KR970026903A - Method for manufacturing activated carbon using waste paper and pulp residue - Google Patents

Method for manufacturing activated carbon using waste paper and pulp residue Download PDF

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Publication number
KR970026903A
KR970026903A KR1019950040517A KR19950040517A KR970026903A KR 970026903 A KR970026903 A KR 970026903A KR 1019950040517 A KR1019950040517 A KR 1019950040517A KR 19950040517 A KR19950040517 A KR 19950040517A KR 970026903 A KR970026903 A KR 970026903A
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KR
South Korea
Prior art keywords
activated carbon
waste paper
pulp residue
producing activated
inert atmosphere
Prior art date
Application number
KR1019950040517A
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Korean (ko)
Other versions
KR100286662B1 (en
Inventor
박양덕
Original Assignee
김종진
포항종합제철 주식회사
신창식
재단법인 산업과학기술연구소
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Publication date
Application filed by 김종진, 포항종합제철 주식회사, 신창식, 재단법인 산업과학기술연구소 filed Critical 김종진
Priority to KR1019950040517A priority Critical patent/KR100286662B1/en
Publication of KR970026903A publication Critical patent/KR970026903A/en
Application granted granted Critical
Publication of KR100286662B1 publication Critical patent/KR100286662B1/en

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    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/30Active carbon
    • C01B32/312Preparation
    • C01B32/318Preparation characterised by the starting materials
    • C01B32/324Preparation characterised by the starting materials from waste materials, e.g. tyres or spent sulfite pulp liquor
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/30Active carbon
    • C01B32/354After-treatment
    • C01B32/384Granulation
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/12Surface area

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Environmental & Geological Engineering (AREA)
  • Materials Engineering (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Paper (AREA)

Abstract

본 발명은 활성탄소의 제조방법에 관한 것으로, 펄프잔사 또는 파쇄폐지를 열경화성 고분자 수지와 혼합하여 경화시켜 탄소화하고 이를 다시 수산화칼륨과 혼합하고 불활성 분위기 하에서 적정온도 및 시간으로 활성화 처리하므로서, 수율 및 비표면적이 우수한 활성탄소의 제조방법을 제공하고자 하는데, 그 목적이 있다.The present invention relates to a method for producing activated carbon, wherein pulp residue or shredded paper is mixed with a thermosetting polymer resin, cured, carbonized, and then mixed with potassium hydroxide and activated at a proper temperature and time under an inert atmosphere, thereby yielding An object of the present invention is to provide a method for producing activated carbon having an excellent surface area.

상기한 목적을 달성하기 위한 본 발명은 파쇄폐지 및 펄프잔사를 원료로 사용하여 활성탄소를 제조하는 방법에 있어서, 단독 또는 복합의 파쇄폐지 및 펄프잔사와 열경화성 수지를 75 : 25 - 50 : 50의 중량비 범위로 혼합하고 충분히 경화시켜 성형체를 제조한 후 불활성 분위기하에서 500℃이상의 온도로 열처리하여 탄화물을 제조한 다음, 상기 제조된 탄화물과 수산화칼륨을 20 : 80 - 33 : 67의 중량비 범위로 혼합하여 불활성 분위기 하에서 500-900℃의 온도범위로 120분 이내에 열처리하는 것을 포함하여 이루어지는 폐지 및 펄프잔사를 이용한 활성탄소 제조방법에 관한 것을 그 요지로 한다.In order to achieve the above object, the present invention provides a method for producing activated carbon using shredded waste paper and pulp residue as raw materials, wherein the shredded waste paper and pulp residue and thermosetting resin of 75 or 25-50: 50 are used alone or in combination. After mixing in a weight ratio and sufficiently hardening to prepare a molded product, and heat treatment at a temperature of 500 ℃ or more in an inert atmosphere to prepare a carbide, then mixing the prepared carbide and potassium hydroxide in a weight ratio range of 20: 80-33: 67 The gist of the present invention relates to a method for producing activated carbon using waste paper and pulp residue comprising heat treatment within a temperature range of 500-900 ° C. within 120 minutes in an inert atmosphere.

Description

폐지 및 펄프잔사를 이용한 활성탄소 제조방법Method for manufacturing activated carbon using waste paper and pulp residue

본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음As this is a public information case, the full text was not included.

Claims (1)

파쇄폐지 및 펄프잔사를 원료로 사용하여 활성탄소를 제조하는 방법에 있어서, 단독 또는 복합의 파쇄폐지 및 펄프잔사와 열경화성 수지를 75 : 25 - 50 : 50의 중량비 범위로 혼합하고 충분히 경화시켜 성형체를 제조한 후 불활성 분위기하에 500℃이상의 온도로 열처리하여 탄화물을 제조한 다음, 상기 제조된 탄화물과 수산화칼륨을 20 : 80 - 33 : 67의 중량비 범위로 혼합하여 불활성 분위기 하에서 500-900℃ 온도 범위로 120분 이내에 열처리하는 것을 포함하여 이루어짐을 특징으로 하는 폐지 및 펄프잔사를 이용한 활성탄소 제조방법.In the method for producing activated carbon using shredded waste paper and pulp residue as raw materials, the shredded waste paper and pulp residue and thermosetting resin are mixed in a weight ratio of 75: 25-50: 50 and sufficiently cured to form a molded article. After the preparation, a carbide was prepared by heat treatment at a temperature of 500 ° C. or higher in an inert atmosphere, and then the carbide and potassium hydroxide were mixed in a weight ratio range of 20: 80-33: 67 to 500-900 ° C in an inert atmosphere. Method for producing activated carbon using waste paper and pulp residue, characterized in that it comprises a heat treatment within 120 minutes. ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.※ Note: The disclosure is based on the initial application.
KR1019950040517A 1995-11-09 1995-11-09 Method for manufacturing activated carbon by using waste paper and pulp residue KR100286662B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
KR1019950040517A KR100286662B1 (en) 1995-11-09 1995-11-09 Method for manufacturing activated carbon by using waste paper and pulp residue

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
KR1019950040517A KR100286662B1 (en) 1995-11-09 1995-11-09 Method for manufacturing activated carbon by using waste paper and pulp residue

Publications (2)

Publication Number Publication Date
KR970026903A true KR970026903A (en) 1997-06-24
KR100286662B1 KR100286662B1 (en) 2001-04-16

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ID=37514819

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KR1019950040517A KR100286662B1 (en) 1995-11-09 1995-11-09 Method for manufacturing activated carbon by using waste paper and pulp residue

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112624093A (en) * 2020-11-03 2021-04-09 中国科学技术大学 Method for preparing graphene on large scale and application

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5058761B2 (en) 2007-11-30 2012-10-24 富士フイルム株式会社 Method for producing activated carbon
CN111232950B (en) * 2020-03-13 2021-06-01 陕西科技大学 Method for preparing multifunctional elastic carbon material by carbonizing household paper

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0624865A (en) * 1992-07-02 1994-02-01 Tokai Carbon Co Ltd Production of porous active carbon molding

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112624093A (en) * 2020-11-03 2021-04-09 中国科学技术大学 Method for preparing graphene on large scale and application

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KR100286662B1 (en) 2001-04-16

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