KR810001683B1

KR810001683B1 - Dyeing method of silk

Info

Publication number: KR810001683B1
Application number: KR1019800003894A
Authority: KR
Inventors: 이병국
Original assignee: 이병국
Priority date: 1980-10-10
Filing date: 1980-10-10
Publication date: 1981-10-27

Abstract

Silk yarn, exhibiting a graceful, silky luster, for silk fabrics was dyed without heating treatment by 4 continuous steps. Thus, skeins of silk yarn were dyed with a mixt. of tannin acid or cutch and hermatine dissolved in water; (1) the skeins were scrubbed in dyeing chamber and dried; (2) and scrubbed in CaCO3-dissolved water, the process was repeated three times; (3) and scrubbed in FeSO4-dissolved warm water; (4) and washed with water, dehydrated, and dried.

Description

Silk thread dyeing method

본 발명은 비단직조용 견사(생사)를 은은하고 무게있는 우아한 색상으로 염색하는 염색방법에 관한 것이다. 종래의 염색조에서 가열 염색한 견사는 가열처리로 인하여 섬유질에 경박하고 야한 광택이 생기는 문제점이 있었고 따라서 비단을 직조하였을 때 경박스럽고 야한 느낌을 주게 되어 비단으로서의 고급품을 생산하지 못하였으며 또한 퇴색이 빨리되는 결점이 있었다. 본 발명은 이러한 종래의 견사 염색방법을 지양하여 가열염색방법을 취하지 않고 갓치 또는 차륜매에서 추출한 탄닌산과 헤마틴(분말, 액)을 주재로 한 염색제를 사용하여 견사의 섬유질을 염색으로 변화시키는 염색처리를 하므로써 은은하고 무게있는 우아한 색상의 견사를 얻도록 함과 아울러 가볍고 꾸김살이 가지 않는 고급비단을 직접 생산할 수 있게 하여 종래의 수출품에 비하여 월등하게 비싼 외화획득 비단상품을 얻을 수 있게 발명한 것인바 이를 상세히 설명하면 다음과 같다.The present invention relates to a dyeing method of dyeing silk yarn for silk weaving (raw yarn) in a subtle and weighty elegant color. The silk thread heat-dyed in the conventional dyeing tank has a problem of light and lustrous luster due to the heat treatment. Therefore, when weaving the silk, it gives a frivolous and rugged feeling, and it cannot produce high-quality products as silk. There was a flaw. The present invention avoids the conventional silk dyeing method, and does not take the heat dyeing method, and dyes the fiber of silk by changing the dyeing fiber by using a dyeing agent based on tannic acid and hematine (powder, liquid) extracted from the larches or the wheel wheel By inventing, silky and silky silk thread of silk color can be obtained, and it is possible to produce high-quality silk that is light and undecorated, and it is invented to obtain silk goods which are much more expensive than conventional export products. It will be described in detail as follows.

본 발명은 먼저 차륜매(車輪梅)에서 추출한 탄닌산 또는 캇치(CUTCH)와 헤마틴(HERMATINE)(분말, 액)에 혼합하여 교반 가열한 뜨거운 A액에 타래견사를 담궈서 약 20시간 방치한 후 건져 내어 탈수하여 건조하는 제1공정과 상기 A액을 2배의 물에 희석한 A'액에 견사타래를 담궈 손으로 비비며 염색한 후 건져내어 건조한 후 생석회 용해수의 윗물을 희석한 생석회 희석수 B액에 타래견사를 담궈 손으로 비비면서 염색한 후 탈수 건조하는 공정을 3회 반복하는 제2공정과 수은 80℃의 물에 유산철 2% 비율로 희석한 C액에 1시간 정도 비벼 염색한 후 1시간 담궜다가 완전 수세 탈수하여 건조하는 제3공정과 논의 이토(泥土)를 물에 혼합한 혼탁수에 담궈서 비빈후 건져서 수세 및 탈수 건조하는 제4공정을 실시하여 완성하는 것이다.The present invention is first mixed with tannin acid or Catch and HERMATINE (powder, liquid) extracted from a wheel mae, soaking the skein dog in hot A solution heated by stirring and left for about 20 hours First step of drying and dehydrating and drying the A solution in A 'solution diluted in 2 times of water, rubbing the silk thread by hand, rubbing and dying. After dipping the skein thread into the solution, rubbing it by hand and dyeing it, dehydrating and drying it three times and dyeing it with C solution diluted at a rate of 2% iron lactate in 80 ° C of mercury for 1 hour The third step of immersing for 1 hour and then completely washing with water and drying is completed. The third step of dipping Ito in turbid water mixed with water is emptied, followed by the fourth step of washing with water and dehydrating and drying.

