KR830002829A - 가연성 운모절연 테이프의 개선된 제조방법 - Google Patents
가연성 운모절연 테이프의 개선된 제조방법Info
- Publication number
- KR830002829A KR830002829A KR1019800001953A KR800001953A KR830002829A KR 830002829 A KR830002829 A KR 830002829A KR 1019800001953 A KR1019800001953 A KR 1019800001953A KR 800001953 A KR800001953 A KR 800001953A KR 830002829 A KR830002829 A KR 830002829A
- Authority
- KR
- South Korea
- Prior art keywords
- epoxide
- resin
- solvent
- mica
- organotin compound
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000010445 mica Substances 0.000 title claims description 9
- 229910052618 mica group Inorganic materials 0.000 title claims description 9
- 238000004519 manufacturing process Methods 0.000 title claims 2
- 239000007924 injection Substances 0.000 claims description 5
- 238000002347 injection Methods 0.000 claims description 5
- YCIMNLLNPGFGHC-UHFFFAOYSA-N catechol Chemical compound OC1=CC=CC=C1O YCIMNLLNPGFGHC-UHFFFAOYSA-N 0.000 claims description 4
- 239000003822 epoxy resin Substances 0.000 claims description 4
- 229920000647 polyepoxide Polymers 0.000 claims description 4
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 2
- 229910052802 copper Inorganic materials 0.000 claims description 2
- 239000010949 copper Substances 0.000 claims description 2
- 150000002118 epoxides Chemical class 0.000 claims 10
- 150000001875 compounds Chemical class 0.000 claims 9
- 238000000034 method Methods 0.000 claims 9
- 239000002904 solvent Substances 0.000 claims 6
- 239000000463 material Substances 0.000 claims 4
- 239000000203 mixture Substances 0.000 claims 4
- 229920005989 resin Polymers 0.000 claims 4
- 239000011347 resin Substances 0.000 claims 4
- 239000003054 catalyst Substances 0.000 claims 3
- 239000007787 solid Substances 0.000 claims 3
- WQGWDDDVZFFDIG-UHFFFAOYSA-N pyrogallol Chemical compound OC1=CC=CC(O)=C1O WQGWDDDVZFFDIG-UHFFFAOYSA-N 0.000 claims 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical group CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims 1
- FERIUCNNQQJTOY-UHFFFAOYSA-M Butyrate Chemical group CCCC([O-])=O FERIUCNNQQJTOY-UHFFFAOYSA-M 0.000 claims 1
- FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Chemical group CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 claims 1
- KKUKTXOBAWVSHC-UHFFFAOYSA-N Dimethylphosphate Chemical group COP(O)(=O)OC KKUKTXOBAWVSHC-UHFFFAOYSA-N 0.000 claims 1
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical group CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 claims 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims 1
- 239000012190 activator Substances 0.000 claims 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims 1
- 229910052782 aluminium Inorganic materials 0.000 claims 1
- 239000004020 conductor Substances 0.000 claims 1
- 125000000524 functional group Chemical group 0.000 claims 1
- 125000005843 halogen group Chemical group 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical group [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims 1
- 239000007788 liquid Substances 0.000 claims 1
- 238000002360 preparation method Methods 0.000 claims 1
- 229940079877 pyrogallol Drugs 0.000 claims 1
- 239000012974 tin catalyst Substances 0.000 claims 1
Classifications
-
- H—ELECTRICITY
- H02—GENERATION; CONVERSION OR DISTRIBUTION OF ELECTRIC POWER
- H02K—DYNAMO-ELECTRIC MACHINES
- H02K3/00—Details of windings
- H02K3/30—Windings characterised by the insulating material
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/68—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the catalysts used
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/13—Phenols; Phenolates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/56—Organo-metallic compounds, i.e. organic compounds containing a metal-to-carbon bond
- C08K5/57—Organo-tin compounds
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B3/00—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties
- H01B3/02—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of inorganic substances
- H01B3/04—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of inorganic substances mica
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B3/00—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties
- H01B3/18—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances
- H01B3/30—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes
- H01B3/40—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes epoxy resins
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2911—Mica flake
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31511—Of epoxy ether
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Physics & Mathematics (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Power Engineering (AREA)
- Organic Insulating Materials (AREA)
- Insulation, Fastening Of Motor, Generator Windings (AREA)
- Epoxy Resins (AREA)
- Insulating Bodies (AREA)
Abstract
Description
Claims (18)
- 하기의 성분으로 이루어지는 화합물의 제조방법
- (1) 용매에 대한 에폭사이드의 중량비가 85 : 15 내지 10 : 90으로서 반고체에폭사이드와 액체에폭사이드의 혼합물, 또는 고체에폭사이드와 엑체에폭사이드의 혼합물, 반고체에폭사이드;
- (2) 하기식의 유기주석 화합물 0.01 내지 5.0phr :
- R3SnX
- 상기식에서 R은 유기작용기이고 X는 할로겐화물, 수산화물, 아세테이트, 부티레이트, 프로피오네이트 또는 디메틸포스페이트에서 선택한 것임
- (3) 카테콜, 피로갈롤과 그 혼합물에서 선택한 활성제 0.001 애지 1phr
- 하기의 순서에 의해 가용성 운모절연 테이프 제조방법.
