KR810001124B1 - Process for preparing deodorant - Google Patents

Abstract

Deodorant having excellent deodorization and detoxification activity was prepd. by extg. of plant components. Thus, mixed comp. which contained dry mugwort 5g, leaf of white birch 30g, Aurantii percarpium 8g, leaf of Lycii fructus 13g, Leonuri herba 6g, fruit of needle juniper 4g, Atractylodes zeolite 10g added 5 liter of water, concentrated by heat and filtered to give deodorant soln.

Description

Manufacturing method of deodorant

The present invention relates to a method for producing a deodorant composition based on the extract of a particular plant. The deodorizing composition of the present invention is an excellent novel deodorizing agent having adsorption and removal action of poison gas in addition to the simple deodorizing action. In the past, there was a deodorant using activated carbon or zeolite, but the deodorant based on activated carbon, which has been used previously, does not have a restoring power of deodorizing power. The effect was extremely limited.

That is, the deodorant by activated carbon has already made the deodorant liquid extremely because the degassing molecule easily becomes large due to moisture.

In addition, the zeolite-based deodorant had no property of neutralizing malodorous components and thus could not obtain a deodorizing effect. Therefore, the inventors of the present invention have been able to invent a very good and surprising deodorant composition from the real ingredients that can be easily obtained in Korea's field while researching a more persistent and powerful deodorant than the heavy deodorant.

When explaining the present invention in detail, dried mugwort 3-5 parts by weight, birch leaves 30-50 parts by weight, dermis 5-10 parts by weight, gojija leaf 10-15 parts by weight, motherwort 5-7 parts by weight, jicho 6 8-40 parts by weight, 2-3 weights of birch leaves, 10-15 parts by weight, 3-5 parts by weight of Cheonnam, and 10-15 parts by weight of 150-200 mesh zeolite were added by adding sufficient amount of water to 30-40 Warm for 1 hour at ˚C, heat distillate at about 110˚C, concentrate until the volume of extract is about 2/3, extract, and add about half of the composition of the same composition ratio. The mixture was then concentrated by heating until it was concentrated to 2/3 volume and then filtered to obtain a concentrated deodorizing solution.

This deodorant may be used in a liquid state as it is, but may also be used as a solid deodorant synthesized in a sponge or the like by mixing with another deodorant such as zeolite.

Individual extracts used in the composition of the present invention alone can not obtain the desired deodorizing effect, it was found that each component exhibits the most excellent and powerful deodorizing effect when mixed and extracted in the above composition ratio.

Although the exact reason for the strong deodorizing effect of the composition of the present invention is not known, the main component in the solution extracted from the composition of the present invention is a derpin-based essential oil component having an alcoholic hydroxyl group, wormwood such as 1.8 cinemol in mugwort and pidosterol in motherwort. As a kind of fatty acid ester and birch, guardene, a kind of phenol glycoside, is hydrolyzed to produce methyl salicylate, which is a characteristic aromatic substance.The dermis contains limonene, and gojija is a polybonoid (C ₂₇ H). ₃₀ O ₁₆ ) components, teractol (C ₁₅ H ₂₆ ) is teratol alcohol to create, saponin component in Cheonnam Province, pine (C ₁₀ H ₁₆ ) component in Dulsonsil leaves contain synergistic fragrance It is estimated to exert a strong deodorant effect by odor, income and deodorant action.

In addition, the crystal structure of zeolite is tetrahedron of oxygen surrounding silicon, and part of the silicon in the central part is replaced with aluminum ions, and alkali and alkaline earth metals such as sodium, potassium, calcium, and barium may be filled in place.

Since these cations move relatively freely in the gap, they are in contact with solutions containing other cations and thus exchange with other ions. These zeolites are used as cation adsorption aids in the present invention, and in particular, lower the pH by 1-2. In addition, it is believed that the adsorption of cationic malodorous gases, such as ammonia and hydrogen sulfide, in the malodor is more powerful.

The pH of the present invention deodorant is also a very important factor. According to the test of the present inventors, the stronger the acidity, the better the deodorizing effect and the pH of the solution extracted by adding zeolite than the pH of the solution from which only the plant components of the present invention were extracted. Was found to be more acidic.

The deodorant of the present invention can be used as a solid or impregnated with a sponge or mixed with other deodorants such as zeolites to further enhance the deodorizing power. Can be used as Hereinafter, the present invention will be described in more detail with reference to Examples.

