KR940703898A - REMOVABLE ADHESIVE HAVING HIGH SHEAR AND LOW ADHESIVE TRANSFER - Google Patents

REMOVABLE ADHESIVE HAVING HIGH SHEAR AND LOW ADHESIVE TRANSFER

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Publication number
KR940703898A
KR940703898A KR1019940702471A KR19940702471A KR940703898A KR 940703898 A KR940703898 A KR 940703898A KR 1019940702471 A KR1019940702471 A KR 1019940702471A KR 19940702471 A KR19940702471 A KR 19940702471A KR 940703898 A KR940703898 A KR 940703898A
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South Korea
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weight
parts
component
adhesive
vinyl
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KR1019940702471A
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Korean (ko)
Inventor
스콧 티. 진켈
젠스 엘. 죠겐센
다니엘 씨. 슐트
Original Assignee
테릴 켄트 쿠알리
미네소타 마이닝 앤드 매뉴팩츄어링 컴패니
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Publication of KR940703898A publication Critical patent/KR940703898A/en

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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J4/00Adhesives based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; adhesives, based on monomers of macromolecular compounds of groups C09J183/00 - C09J183/16
    • C09J4/06Organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond in combination with a macromolecular compound other than an unsaturated polymer of groups C09J159/00 - C09J187/00
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F291/00Macromolecular compounds obtained by polymerising monomers on to macromolecular compounds according to more than one of the groups C08F251/00 - C08F289/00

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Adhesives Or Adhesive Processes (AREA)

Abstract

본 발명은, 하나이상의 불포화된 비닐 단량체와 하나의 유화제 단량체를 포함하는 제1성분; 탄성중합체 미소구를 포함하는 제2성분; 및 점착성 수지를 포함하는 제3성분을 포함하는 압감성 접착제에 관한 것이다.The present invention comprises a first component comprising at least one unsaturated vinyl monomer and one emulsifier monomer; A second component comprising elastomeric microspheres; And a third component including a tacky resin.

Description

고-전단성 및 저-접착제 전이율을 지닌 제거성 접착제(REMOVABLE ADHESIVE HAVING HIGH SHEAR AND LOW ADHESIVE TRANSFER)REMOVABLE ADHESIVE HAVING HIGH SHEAR AND LOW ADHESIVE TRANSFER

본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음Since this is an open matter, no full text was included.

Claims (25)