- (1) 상기의 항에 따른 성분화합물 제조
- (2) 사용성 쉬트물질 구성운모에 화합물을 가하여, 잠복촉매로서 작용하는 유기주석 화합물에 의해 유기주석 화합물이 운모와 접촉함
- (3) 쉬트물질에서 운모와 접촉하는 미반응의 유기주석 화합물의 증가량에 의해서 유기주석 화합물의 반응이나 에폭사이드수지의 가공에 의하지 아니하고 쉬트물질에서 에폭사이드수지-용매-유기주석 촉매로부터 최소한 용매 95%이상의 제거 여기에서 첨가한 유기주석 화합물의 양은 미반응상태에서 열경화상태로(수지촉매온도 150℃)쉬트물질에서 에폭사이드수지에 효과적으로 유기주석 화합물을 가한다.
- 25℃에서 25내지 200cps의 점도를 갖는 혼합물형성을 위해, 75℃이상의 온도에서 혼합을 하는 (1)단계와, 용매가 1내지 10분동안에 65℃내지 150℃의 수지용매 촉매온도로 (3)단계에서 제거하는 것을 특징으로 하는 청구범위 제2항에 따른 방법.
- 용매첨가전에 에폭사이드를 40℃ 내지 100℃로 가열하는 것을 특징으로 하는 청구범위 제2항, 제3항에 따른 방법.
- 에폭사이드 100부당 유기주석 0.05내지 1.0부를 사용함을 특징으로 하는 청구범위 제2항, 제3항에 따른 방법.
- 운모테이프 중량의 5내지 25%가 에폭사이드인 것을 특징으로 하는 청구범위 제2항 내지 제5항에 따른 방법.
- 주입수지와 수지, 에폭사이드 전부와 테이프를 감싼 모터코일에서의 테이프를 감싸는 최종단계에서의 첨가를 특징으로 하는 청구범위 제2항에서 제6항에 따른 방법.
- 주입수지가 에폭시수지임을 특징으로 하는 청구범위 제7항에 따른 방법.
- 에폭시사이드-촉매온도가 최소한 150℃로서, 구리 또는 알루미늄을 구성하는 전기콘덕터 주위의 테이프로 감싸는 마지막 첨가단계를 특징으로 하는 청구범위 제2항에서 제8항에 따른 방법.
- ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US039,918 | 1979-05-17 | ||
| US06/039,918 US4296018A (en) | 1979-05-17 | 1979-05-17 | Catechol or pyrogallol containing flexible insulating tape having low gel time |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR830002829A true KR830002829A (ko) | 1983-05-30 |
| KR840001788B1 KR840001788B1 (ko) | 1984-10-20 |
Family
ID=21908047
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1019800001953A Expired KR840001788B1 (ko) | 1979-05-17 | 1980-05-17 | 가요성 운모절연 테이프의 제조방법 |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US4296018A (ko) |
| JP (1) | JPS55152718A (ko) |
| KR (1) | KR840001788B1 (ko) |
| BR (1) | BR8003070A (ko) |
| CA (1) | CA1152676A (ko) |
| FR (1) | FR2456760A1 (ko) |
| IN (1) | IN153135B (ko) |
| IT (1) | IT8022146A0 (ko) |
| SE (1) | SE8003672L (ko) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4427740A (en) * | 1982-04-09 | 1984-01-24 | Westinghouse Electric Corp. | High maximum service temperature low cure temperature non-linear electrical grading coatings resistant to V.P.I. resins containing highly reactive components |
| FR2534735B1 (fr) * | 1982-10-15 | 1985-07-05 | Habia Sa | Revetement isolant |
| US4606785A (en) * | 1984-11-15 | 1986-08-19 | Westinghouse Electric Corp. | Simplified method of making high strength resin bonded mica tape |
| US6103382A (en) * | 1997-03-14 | 2000-08-15 | Siemens Westinghouse Power Corporation | Catalyzed mica tapes for electrical insulation |
| CN1087751C (zh) * | 1998-04-09 | 2002-07-17 | 中国科学院化学研究所 | 一种环氧树脂组合物 |
| US6384152B2 (en) | 1999-07-19 | 2002-05-07 | Siemens Westinghouse Power Corporation | Insulating resin of epoxy resin, epoxy diluent, phenolic accelerator and organotin catalyst |
| US6361632B1 (en) | 1999-11-24 | 2002-03-26 | Siemens Westinghouse Power Corporation | Method to increase compressive creep capabilities of high voltage coil insulation |
| US6190775B1 (en) * | 2000-02-24 | 2001-02-20 | Siemens Westinghouse Power Corporation | Enhanced dielectric strength mica tapes |
| US20050260522A1 (en) * | 2004-02-13 | 2005-11-24 | William Weber | Permanent resist composition, cured product thereof, and use thereof |
| US8678555B1 (en) * | 2012-11-01 | 2014-03-25 | Funai Electric Co., Ltd. | Encapsulation of inkjet heater chip for ion beam cross-section polishing and method of preparing chip cross-section sample |
| DE102015213537A1 (de) * | 2015-07-17 | 2017-01-19 | Siemens Aktiengesellschaft | Fester, insbesondere bandförmiger, Isolationswerkstoff, Formulierung für ein Imprägniermittel zur Herstellung eines Isolationssystems in einem Vakuumimprägnierverfahren damit und Maschinen mit derartigem Isolationssystem |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL282843A (ko) * | 1961-10-03 | |||