Example 1

[Production of deodorant liquid]

5 liters of water was added to a mixed composition of dried wormwood 5g birch leaf 30g, dermis 8g, goji berry leaf 13g, motherwort 6g, jigocho 7g, dusongsil leaf 4g, creation 12g, 4g cheonnam and 10g zeolite 10g After warming to lukewarm (30-40˚C) for 1 hour, distillation by heating (100 -110˚C), concentrated extraction until solution is about 3 liters, filtered under reduced pressure and dried again in this filtrate concentrate. Add 16 g of crunchy tree leaf, 4 g of dermis, 6 g of Goji leaf, 6 g of motherwort, 3 g of Jichocho, 2 g of Duksongsil leaf, 6 g of creation, 2 g of Cheonnam and 5 g of zeolite of 150-200 mesh. Heated and concentrated until it was extracted and filtered to obtain 2 liters of concentrated deodorizing solution.

Example 2

[Production of Solid Deodorant]

120 ml of the deodorizing solution obtained in Example 1 and 100 g of 200 mesh zeolite were thoroughly mixed with an appropriate amount of fertilizer, impregnated in a sponge having a thickness of 1.5 cm, a length of 50 cm, and a width of 50 cm, dried in a decimator, and then dried to a suitable size. Solid deodorant was prepared.

Test 1: Deodorization test of the sponge containing the present invention composition

end. Test: A: Inventive deodorant of Example 2

B: well-known palm activated carbon

I. Test method: Pork and leek fish were placed in two wooden boxes, 60 cm wide, 60 cm long and 90 cm high, sealed for 24 hours at 40 ° C and 90% humidity. Were put into each wooden box, and after a certain time, the degree of odor was sensory judged.

All. Test Result: The test conditions and sensory evaluation results are shown in Table 1 below.

TABLE 1

Deodorization test result table

Odor determination degree:

0: no smell, 1: slight smell, 2: smell, 3: odor

Test 2: Deodorization test of the present invention deodorant

end. Sample: A ': 100cc of the present invention deodorant of Example 1

B ': 20 pieces of activated carbon in a thin paper bag

I. Test method: Spray 10cc of ammonia water in a room with a wind velocity of 0.5-10m / sec and a temperature of 20m with a width of 3m, a length of 4m, and a height of 3.5m, and seal the sample A 'through a hole of 1cm diameter in the middle of the door. 5 samples of B'20 were suspended in the air of 2m above the ground at a distance of 2m and sealed by spraying 10cc of ammonia water, and after a predetermined time, the degree of odor was sensory determined.

All. Test result

The test results are shown in Table 2 below.

TABLE 2

Deodorization test result table

Odor determination degree:

No odor, 1: slight odor, 2: odor, 3: weak, 4: intense odor

[Test 3: Synergy test of the present invention deodorant liquid]

This test is to compare each deodorizing effect by preparing a deodorant according to the method of each single component, three kinds of plant components, and nine kinds of vegetable fires of the same weight.

However, the component ratio of each composition was formed in the same ratio as the corresponding secretion ratio of the composition of this invention.

A: Test method

Hydrogen gas is blown into a room with a room temperature of 25-26˚C, 3.3cm wide, 5.3cm high, and 2.8cm high, and the odor level is 4 degrees and the deodorant is 1 liter for each test. Was vaporized into a humidifier, the door was sealed, and after a certain period of time, it entered the room and subjected to an audible response test. The test results are shown in the following table.

[I. Test Result Table 3-1]

[Test Result Table 3-2]

[Test Result Table 3-3]

[Test Result Table 3-4]

Claims (1)

Dried mugwort 3-5 parts by weight, crunchy tree leaves 30-50 parts by weight, dermis 5-10 parts by weight, goji berry leaves 10-15- parts by weight, motherwort herb 5-7 parts by weight, jichocho 6-8 parts by weight, Dosongsil To the mixed composition consisting of 3-5 parts by weight, 10-15 parts by weight of worms, 3-5 parts by weight of Cheonnam and 10-15 parts by weight of zeolite of 150-200 mesh, add enough wet water to 1 to 30-40 ° C. After heating, the mixture was heated and distilled to 110˚C, concentrated until the concentration of the concentrate was about 2/3, and then extracted and filtered. Then, about half of the mixed composition of the same composition was added. Heat-concentrate until it is / 3, and then extract and filter to prepare a deodorant.