KR870002112A - 벤조티아졸 술펜 아미드의 제조방법 - Google Patents
벤조티아졸 술펜 아미드의 제조방법 Download PDFInfo
- Publication number
- KR870002112A KR870002112A KR1019850005935A KR850005935A KR870002112A KR 870002112 A KR870002112 A KR 870002112A KR 1019850005935 A KR1019850005935 A KR 1019850005935A KR 850005935 A KR850005935 A KR 850005935A KR 870002112 A KR870002112 A KR 870002112A
- Authority
- KR
- South Korea
- Prior art keywords
- amine
- benzothiazole sulfenamide
- aqueous alkali
- added
- water
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D277/00—Heterocyclic compounds containing 1,3-thiazole or hydrogenated 1,3-thiazole rings
- C07D277/60—Heterocyclic compounds containing 1,3-thiazole or hydrogenated 1,3-thiazole rings condensed with carbocyclic rings or ring systems
- C07D277/62—Benzothiazoles
- C07D277/68—Benzothiazoles with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached in position 2
- C07D277/82—Nitrogen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D277/00—Heterocyclic compounds containing 1,3-thiazole or hydrogenated 1,3-thiazole rings
- C07D277/60—Heterocyclic compounds containing 1,3-thiazole or hydrogenated 1,3-thiazole rings condensed with carbocyclic rings or ring systems
- C07D277/62—Benzothiazoles
- C07D277/68—Benzothiazoles with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached in position 2
- C07D277/70—Sulfur atoms
- C07D277/76—Sulfur atoms attached to a second hetero atom
- C07D277/80—Sulfur atoms attached to a second hetero atom to a nitrogen atom
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Thiazole And Isothizaole Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Cosmetics (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (3)
- 아민 또는 아민용액을 물중에 넣고 디벤조티아졸일 디술파이드 및 수성알칼리를 분리저장용기로부터 동시에 첨가함을 특징으로 하여, 산화제의 부제하에서 그리고 수성알칼리의 존재하에서 디벤조티아졸일 디술파이드와 수용성 아민으로부터 벤조티아졸 술펜 아미드를 제조하는 방법.
- 제1항에 있어서, 수성 알칼리를 pH가 10내지 13, 바람직하게는 11내지 12의 값으로 조정되도록 첨가하며 반응을 0내지 80℃, 바람직하게는 20내지 60℃에서 수행함을 특징으로 하는 방법.
- 제1항에 있어서, 아민으로서 3급-부틸아민, 시클로헥실 아민, 이소프로필 아민 또는 모르폴린을 첨가함을 특징으로 하는 방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19843430435 DE3430435A1 (de) | 1984-08-18 | 1984-08-18 | Verfahren zur herstellung von benzothiazolylsulfenamiden |
| DEP3430435.5 | 1984-08-18 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR870002112A true KR870002112A (ko) | 1987-03-30 |
| KR920001765B1 KR920001765B1 (ko) | 1992-03-02 |
Family
ID=6243360
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1019850005935A KR920001765B1 (ko) | 1984-08-18 | 1985-08-17 | 벤조티아졸 술펜 아미드의 제조방법 |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US4801707A (ko) |
| EP (1) | EP0173871B1 (ko) |
| JP (1) | JPS6157566A (ko) |
| KR (1) | KR920001765B1 (ko) |
| BR (1) | BR8503906A (ko) |
| DE (2) | DE3430435A1 (ko) |
| ES (1) | ES8606311A1 (ko) |
| IN (1) | IN160763B (ko) |
| ZA (1) | ZA856225B (ko) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3517084A1 (de) * | 1985-05-11 | 1986-11-13 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung von benzothiazolsulfenamiden |
| CN105503772A (zh) * | 2014-09-25 | 2016-04-20 | 中国石油化工股份有限公司 | 一种n－叔丁基苯并噻唑次磺酰胺制备方法 |
| CN106316981A (zh) * | 2015-06-19 | 2017-01-11 | 中国石油化工股份有限公司 | 一种n-环己基-2-苯并噻唑次磺酰胺制备方法 |
| CN112625003B (zh) * | 2020-12-30 | 2023-11-28 | 蔚林新材料科技股份有限公司 | N-环己基-2-苯并噻唑次磺酰胺及其合成工艺 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1695533C3 (de) * | 1967-05-19 | 1974-02-07 | Monsanto Co., St. Louis, Mo. (V.St.A.) | Verfahren zur Herstellung von 2-Benzothiazolsulfenamiden |
| FR2206761A5 (ko) * | 1972-11-13 | 1974-06-07 | Rhone Poulenc Sa | |
| US4182873A (en) * | 1972-10-04 | 1980-01-08 | Rhone-Poulenc S.A. | Process for the preparation of thiazolesulphenamides |
| JPS5344563A (en) * | 1976-10-05 | 1978-04-21 | Ouchi Shinkou Kagaku Kougiyou | Preparation of benzothiazolylsulfenamide |
| DE2815964A1 (de) * | 1978-04-13 | 1979-10-18 | Bayer Ag | Verfahren zur herstellung von benzthiazolylsulfensaeuremorpholid |
| DE3325724A1 (de) * | 1983-07-16 | 1985-01-24 | Akzo Gmbh, 5600 Wuppertal | Verfahren zur herstellung von thiazolyl-2-sulfenamiden |
-
1984
- 1984-08-18 DE DE19843430435 patent/DE3430435A1/de not_active Withdrawn
-
1985
- 1985-07-16 IN IN555/DEL/85A patent/IN160763B/en unknown
- 1985-08-05 EP EP85109812A patent/EP0173871B1/de not_active Expired
- 1985-08-05 DE DE8585109812T patent/DE3566256D1/de not_active Expired
- 1985-08-14 JP JP60177770A patent/JPS6157566A/ja active Pending
- 1985-08-16 BR BR8503906A patent/BR8503906A/pt unknown
- 1985-08-16 ES ES546192A patent/ES8606311A1/es not_active Expired
- 1985-08-16 ZA ZA856225A patent/ZA856225B/xx unknown
- 1985-08-17 KR KR1019850005935A patent/KR920001765B1/ko active IP Right Grant
-
1986
- 1986-12-24 US US06/946,695 patent/US4801707A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| ZA856225B (en) | 1986-04-30 |
| ES546192A0 (es) | 1986-04-01 |
| JPS6157566A (ja) | 1986-03-24 |
| EP0173871A1 (de) | 1986-03-12 |
| BR8503906A (pt) | 1986-05-27 |
| IN160763B (ko) | 1987-08-01 |
| ES8606311A1 (es) | 1986-04-01 |
| US4801707A (en) | 1989-01-31 |
| EP0173871B1 (de) | 1988-11-17 |
| DE3430435A1 (de) | 1986-02-27 |
| DE3566256D1 (en) | 1988-12-22 |
| KR920001765B1 (ko) | 1992-03-02 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A201 | Request for examination | ||
| G160 | Decision to publish patent application | ||
| E701 | Decision to grant or registration of patent right | ||
| NORF | Unpaid initial registration fee |