KR950701654A - Adhesive agent containing polysiloxane-grafted polymer and cosmetic compositions thereof - Google Patents

Adhesive agent containing polysiloxane-grafted polymer and cosmetic compositions thereof

Info

Publication number
KR950701654A
KR950701654A KR1019940704063A KR19940704063A KR950701654A KR 950701654 A KR950701654 A KR 950701654A KR 1019940704063 A KR1019940704063 A KR 1019940704063A KR 19940704063 A KR19940704063 A KR 19940704063A KR 950701654 A KR950701654 A KR 950701654A
Authority
KR
South Korea
Prior art keywords
polysiloxane
weight
monomer
vinyl
adhesive
Prior art date
Application number
KR1019940704063A
Other languages
Korean (ko)
Inventor
마트 토거슨 피터
토마스 발츄나스 앤토니
Original Assignee
제이코버스 코넬리스 레이서
더 프록터 앤드 갬블 캄파니
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to US88397492A priority Critical
Priority to US07/883,974 priority
Application filed by 제이코버스 코넬리스 레이서, 더 프록터 앤드 갬블 캄파니 filed Critical 제이코버스 코넬리스 레이서
Priority to PCT/US1993/004429 priority patent/WO1993023446A2/en
Publication of KR950701654A publication Critical patent/KR950701654A/en

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K8/00Cosmetics or similar toilet preparations
    • A61K8/18Cosmetics or similar toilet preparations characterised by the composition
    • A61K8/72Cosmetics or similar toilet preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toilet preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/895Polysiloxanes containing silicon bound to unsaturated aliphatic groups, e.g. vinyl dimethicone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILET PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILET PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/02Preparations for cleaning the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILET PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/06Preparations for styling the hair, e.g. by temporary shaping or colouring
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F290/00Macromolecular compounds obtained by polymerising monomers on to polymers modified by introduction of aliphatic unsaturated end or side groups
    • C08F290/08Macromolecular compounds obtained by polymerising monomers on to polymers modified by introduction of aliphatic unsaturated end or side groups on to polymers modified by introduction of unsaturated side groups
    • C08F290/14Polymers provided for in subclass C08G
    • C08F290/148Polysiloxanes
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIAL AS ADHESIVES
    • C09J155/00Adhesives based on homopolymers or copolymers, obtained by polymerisation reactions only involving carbon-to-carbon unsaturated bonds, not provided for in groups C09J123/00 - C09J153/00
    • C09J155/005Homopolymers or copolymers obtained by polymerisation of macromolecular compounds terminated by a carbon-to-carbon double bond
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIAL AS ADHESIVES
    • C09J4/00Adhesives based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; adhesives, based on monomers of macromolecular compounds of groups C09J183/00 - C09J183/16
    • C09J4/06Organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond in combination with a macromolecular compound other than an unsaturated polymer of groups C09J159/00 - C09J187/00
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILET PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/04Preparations for permanent waving or straightening the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILET PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/12Preparations containing hair conditioners

Abstract

(a) typically comprising a polysiloxane grafted polymer prepared by polymerizing a polysiloxane containing monomer and a polysiloxane free monomer by free radical polymerization; (b) has a weight average molecular weight of at least about 20,000 and contains about 1 to about 50 weight percent polysiloxane containing monomers; (c) about 15% by weight of the silicone grafted polymer and the unreacted polysiloxane containing monomer having a viscosity of less than about 10,000,000 centistokes at 25 ° C. based on the total silicone present as the unreacted silicone monomer and the polysiloxane grafted polymer. A polymeric adhesive of less than or equal to% is disclosed. The adhesive also contains up to about 4% by weight of polysiloxane grafted polymer and unreacted polysiloxane containing monomer having a viscosity of less than about 10,000,000 centistokes at 25 ° C. Also disclosed is a cosmetic composition containing the adhesive.

Description

ADHESIVE AGENT CONTAINING POLYSILOXANE-GRAFTED POLYMER AND CONSMETIC COMPOSITIONS THEREOF

Since this is an open matter, no full text was included.

Claims (12)

