KR870003052A - 3'-브로모디페닐 에테르의 제조방법 - Google Patents
3'-브로모디페닐 에테르의 제조방법 Download PDFInfo
- Publication number
- KR870003052A KR870003052A KR1019860002244A KR860002244A KR870003052A KR 870003052 A KR870003052 A KR 870003052A KR 1019860002244 A KR1019860002244 A KR 1019860002244A KR 860002244 A KR860002244 A KR 860002244A KR 870003052 A KR870003052 A KR 870003052A
- Authority
- KR
- South Korea
- Prior art keywords
- diacyl peroxide
- diphenyl ether
- radicals
- equivalents
- equivalent
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C205/00—Compounds containing nitro groups bound to a carbon skeleton
- C07C205/27—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by etherified hydroxy groups
- C07C205/35—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by etherified hydroxy groups having nitro groups and etherified hydroxy groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton
- C07C205/36—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by etherified hydroxy groups having nitro groups and etherified hydroxy groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton to carbon atoms of the same non-condensed six-membered aromatic ring or to carbon atoms of six-membered aromatic rings being part of the same condensed ring system
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/06—Preparation of nitro compounds
- C07C201/12—Preparation of nitro compounds by reactions not involving the formation of nitro groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (10)
- 대기압정도의 불활성 기권하 극성 반양자성 용매내에서 광을 조사하거나 또는 조사함이 없이 일반식(Ⅱ)의 디페닐에테르를 일반식(Ⅲ)의 디아실 퍼옥시드 및 분자브롬(Br2)과 함께 65-150℃의 온도에서 반응시킴을 특징으로 하는, 2-클로로-4-트리 플루오로메틸-3'-브로드-4'-니트로디페닐 에테르의 제조방법.식중, R1은 알카리금속 또는 알카리토류금속이고,R2및 R3는 각각 알리파틱라디칼, 아로카틱라디칼 또는 알킬아로마틱라디칼임.
- 제1항에 있어서, 일반식(Ⅱ)의 디페닐에테르 1당량당 1-5당량의 일반식(Ⅲ)의 디아실 퍼옥시드를 반응시킴을 특징으로 하는 제조방법.식중, R1은 알카리금속 또는 알카리토류금속이고,R2및 R3는 각각 알리파틱라디칼, 아로마틱라디칼 또는 알킬아로마틱라디칼임.
- 제2항에 있어서, 상기 디페닐에테르 1당량당 3당량의 디아실 퍼옥시드를 반응시킴을 특징으로 하는 제조방법.
- 제2항에 있어서, 디아실 퍼옥시드가 디아로마틱 디아실 퍼옥시드임을 특징으로 하는 제조방법.
- 제4항에 있어서, 디아실 퍼옥시드가 디벤조일 퍼옥시드임을 특징으로 하는 제조방법.
- 제1항에 있어서, 일반식(Ⅱ)의 디페닐에테르 1당량당 1-5당량의 브롬(Br2)를 반응시킴을 특징으로 하는 제조방법.식중, R1은 알칼리금속 또는 알카리토류금속임.
- 제6항에 있어서, 상기 디페닐에테르 1당량당 2당량의 브롬(Br2)을 반응시킴을 특징으로 하는 제조방법.
- 제1항에 있어서, 반응온도가 75-110℃임을 특징으로 하는 제조방법.
- 제1항에 있어서, 조사되는 광의 세기가 25와트 이상임을 특징으로 하는 제조방법.