(a) 하나이상의 말단 불포화된 비닐 단량체 및 하나이상의 비닐, 불포화된 동종중합성 유화제 단량체로 구성된 제1성분, (b) 하나이상의 불용성, 자체 점착성, 탄성중합성, 중합체 미소구를 포함하는 제2성분, 및 (c) 높은 접착도 및 높은 정적 전단력을 지닌 수지를 포함하는 제3성분으로 구성되는 제거성 압감성 접착제.(a) a first component consisting of at least one terminal unsaturated vinyl monomer and at least one vinyl, unsaturated homopolymerizable emulsifier monomer, (b) a second comprising at least one insoluble, self-adhesive, elastomeric, polymeric microsphere And a component, and (c) a third component comprising a resin having high adhesion and high static shear force. 제1항에 있어서, 약 40중량부 내지 약 97중량부의 제1성분, 약 3중량부 내지 약 55중량부의 제2성분, 및 약 5중량부 내지 약 55중량부의 제3성분으로 구성되는 압감성 접착제.The pressure sensitive composition of claim 1 comprising about 40 parts by weight to about 97 parts by weight of a first component, about 3 parts by weight to about 55 parts by weight of a second component, and about 5 parts by weight to about 55 parts by weight of a third component. glue. 제1항에 있어서, 상기 제1성분이, 60 내지 100중량%가 비-t-알킬 아크릴레이트류 중에서 선택되고 상기 각 알킬 아크릴레이트는 단일 알킬쇄중의 탄소수의 절반이상을 가지며, 상기 알킬쇄의 평균길이는 4이상, 12 이하인, 95 내지 99.8중량부의 상기 말단 불포화된 비닐단량체; 및 친수성부와 소수성부를 모두 가지며 5개 이상, 40개 이하의 탄소원자를 포함하는 0.2 내지 5중량부의 상기 비닐-불포화된 동종중합성 유화제 단량체를 포함하는 접착제.The alkyl chain according to claim 1, wherein the first component is 60 to 100% by weight selected from non-t-alkyl acrylates, and each alkyl acrylate has at least half of the number of carbon atoms in a single alkyl chain, 95 to 99.8 parts by weight of the terminal unsaturated vinyl monomers, wherein an average length of 4 or more and 12 or less; And 0.2 to 5 parts by weight of said vinyl-unsaturated homopolymerizable emulsifier monomer having both hydrophilic and hydrophobic parts and containing at least 5 and at most 40 carbon atoms. 제1항에 있어서, 상기 제1성분이, 70 내지 100중량%가 비-t-알킬 아크릴레이트류 중에서 선택되고 상기 각 알킬 아크릴레이트는 단일 알킬쇄중의 탄소수의 절반이상을 가지며 상기 알킬쇄의 평균길이는 4 이상, 12 이하인, 88 내지 99중량부의 상기 말단 불포화된 비닐단량체; 및 친수성부와 소수성부를 모두 가지며 5개 이상, 40개 이하의 탄소원자를 포함하는 0.2 내지 5중량부의 상기 비닐-불포화된 동종중합성 유화체 단량체 ; 및 유리 라디칼 중합성 불포화기를 가진 0 내지 10중량부의 하나이상의 양이온성 단량체를 포함하는 접착제.The method according to claim 1, wherein the first component, 70 to 100% by weight is selected from non-t-alkyl acrylates, each alkyl acrylate having at least half of the number of carbon atoms in a single alkyl chain and An average length of 4 or more and 12 or less, 88 to 99 parts by weight of the terminal unsaturated vinyl monomer; And 0.2 to 5 parts by weight of the vinyl-unsaturated homopolymerizable emulsion monomer having both hydrophilic and hydrophobic parts and containing at least 5 and at most 40 carbon atoms; And 0-10 parts by weight of one or more cationic monomers having free radical polymerizable unsaturated groups. 제1항에 있어서, 상기 제3성분이, 유리전이온도가 약 -130℃ 내지 약 -90℃인 경성수지를 포함하는 접착제.The adhesive of claim 1 wherein the third component comprises a hard resin having a glass transition temperature of about -130 ° C to about -90 ° C. 제5항에 있어서, 상기 경성수지가 에폭시, 니트로셀룰로즈, 에틸렌 및 이들의 혼합물로 이루어진 군 중에서 선택되는 접착제.The adhesive according to claim 5, wherein the hard resin is selected from the group consisting of epoxy, nitrocellulose, ethylene and mixtures thereof. 제1항에 있어서, 상기 제3성분이 유리전이온도가 약 -89℃ 내지 약 130℃인 연성 수지를 포함하는 접착제.The adhesive of claim 1 wherein the third component comprises a flexible resin having a glass transition temperature of about -89 ° C to about 130 ° C. 제1항에 있어서, 상기 연성수지가 폴리올레핀, 폴리부틸렌, 폴리헥센, 폴리옥텐, 실리콘, 천연고무, 아크릴레이트, 메타크릴레이트, 비닐 아세테이트, 비닐 에테르 및 이들의 혼합물로 이루어진 군중에서 선택되는 접착제.The adhesive according to claim 1, wherein the soft resin is selected from the group consisting of polyolefin, polybutylene, polyhexene, polyoctene, silicone, natural rubber, acrylate, methacrylate, vinyl acetate, vinyl ether, and mixtures thereof. . 제1항에 있어서, 상기 제2성분이 공동의 불용성, 점착성, 탄성중합성 공중합체 미소구를 포함하는 접착제.The adhesive of claim 1 wherein the second component comprises a cavity insoluble, tacky, elastomeric copolymer microsphere. 제1항에 있어서, 상기 제2성분이 고형의, 불용성, 점착성, 탄성중합성 공중합체 미소구를 포함하는 접착제.The adhesive of claim 1 wherein the second component comprises a solid, insoluble, tacky, elastomeric copolymer microsphere. 제1항에 있어서, 상기 유화제 단량체가 스티렌 설포네이트의 1가염인 접착제.The adhesive of claim 1 wherein the emulsifier monomer is a monovalent salt of styrene sulfonate. 제1항에 있어서, 계면 활성제를 부가로 포함하는 접착제.The adhesive of claim 1 further comprising a surfactant. (a) 하나 이상의 말단 불포화된 비닐단량체 및 하나이상의 비닐, 불포화된 동종중합성 유화제 단량체로 구성된 제1성분, (b) 하나이상의 불용성, 자체 접착성, 탄성중합성, 중합체 미소구를 포함하는 제2성분, 및 (c) 높은 접착도 및 높은 전단력을 지닌 수지를 포함하는 제3성분으로 구성되는 압감성 접착제의 코팅이 기재의 한면 이상의 한부분 이상에 도포된 제품.(a) a first component comprising at least one terminal unsaturated vinyl monomer and at least one vinyl, unsaturated homopolymerizable emulsifier monomer, (b) at least one insoluble, self-adhesive, elastomeric, polymeric microsphere A product wherein a coating of a pressure sensitive adhesive consisting of a two component and (c) a third component comprising a resin having high adhesion and high shear is applied to at least one portion of one or more sides of the substrate. 