer for combining anhydrous milk fat and dry milk solids 0.14-0.15% Total dry matter 15.24-15.4%

Manufacturing Technology Process

Adding skimmed milk thickener and a stabilizer to bind anhydrous milk fat and dry milk to a mixture of water filtrate and skimmed milk at 35-60 ° C Dissolve the fat and add to the mixture, stirring At 40-75 ° C Homogenize at 197-210 kp / cm ² At 60-78 ° C Pasteurizing 14-17 sec., 75-82 ° C at temperature Chill to 4-5 ° C Hold until 5-7 or. Fill it into cans or bottles Sterilize by rotating the dishes at 110-138 ° C, 12-25 min. Cool the dishes to constant rotation 22-27 ° C Ripening at 4-5 ° C 6-8 or.

1. Recombined, sterilized milk with a fat content of 3.5%, obtained by mixing skimmed milk with water filtrate, characterized in that the reconstituted milk is made from specially purified milk and specially purified water.

Claims (6)

DEFINITION OF INVENTION 2. Recombined, sterilized 3.5% fat milk obtained by mixing skimmed milk with water filtrate according to claim 1, characterized in that the skimmed milk is pumped into a heat exchanger 2, where it is heated to 45 ° -48 ° C and directed to the bactofug. 3, further fed by pump 4 to a microfiltration unit 5 using ISOFLUX ceramic filters 6.9-8.9, 1.1-1.6 microns permeable at 48 ° C to 53 ° C, the filtrate is directed to a pasteurizer 6 where at 56 , 5-58.5 ° C is maintained until the alkaline phosphatase sample is negative, cooled in a heat exchanger at 7 to 4.0-6.0 ° C and stored in intermediate tanks, filters for further production with 5000-20000 dm ³ / h, concentrate throughput 100-1000 dm ³ / h, permeate consumption 19000-19900 dm ³ / h, operating temperature 25-52 ° C, ceramic filters with a throughput of 1.1-1.6 microns, filtration area 25 -52 m ² , concentration loops 2-4, filter amount of 10-16. 3. Recombined sterilized 3.5% fat milk obtained by mixing skimmed milk with water filtrate according to claim 1 or 2, characterized in that the water purification is performed by the reverse osmosis method using a spiral of 6.9-8.9, the number of filters being 10- 16, filtration area 565-1500 m ² , 2-6 membrane tubes. 4. Recombined, sterilized, 3.5% fat milk obtained by mixing skimmed milk with water filtrate according to claim 1, 2 or 3, characterized in that the admixture of the water filtrate and the skimmed milk mixture contains a non-fat milk thickener and a stabilizer for anhydrous milk fat and to combine the dry milk solids at 35-60 ° C, dissolve the fat and add to the mixture, stirring at 4075 ° C, homogenize at 197-210 kp / cm ^{2 at} 60-78 ° C, pasteurize for 14-17 sec. 75-82 ° C, cooled to 4-5 ° C, kept at 5-7 hrs, filling into cans or bottles, sterilized by rotating the dishes at 110 ° 138 ° C for 12-25 min, cooling the dishes with constant rotation to 22-27 ° C, maturing to 6-8 or. At 4-5 ° C. 5. Recombined sterilized milk with a fat content of 3,5%, obtained by mixing skimmed milk with water filtrate, characterized in that the product has the following composition: stabilizer for anhydrous milk fat and dry milk solids up to 0,15% anhydrous milk fat non-fat milk thick skimmed milk water filtrate up to 3,45% up to 8,6% 10-45% 65-90% dry matter content 3.5% fat sterilized milk anhydrous milk fat 3.45-3.5% protein 3.15-3.20% non-fat milk fat 8.50-8.60% stabilizer for anhydrous milk fat and 0.14-0.15% of dry matter to combine total solids