- 제9항에 있어서, 조사되는 광의 세기가 75와트 이상임을 특징으로 하는 제조방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US776,350 | 1985-09-16 | ||
US06/776,350 US4588487A (en) | 1985-09-16 | 1985-09-16 | Process for the preparation of 3'-halodiphenylethers |
Publications (2)
Publication Number | Publication Date |
---|---|
KR870003052A true KR870003052A (ko) | 1987-04-14 |
KR940005912B1 KR940005912B1 (ko) | 1994-06-24 |
Family
ID=25107144
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019860002244A KR940005912B1 (ko) | 1985-09-16 | 1986-03-26 | 3'-브로모디페닐에테르의 제조방법 |
Country Status (8)
Country | Link |
---|---|
US (1) | US4588487A (ko) |
EP (1) | EP0218314B1 (ko) |
JP (1) | JPS6267050A (ko) |
KR (1) | KR940005912B1 (ko) |
AT (1) | ATE54134T1 (ko) |
AU (1) | AU587026B2 (ko) |
CA (1) | CA1260016A (ko) |
DE (1) | DE3672246D1 (ko) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4594133A (en) * | 1985-09-16 | 1986-06-10 | Rohm And Haas Company | Process for preparing 3'-halodiphenylethers |
JP4774763B2 (ja) * | 2004-03-25 | 2011-09-14 | 住友化学株式会社 | 精製酢酸3−メチル−2−ブテニルの製造方法 |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3966453A (en) * | 1972-01-27 | 1976-06-29 | Ishihara Sangyo Kaisha Ltd. | Herbicidal 2-halo-4-trifluoromethyl-4'-cyanophenyl-ethers |
US3950435A (en) * | 1972-01-27 | 1976-04-13 | Ishihara Sangyo Kaisha Ltd. | Herbicidal diphenyl ethers |
US4046798A (en) * | 1973-02-12 | 1977-09-06 | Rohm And Haas Company | Herbicidal 4-trifluoromethyl-4'nitrodiphenyl ethers |
US4093446A (en) * | 1972-03-14 | 1978-06-06 | Rohm And Haas Company | Herbicidal 4-trifluoromethyl-4-nitrodiphenyl ethers |
CA1079303A (en) * | 1973-02-12 | 1980-06-10 | Horst O. Bayer | Herbicidal 4-trifluoromethyl-4'-nitrodiphenyl ethers |
US4485254A (en) * | 1978-08-04 | 1984-11-27 | Rohm And Haas Company | Process for preparing phenoxybenzoic acids |
US4358308A (en) * | 1981-10-19 | 1982-11-09 | Rohm And Haas Company | Herbicidal 4-perfluoroacetyl-, 4-perfluoromethylthio-, 4-perfluoromethylsulfinyl-, and 4-perfluoromethylsulfonyl-4'-nitrodiphenyl ethers |
US4419124A (en) * | 1981-10-19 | 1983-12-06 | Rohm And Haas Company | Herbicidal 4-trifluoromethyl-3'-nitrogen-substituted-4'-substituted diphenyl ethers |
US4594133A (en) * | 1985-09-16 | 1986-06-10 | Rohm And Haas Company | Process for preparing 3'-halodiphenylethers |
-
1985
- 1985-09-16 US US06/776,350 patent/US4588487A/en not_active Expired - Fee Related
-
1986
- 1986-03-17 CA CA000504272A patent/CA1260016A/en not_active Expired
- 1986-03-26 KR KR1019860002244A patent/KR940005912B1/ko active IP Right Grant
- 1986-04-18 DE DE8686302904T patent/DE3672246D1/de not_active Expired - Fee Related
- 1986-04-18 EP EP86302904A patent/EP0218314B1/en not_active Expired - Lifetime
- 1986-04-18 AT AT86302904T patent/ATE54134T1/de not_active IP Right Cessation
- 1986-04-23 AU AU56513/86A patent/AU587026B2/en not_active Ceased
- 1986-05-07 JP JP61103253A patent/JPS6267050A/ja active Pending
Also Published As
Publication number | Publication date |
---|---|
KR940005912B1 (ko) | 1994-06-24 |
JPS6267050A (ja) | 1987-03-26 |
ATE54134T1 (de) | 1990-07-15 |
AU587026B2 (en) | 1989-08-03 |
DE3672246D1 (de) | 1990-08-02 |
CA1260016A (en) | 1989-09-26 |
EP0218314B1 (en) | 1990-06-27 |
EP0218314A1 (en) | 1987-04-15 |
AU5651386A (en) | 1987-03-19 |
US4588487A (en) | 1986-05-13 |
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A201 | Request for examination | ||
G160 | Decision to publish patent application | ||
E701 | Decision to grant or registration of patent right | ||
NORF | Unpaid initial registration fee |