제13항에 있어서, 상기 접착제가 약 40중량부 내지 약 97중량부의 제1성분, 약 3중량부 내지 약 55중량부의 제2성분, 및 약 5중량부 내지 약 55중량부의 제3성분으로 구성되는 제품.The method of claim 13, wherein the adhesive consists of about 40 parts by weight to about 97 parts by weight of a first component, about 3 parts by weight to about 55 parts by weight of a second component, and about 5 parts by weight to about 55 parts by weight of a third component Product. 제13항에 있어서, 상기 제1성분이, 60 내지 100중량%가 비-t-일킬 아크릴레이트류 중에서 선택되고 상기 각 알킬 아크릴레이트는 단일 알킬쇄중의 탄소수의 절반이상을 가지며, 상기 알킬쇄의 평균길이는 4개 이상, 12개 이하인, 95 내지 99.8중량부의 상기 말단 불포화된 비닐단량체; 및 친수성부와 소수성부를 모두 가지며 5개 이상, 40개 이하의 탄소원자를 포함하는 0.2 내지 5중량부의 상기 비닐-불포화된 동종중합성 유화제 단량체를 포함하는 제품.The method according to claim 13, wherein the first component, 60 to 100% by weight is selected from non-t-ylalkyl acrylates and each alkyl acrylate has at least half of the carbon number in a single alkyl chain, the alkyl chain An average length of 4 to 12 or less, 95 to 99.8 parts by weight of the terminal unsaturated vinyl monomer; And from 0.2 to 5 parts by weight of said vinyl-unsaturated homopolymerizable emulsifier monomer having both hydrophilic and hydrophobic parts and containing at least 5 and at most 40 carbon atoms. 제13항에 있어서, 상기 제1성분이, 70 내지 100중량%가 비-t-알킬 아크릴레이트류 중에서 선택되고 상기 각 알킬 아크릴레이트는 단일 알킬쇄중의 탄소수의 절반이상을 가지며, 상기 알킬쇄의 평균길이는 4개 이상, 12개 이하인, 88 내지 99중량부의 상기 말단 불포화된 비닐단량체; 친수성부와 소수성부를 모두 가지며 5개 이상, 40개 이항의 탄소원자를 포함하는 0.2 내지 5중량부의 하나이상의 비닐-불포화된 동종중합성 유화제 단량체; 및 유리 라디칼 중합성 불포화기를 가진 0 내지 10중량부의 하나이상의 양이온성 단량체를 포함하는 제품.14. The alkyl chain according to claim 13, wherein the first component is selected from the group consisting of 70 to 100% by weight of non-t-alkyl acrylates, and each alkyl acrylate has at least half of the number of carbon atoms in the single alkyl chain. The average length of the at least 4, 12 or less, 88 to 99 parts by weight of the terminal unsaturated vinyl monomer; 0.2 to 5 parts by weight of at least one vinyl-unsaturated homopolymerizable emulsifier monomer having both hydrophilic and hydrophobic parts and containing at least 5 and 40 binomial carbon atoms; And 0-10 parts by weight of one or more cationic monomers having free radical polymerizable unsaturated groups. 제13항에 있어서, 상기 제3성분이, 유리전이온도가 약 -130℃ 내지 약 -90℃인 경성수지를 포함하는 제품.The article of claim 13, wherein the third component comprises a hard resin having a glass transition temperature of about −130 ° C. to about −90 ° C. 15. 제16항에 있어서, 상기 경성수지가 에폭시, 니트로셀룰로즈, 에틸렌 및 이들의 혼합물로 이루어진 군중에서 선택되는 제품.17. The product of claim 16, wherein said hard resin is selected from the group consisting of epoxy, nitrocellulose, ethylene, and mixtures thereof. 제13항에 있어서, 상기 제3성분이, 유리전이온도가 약 -89℃ 내지 약 130℃인 연성수지를 포함하는 제품.The article of claim 13, wherein the third component comprises a flexible resin having a glass transition temperature of about −89 ° C. to about 130 ° C. 15. 제19항에 있어서, 상기 연성수지가 폴리올레핀, 폴리부틸렌, 폴리헥센, 폴리옥텐, 실리콘, 천연고무, 아크릴레이트, 메타크릴레이트, 비닐 아세테이트, 비닐 에테르 및 이들의 혼합물로 이루어진 군중에서 선택되는 제품.20. The product of claim 19, wherein the soft resin is selected from the group consisting of polyolefins, polybutylenes, polyhexenes, polyoctenes, silicones, natural rubbers, acrylates, methacrylates, vinyl acetates, vinyl ethers, and mixtures thereof. . 제13항에 있어서, 상기 제2성분이 공동의 불용성, 점착성, 탄성중합성 공중합체 미소구를 포함하는 제품.The article of claim 13, wherein said second component comprises a cavity insoluble, tacky, elastomeric copolymer microsphere. 제13항에 있어서, 상기 제2성분이 고형의 불용성, 점착성, 탄성중합성 공중합체 미소구를 포함하는 제품.The article of claim 13, wherein said second component comprises solid insoluble, tacky, elastomeric copolymer microspheres. 제13항에 있어서, 상기 유화제 단량체가 스티렌 설포네이트의 1가염인 제품.The product of claim 13, wherein said emulsifier monomer is a monovalent salt of styrene sulfonate. 제13항에 있어서, 상기 접착제 조성물에 첨가된 계면 활성제를 부가로 포함하는 제품.The article of claim 13, further comprising a surfactant added to the adhesive composition. 제13항에 있어서, 상기 기재의 상기 코팅부에 접착된 보호성 릴리이스 라이너(release liner)를 부가로 포함하는 제품.The article of claim 13, further comprising a protective release liner adhered to the coating of the substrate. ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.※ Note: The disclosure is based on the initial application.
KR1019940702471A 1992-01-21 1993-01-12 REMOVABLE ADHESIVE HAVING HIGH SHEAR AND LOW ADHESIVE TRANSFER KR940703898A (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US82325792A 1992-01-21 1992-01-21
US07/823,257 1992-01-21
PCT/US1993/000192 WO1993014171A1 (en) 1992-01-21 1993-01-12 Removable adhesive having high shear and low adhesive transfer