| FR1364456A (fr) * | 1962-07-27 | 1964-06-19 | Consortium Elektrochem Ind | Procédé de durcissement d'époxydes |
| US3294865A (en) * | 1965-12-13 | 1966-12-27 | Celanese Coatings Company Inc | Curing of epoxy resins with polycarboxylates, polyhydric phenols or polyhydric alcohols and, as an accelerator, an alkali metal salt |
| US3728306A (en) * | 1971-07-27 | 1973-04-17 | Gen Electric | Composition comprising an epoxy resin with an organostannoic acid-carboxylic acid anhydride reaction product |
| BE790022A (fr) * | 1971-10-14 | 1973-04-12 | Westinghouse Electric Corp | Ameliorations apportees ou se rapportant a des compositions resineuses epoxydes |
| US3716598A (en) * | 1971-10-28 | 1973-02-13 | Gen Electric | Hardenable epoxy resin compositions |
| CA996849A (en) * | 1972-08-02 | 1976-09-14 | General Electric Company | Insulating material |
| US4169825A (en) * | 1975-05-15 | 1979-10-02 | The Sherwin-Williams Company | High solids coating compositions |
| US3998983A (en) * | 1975-06-27 | 1976-12-21 | Westinghouse Electric Corporation | Resin rich epoxide-mica flexible high voltage insulation |
| US4013987A (en) * | 1975-08-22 | 1977-03-22 | Westinghouse Electric Corporation | Mica tape binder |
| US4137275A (en) * | 1976-04-27 | 1979-01-30 | Westinghouse Electric Corp. | Latent accelerators for curing epoxy resins |
| US4112183A (en) * | 1977-03-30 | 1978-09-05 | Westinghouse Electric Corp. | Flexible resin rich epoxide-mica winding tape insulation containing organo-tin catalysts |
| JPS6029730B2 (ja) * | 1977-08-06 | 1985-07-12 | 三菱電機株式会社 | エポキシ樹脂組成物 |
| US4178323A (en) * | 1978-12-26 | 1979-12-11 | Ford Motor Company | High solids coating composition with hydroxy functional acrylic organophosphate reactive catalyst-II |
-
1979
- 1979-05-17 US US06/039,918 patent/US4296018A/en not_active Expired - Lifetime
-
1980
- 1980-05-12 IN IN563/CAL/80A patent/IN153135B/en unknown
- 1980-05-14 FR FR8010906A patent/FR2456760A1/fr active Pending
- 1980-05-15 CA CA000352004A patent/CA1152676A/en not_active Expired
- 1980-05-16 SE SE8003672A patent/SE8003672L/xx not_active Application Discontinuation
- 1980-05-16 IT IT8022146A patent/IT8022146A0/it unknown
- 1980-05-16 BR BR8003070A patent/BR8003070A/pt unknown
- 1980-05-16 JP JP6417980A patent/JPS55152718A/ja active Granted
- 1980-05-17 KR KR1019800001953A patent/KR840001788B1/ko not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| KR840001788B1 (ko) | 1984-10-20 |
| SE8003672L (sv) | 1980-11-18 |
| IN153135B (ko) | 1984-06-02 |
| JPS55152718A (en) | 1980-11-28 |
| CA1152676A (en) | 1983-08-23 |
| IT1140952B (ko) | 1986-10-10 |
| BR8003070A (pt) | 1980-12-23 |
| IT8022146A0 (it) | 1980-05-16 |
| FR2456760A1 (fr) | 1980-12-12 |
| US4296018A (en) | 1981-10-20 |
| JPS5711565B2 (ko) | 1982-03-05 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PA0109 | Patent application |
Patent event code: PA01091R01D Comment text: Patent Application Patent event date: 19800517 |
|
| PG1501 | Laying open of application | ||
| PE0902 | Notice of grounds for rejection |
Comment text: Notification of reason for refusal Patent event date: 19840316 Patent event code: PE09021S01D |
|
| PG1605 | Publication of application before grant of patent |
Comment text: Decision on Publication of Application Patent event code: PG16051S01I Patent event date: 19840922 |
|
| E701 | Decision to grant or registration of patent right | ||
| PE0701 | Decision of registration |
Patent event code: PE07011S01D Comment text: Decision to Grant Registration Patent event date: 19841231 |