KR910011782A - Method for preparing monoolefin compound substituted with aminoalkyl - Google Patents

Method for preparing monoolefin compound substituted with aminoalkyl Download PDF

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Publication number
KR910011782A
KR910011782A KR1019890019966A KR890019966A KR910011782A KR 910011782 A KR910011782 A KR 910011782A KR 1019890019966 A KR1019890019966 A KR 1019890019966A KR 890019966 A KR890019966 A KR 890019966A KR 910011782 A KR910011782 A KR 910011782A
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South Korea
Prior art keywords
substituted
aminoalkyl
compound
group
alkali metal
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KR1019890019966A
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Korean (ko)
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KR930001338B1 (en
Inventor
박병욱
표성수
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이승동
주식회사 선경인더스트리
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Priority to KR1019890019966A priority Critical patent/KR930001338B1/en
Publication of KR910011782A publication Critical patent/KR910011782A/en
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Publication of KR930001338B1 publication Critical patent/KR930001338B1/en

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/44—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers
    • C07C209/48—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers by reduction of nitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/82—Purification; Separation; Stabilisation; Use of additives
    • C07C209/90—Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00—Compounds containing amino groups bound to a carbon skeleton
    • C07C211/01—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms
    • C07C211/25—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms of an unsaturated carbon skeleton containing rings other than six-membered aromatic rings

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

내용 없음No content

Description

아미노알킬로 치환된 모노올레핀화합물의 제조방법Method for preparing monoolefin compound substituted with aminoalkyl

본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음As this is a public information case, the full text was not included.

Claims (6)

방향족화합물 또는 관능기가 치환된 방향족화합물로 부터 아미노알킬 치환된 모노올레핀 화합물을 제조함에 있어서, 다음일반식(Ⅱ)로 표시되는 화합물과 다음 일반식(Ⅲ)으로 표시되는 화합물에다 알카리금속 및 디아민화합물을 반응시켜서 다음 일반식(I)로 표시되는 아미노알킬로 치환된 모노올레핀화합물을 제조하는 방법.In preparing an aminoalkyl substituted monoolefin compound from an aromatic compound or an aromatic compound substituted with a functional group, an alkali metal and a diamine compound in the compound represented by the following general formula (II) and the compound represented by the following general formula (III) Reacting to prepare a monoolefin compound substituted with aminoalkyl represented by the following general formula (I). 상기 식들중에서, A는 아미노알킬로 치환된 탄소원자수가 5~10개인 사이클로 알켄 탄화수소기를 나타내고, A1은 아미노알킬로 치환된 탄소원자수가 5~10개인 방향족 탄화수소기를 나타내며, X는 알킬기에 치환된 관능기로서 알카리금속에 의해서 환원이 되지 않는 아민기를 나타내거나 혹은 환원이 가능한 관능기인 니트릴기를 나타내며, A2는 알카리금속에 의해서 환원이 가능한 관능기가 치환된 탄소원자수가 5~10개인 사이클로 알켄 탄화수소기를 나타내며, Y는 알킬기에 치환된 알카리금속에 의해서 환윈이 가능한 관능기를 나타내며, n은 1~3의 정수를 나타낸다.In the above formulas, A represents a cycloalkene hydrocarbon group having 5 to 10 carbon atoms substituted with aminoalkyl, A 1 represents an aromatic hydrocarbon group having 5 to 10 carbon atoms substituted with aminoalkyl, and X is substituted with an alkyl group A functional group represents an amine group which is not reduced by an alkali metal or a nitrile group which is a functional group that can be reduced, and A 2 represents a cycloalkene hydrocarbon group having 5 to 10 carbon atoms in which a functional group capable of reduction by an alkali metal is substituted. And Y represent the functional group which can be ringed by the alkali metal substituted by the alkyl group, n represents the integer of 1-3. 제1항에 있어서, 상기 알카리금속으로는 리튬, 나트륨 및 프테슘중에서 선택된 어느하나를 사용하는 것을 특징으로 하는 아미노알킬로 치환된 모노올레핀화합물의 제조방법.The method of claim 1, wherein the alkali metal is any one selected from lithium, sodium, and potassium. 제1항에 있어서, 상기 디아민화합물로 에틸렌디아민 또는 프로필렌디아민을 사용하는 것을 특징으로 하는 아미노알킬로 치환된 모노올레핀화합물을 제조방법.The method for producing an aminoalkyl substituted monoolefin compound according to claim 1, wherein ethylenediamine or propylenediamine is used as the diamine compound. 제1항에 있어서, 상기 반응은 40℃~160℃에서 수행하는 것을 특징으로 하는 아미노알킬로 치환된 모노올레핀화합물을 제조방법.According to claim 1, wherein the reaction is a method for producing an aminoalkyl substituted monoolefin compound, characterized in that performed at 40 ℃ ~ 160 ℃. 제1항 또는 제4항에 있어서, 상기 반응은 메탄올, 에탄올, 프로판올, 부탄올 및 펜탄올중에서 선택된 저급알코올 존재하에 수행하는 것을 특징으로 하는 아미노알킬로 치환된 모노올레핀화합물을 제조방법.The method of claim 1 or 4, wherein the reaction is performed in the presence of a lower alcohol selected from methanol, ethanol, propanol, butanol and pentanol. 제1항에 있어서, 상기 일반식(Ⅲ)에서 Y는 니트릴기인 것을 특징으로 하는 아미노알킬로 치환된 모노올레핀화합물을 제조방법.The method for producing an aminoalkyl substituted monoolefin compound according to claim 1, wherein Y in the general formula (III) is a nitrile group. ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.※ Note: The disclosure is based on the initial application.
KR1019890019966A 1989-12-28 1989-12-28 Process for the preparation of substituted mono olefin compound by amino alkyl KR930001338B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
KR1019890019966A KR930001338B1 (en) 1989-12-28 1989-12-28 Process for the preparation of substituted mono olefin compound by amino alkyl

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
KR1019890019966A KR930001338B1 (en) 1989-12-28 1989-12-28 Process for the preparation of substituted mono olefin compound by amino alkyl

Publications (2)

Publication Number Publication Date
KR910011782A true KR910011782A (en) 1991-08-07
KR930001338B1 KR930001338B1 (en) 1993-02-26

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KR1019890019966A KR930001338B1 (en) 1989-12-28 1989-12-28 Process for the preparation of substituted mono olefin compound by amino alkyl

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