Publications (1)

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KR940703898A true KR940703898A (en) 1994-12-12

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EP (1) EP0623160A1 (en)
JP (1) JPH07503035A (en)
KR (1) KR940703898A (en)
AU (1) AU3441093A (en)
CA (1) CA2123878A1 (en)
HU (1) HUT68125A (en)
MX (1) MX9300257A (en)
WO (1) WO1993014171A1 (en)
ZA (1) ZA93200B (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3922464A (en) * 1972-05-26 1975-11-25 Minnesota Mining & Mfg Removable pressure-sensitive adhesive sheet material
US3857731A (en) * 1973-04-06 1974-12-31 Minnesota Mining & Mfg Acrylate microsphere-surfaced sheet material
US4243500A (en) * 1978-12-04 1981-01-06 International Coatings, Co., Inc. Pressure sensitive adhesives
US4629663A (en) * 1984-10-29 1986-12-16 Minnesota Mining And Manufacturing Company Removable pressure-sensitive adhesive tape
AU3313689A (en) * 1988-05-18 1989-11-23 Minnesota Mining And Manufacturing Company Tackified pressure sensitive adhesive

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HUT68125A (en) 1995-05-29
JPH07503035A (en) 1995-03-30
EP0623160A1 (en) 1994-11-09
WO1993014171A1 (en) 1993-07-22
MX9300257A (en) 1993-07-01
AU3441093A (en) 1993-08-03
CA2123878A1 (en) 1993-07-22
ZA93200B (en) 1994-07-12
HU9402138D0 (en) 1994-09-28

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