이와 같이 된 본 발명의 견사는 차륜매에서 추출한 탄닌산 또는 캇치와 헤마틴을 주재로 한 이상(泥狀)의 염색제를 사용한 비가열 염색방법으로 견사의 탈지작용과 섬유질 전체를 염색 섬유질로 변화되는 염색처리가 되어 영구불변이라 할 정도로 퇴색현상이 일어나지 않으며 탈지작용으로 무게가 가벼워지고 직조한 비단은 은은하고 무게있는 우아한 색상을 지니게 되어 더없이 고급스러운 비단을 수출 수요자에게 공급할 수 있는 것이다.Thus, the silk of the present invention is a non-heating dyeing method using a tannin acid extracted from a wheel hawk or more than one dyeing agent based on cut and hematine and dyeing action of the silk is changed to dyeing fiber as a whole It is treated so that it does not fade to the extent that it is permanent, and the weight is lightened by degreasing, and the woven silk has a soft and elegant elegant color, which can supply more luxurious silk to export demand.

본 발명의 실시예를 상술하면 다음과 같다.An embodiment of the present invention will be described in detail as follows.

[제1공정][Step 1]

캇치 2kg과 헤마틴(분말, 액) 300g을 물 200cc에 혼합교반하면서 가열하여 뜨거운 A액을 얻고 뜨거운 A액 염색조에 타래견사(생사) 100타래(5kg)을 담궈 뒤집음 손질후 약 20시간 재운 다음 건져서 액을 짜서 탈수하여 건조한다.2kg of cut and 300g of hematine (powder, liquid) are mixed and stirred in 200cc of water to obtain hot A liquid.Then, 100 threads (5kg) of raw silk thread (5 kg) are inverted in a hot A liquid dyeing bath and inverted. Next, squeeze out the liquid, dehydrate it and dry it.

[제2공정][Step 2]

상온으로 내려간 A액을 2배의 물로 희석한 A'액의 염색조에 타래견사를 담궈 손으로 비비며 염색한 후 건져내 탈수하여 건조하고 물 50ℓ에 생석회 10kg을 넣어 용해한 후 생석회분을 가라앉힌 윗물을 떠서 물 10ℓ에 윗물 200cc 비율로 재차 혼합하여 얻은 B액 침지조에 타래견사를 담궈 실을 손으로 비비면서 B액이 견사섬유질에 충분히 침투되도록 한 후 탈수하여 건조하는 공정을 3회 반복한다.Dip the skein of A 'solution, diluted to twice the amount of water, into a dyeing tank of A' solution diluted with twice the amount of water. Rub it out by hand, dye it, dry it, dehydrate it, dry it. Repeat the process of soaking the silk thread in B liquid immersion tank obtained by mixing again at 200cc ratio of 10 liters of water and rubbing the thread by hand to allow the liquid B to penetrate into the silk fiber and dehydrating and drying three times.

[제3공정][Step 3]

수은 80℃의 물에 유산철 2%의 비율로 희석한 C액 염색조에 제3공정을 실시한 타래견사를 담궈 손으로 비비면서 액의 침투 촉진작용 손질을 한 다음 1시간 정도 담궈 두었다가 건져 내어 물에 헹궈서 씻은 다음 탈수하여 완전 건조한다.Dilute the skein silk thread, which was subjected to the third process, in a C-liquid dye bath diluted at a rate of 2% ferric lactate in water at 80 ° C of mercury. Rub it by hand and clean the solution for promoting penetration. Rinse, wash and dehydrate to dry completely.

[제4공정][Step 4]

논의 이토(泥土)를 물에 혼합한 혼탁수에 제3공정을 실시한 타래 견사를 소쿠리에 넣어 담궈서 손으로 비비는 공정을 실시한 후 건져내어 수세하고 탈수 건조한다.Discussion After dipping the skein silk from the third step into a turbid water mixed with Ito, put it in a colander, rub it by hand, take it out, wash it with water, and dehydrate it.

Claims

As described above in the main body, tannin acid or catechi extracted from the wheel hawk and hematine are mixed with water, boiled and immersed in the A solution dye bath, which was then boiled and dyed in the A 'solution dye bath. The second process of repeating the process of rubbing and trimming the thread in the dilute solution B diluted with lime, and the third process of rubbing and dyeing it in a C solution dye bath diluted with iron lactate in hot water and dipping it in turbid water Silk yarn dyeing method combining the fourth step of washing with water and dehydration drying.