  1. Weight percent of silicone present as polysiloxane-grafted polymer and unreacted polysiloxane containing monomer at 25 ° C. based on total silicone present as polysiloxane-grafted polymer and unreacted polysiloxane containing monomer. Polysiloxane-grafted polymer and unreacted having a weight average molecular weight of 20,000 or more, containing 1 to 50% by weight of polysiloxane containing monomers, and having a viscosity of less than 10,000,000 centistokes at 25 ° C. A polymeric adhesive comprising a polysiloxane-grafted polymer prepared by polymerizing a polysiloxane containing monomer and a polysiloxane free monomer containing up to 4% by weight of a polysiloxane containing monomer.
  2. The polysiloxane-grafted polymer and unreacted polysiloxane containing polysiloxane-grafted polymer and unreacted polysiloxane-containing monomer according to claim 1 having a viscosity of less than 10,000,000 Celtiftock at 25 ° C. based on total silicone present. Less than or equal to 3% by weight of the polysiloxanes-grafted polymer and unreacted polysiloxanes containing monomers having a viscosity of 10% or less, preferably 5% or less, and having a viscosity of 25.00 C. less than 10,000,000 centistokes at 25 ° C. To 1% by weight or less.
  3. The adhesive according to claim 1 or 2, wherein the adhesive has a weight average molecular weight of at least 75,000, preferably at least 100,000, more preferably from 100,000 to 750,000.
  4. The polymer according to any one of claims 1 to 3, wherein the polymer contains 50 to 99% by weight of an ethylenically unsaturated polymerizable monomer based on the weight of the adhesive, and a polysiloxane having a molecular weight of 1,000 or more. Adhesives comprising from 1 to 50%, preferably from 2 to 25%, by weight of monomers:
    X (Y) n Si (R) 3-m (Z) m
    Wherein X is a vinyl group copolymerizable with the A and B monomers, Y is a divalent bonding group, R is hydrogen, hydroxy, lower alkyl, aryl, alkaryl, alkylamino or alkoxy and Z is 500 It is a monovalent siloxane polymeric moiety having a number average molecular weight or more, which is essentially non-reactive under copolymerization conditions, becomes a pendant of the vinyl polymeric main chain after polymerization, n is 0 or 1 and m is an integer of 1 to 3. .
  5. The adhesive of claim 4 wherein said polysiloxane free monomer is free radically polymerizable vinyl.
  6. Of claim 4 or claim 5, wherein the non-polysiloxane-containing monomers is C 1 -C 18 alcohol ester of acrylic acid or C 1 -C 18 alcohol esters of methacrylic acid, styrene, polystyrene macromer, vinyl acetate, vinyl chloride, Vinyl propionate, vinylidene chloride, alpha-methylstyrene, t-butylstyrene, butadiene, cyclohexadiene, ethylene propylene, vinyl toluene, acrylic acid, methacrylic acid, N, N-dimethylacrylamide, dimethyl aminoethyl methacryl Latex, quaternized dimethylaminoethyl methacrylate, methacrylamide, Nt-butyl-acrylamide, maleic acid, maleic anhydride, half ester of maleic anhydride, crotonic acid, ataconic acid, acrylamide, acrylate alcohol, Hydroxy ethyl methacrylate, diaryldimethyl ammonium chloride, vinyl pilolidone, vinyl ether, maleimide, vinyl pyridine Hydrophobic monomers selected from the group consisting of vinyl imidazole, styrene sulphonate, allyl alcohol, vinyl caprolactam, and mixtures thereof; And acrylic acid, methacrylic acid, N, N-dimethylacrylamide, dimethylaminoethyl methacrylate, quaternized dimethylaminoethyl methacrylate, methacrylamide, Nt-butyl acrylamide, maleic acid, maleic anhydride and their Half ester, crotonic acid, ataconic acid, acrylamide, acrylate alcohol, hydroxyethyl methacrylate, diallyldimethyl ammonium chloride, vinyl pyrrolidone, vinyl ether, maleimide, vinyl pyridine, vinyl imidazole, other polar vinyl Hydrophilicity selected from the group consisting of hydrophilic monomers selected from the group consisting of heterocyclic, styrene sulfonate, allyl alcohol, vinyl alcohol, vinyl caprolactam, salts of the acids and amines, and mixtures thereof.
  7. 7. Hydrophilic according to claim 6, wherein said hydrophobic monomer is selected from the group consisting of t-butyl acrylate, t-butyl methacrylate and mixtures thereof.
  8. The method according to claim 6 or 7, wherein the hydrophilic monomer is acrylic acid, NN-dimethylacrylamide, dimethylaminoethyl methacrylate, quaternized dimethylaminoethyl methacrylate, vinyl pyrrolidone, salts of the acid and amine, And an adhesive selected from the group consisting of mixtures thereof.
  9. 9 to 8% by weight of the hydrophobic monomer, 14 to 95% by weight of the hydrophilic monomer, and 1 to 40% by weight of the polysiloxane containing monomer, preferably 5 to 70% by weight. An adhesive comprising% of said hydrophobic monomer, 29 to 80% by weight of said hydrophilic monomer, and 2 to 25% by weight of said polysiloxane containing monomer.
  10. 9 to 8% by weight of the hydrophobic monomer, 20 to 80% by weight of the hydrophilic monomer, and 1 to 40% by weight of the polysiloxane containing monomer, preferably 5 to 70% by weight. An adhesive comprising% of said hydrophobic monomer, 29 to 60% by weight of said hydrophilic monomer, and 2 to 25% by weight of said polysiloxane containing monomer.
  11. A hair care composition useful for hair styling, comprising the adhesive of any one of claims 1 to 10 and a carrier suitable for adapting to hair.
  12. The hair protection composition of claim 11, wherein the carrier comprises water, C 1 -C 6 monohydric alcohols or mixtures thereof and is suitable for spray application to the hair.
    ※ Note: The disclosure is based on the initial application.
KR1019940704063A 1992-05-15 1993-05-11 Adhesive agent containing polysiloxane-grafted polymer and cosmetic compositions thereof KR950701654A (en)

Priority Applications (3)

Application Number Priority Date Filing Date Title
US88397492A true 1992-05-15 1992-05-15
US07/883,974 1992-05-15
PCT/US1993/004429 WO1993023446A2 (en) 1992-05-15 1993-05-11 Adhesive agent containing polysiloxane-grafted polymer, and cosmetic compositions thereof

Publications (1)

Publication Number Publication Date
KR950701654A true KR950701654A (en) 1995-04-28

Family

ID=25383698

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019940704063A KR950701654A (en) 1992-05-15 1993-05-11 Adhesive agent containing polysiloxane-grafted polymer and cosmetic compositions thereof

Country Status (17)

Country Link
EP (1) EP0640105A1 (en)
JP (1) JPH07508060A (en)
KR (1) KR950701654A (en)
CN (1) CN1081195A (en)
AU (1) AU677005B2 (en)
BR (1) BR9306363A (en)
CA (1) CA2135186A1 (en)
CZ (1) CZ277394A3 (en)
FI (1) FI945358A0 (en)
HU (1) HUT70074A (en)
MA (1) MA22892A1 (en)
MX (1) MX9302865A (en)
MY (1) MY131313A (en)
NO (1) NO944303L (en)
SK (1) SK136194A3 (en)
TR (1) TR28139A (en)
WO (1) WO1993023446A2 (en)

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