KR20230097527A - Jelly containing nicotine and the manufacturing method thereof - Google Patents

Abstract

The present invention relates to a method for manufacturing jelly containing nicotine and food gel HA, and the manufacturing process is simple and productivity can be increased. It has no fear of irritating the skin, is easy to carry, can be easily consumed, and has excellent taste and fragrance, so it is suitable for consumer's preference.

Description

Jelly containing nicotine and the manufacturing method thereof {Jelly containing nicotine and the manufacturing method thereof}

The present invention relates to a jelly containing nicotine and a method for preparing the same.

Smokeless tobacco is a product that melts in the mouth and is absorbed through the mucous membrane, helping the absorption of nicotine in the oral mucosa. Representative examples of smokeless tobacco include nicotine patches and nicotine gum.

In the case of nicotine gum, if you feel a little tingling while chewing it slowly over about an hour, place the gum between your teeth and cheek to absorb nicotine through the mucous membrane in your mouth. If nicotine gum is chewed too quickly, the nicotine blood level may be too high, and the excessive nicotine released at once when chewing can irritate the mouth and throat, strain the jaw joint, feel sick to the stomach, and increase the heart rate. there is.

In the case of nicotine patches, nicotine is continuously supplied to the body at a certain concentration in the blood, but skin irritation can be a problem when used for a long time, and side effects such as damage due to skin friction, nausea or vomiting, dizziness, increased heart rate, sleep disorder, etc. This can be.

Accordingly, the inventors of the present invention developed a nicotine jelly stick that has an appropriate viscosity, so there is no difficulty in chewing movement, no fear of skin irritation, and is easy to carry and ingest, and completed the present invention. This is a form that did not exist before, and the present invention provides a novel nicotine jelly.

KR 10-2001-0078976

The technical problem to be achieved by the present invention is to provide a method for producing nicotine jelly.

In addition, another object of the present invention is to provide a nicotine jelly prepared using the above manufacturing method.

However, the technical problem to be achieved by the present invention is not limited to the above-mentioned problems, and other problems not mentioned will be clearly understood by those skilled in the art from the description below.

In order to solve the above problems, the present invention provides a method for producing nicotine jelly comprising the following steps:

(1) adding and mixing nicotine and food gel HA;

(2) transferring the mixture of step (1) to a stirring tank and then warming it;

(3) after step (2), further adding at least one selected from the group consisting of fruit juice, vitamins, caffeine, and GABA to the stirring tank and then stirring;

(4) stirring and sterilizing under reduced pressure to produce a concentrate;

(5) further agitating the concentrate of step (4);

(6) lowering the stirring speed, filtering, and transferring to a service tank; and

(7) Manufacturing jelly using the contents of the service tank in step (6).

As an embodiment of the present invention, in step (1), the food gel HA may be dispersed without agglomeration.

As another embodiment of the present invention, in step (1), 0.01 to 10 mg of nicotine and 0.001 to 10 mg of food gel HA may be added and mixed.

As an embodiment of the present invention, the step (2) may be to warm to 80 to 90 ℃.

As another embodiment of the present invention, step (2) may include transferring the mixture to a stirring tank, adjusting the sugar content by adding fructooligosaccharide or ovarian active maltodextrin, and then heating the mixture.

As an embodiment of the present invention, after step (2) and before step (3), a thickener may be additionally added, and a step of stirring until the thickener is dissolved may be optionally included.

As another embodiment of the present invention, the stirring step after adding the thickener may be stirring at 50 to 60 rpm.

As another embodiment of the present invention, after the step and before the step (3), a step of mixing sodium citrate or calcium lactate in the stirring tank may be further included.

As an embodiment of the present invention, step (3) may be stirring at 40 to 50 rpm for 5 to 10 minutes.

As an embodiment of the present invention, step (4) may be stirring at 20 to 30 rpm under a reduced pressure of 0.01 to 1 MPa for 20 to 60 minutes at 80 to 90 ° C.

As an embodiment of the present invention, step (5) may be additional stirring at 20 to 30 rpm under reduced pressure.

As another embodiment of the present invention, after step (5) and before step (6), adding anhydrous citric acid or fruit flavor, administering purified water, and further comprising the steps of adjusting the sugar level using agave syrup it could be

As an embodiment of the present invention, step (6) may be to filter after stirring at 75 to 85 ° C. at 10 to 20 rpm.

As another embodiment of the present invention, step (6) may be filtering with a 30 to 50 mesh.

In addition, the present invention provides a nicotine jelly prepared by the method for producing nicotine jelly described above.

As an embodiment of the present invention, the nicotine jelly may have a pH of 2 to 5, preferably 2.58, and a sugar content of Brix 30 to 70, preferably 64.

As another embodiment of the present invention, the nicotine jelly may be in a stick form.

As another embodiment of the present invention, the nicotine jelly contains nicotine 5-10%, food gel HA 1-2%, fructooligosaccharide 3-6%, ovarian active maltodextrin 1-5%, agave syrup 0.1-2% , sodium citrate 0.3~0.6%, calcium lactate 0.3~0.6%, fruit juice 0.1~10%, vitamins, caffeine 0.1~10%, GABA 0.1~10%, anhydrous citric acid 0.05~0.5%, fruit flavor 0.05~ It may be prepared by mixing 0.5% and 30 to 50% of purified water. Preferably, nicotine 7%, food gel HA 1.6%, fructooligosaccharide 5%, ovarian active maltodextrin 3%, agave syrup 1%, sodium citrate 0.5%, calcium lactate 0.5%, fruit juice 0.1-10%, vitamins , caffeine 0.1-10%, GABA 0.1-10%, anhydrous citric acid 0.2%, fruit flavor 0.2%, and purified water 30-50%.

The present invention relates to a method for manufacturing jelly containing nicotine and food gel HA, and the manufacturing process is simple and productivity can be increased. It has no fear of irritating the skin, is easy to carry, can be easily consumed, and has excellent taste and fragrance, so it is suitable for consumer's preference.

The present invention (1) adding and mixing nicotine and food gel HA; (2) transferring the mixture of step (1) to a stirring tank and then warming it; (3) after step (2), further adding at least one selected from the group consisting of fruit juice, vitamins, caffeine, and GABA to the stirring tank and then stirring; (4) stirring and sterilizing under reduced pressure to produce a concentrate; (5) further agitating the concentrate of step (4); (6) lowering the stirring speed, filtering, and transferring to a service tank; And (7) preparing jelly using the contents of the service tank in step (6); provides a method for producing nicotine jelly, including.

The present invention relates to nicotine jelly that did not exist before and a method for producing the same, and provides a simple method for producing nicotine jelly that can be consumed anytime, anywhere, can be enjoyed as a light snack, and has a good taste and high consumer preference. do.

In the present invention, "(1) nicotine and food gel HA mixing step" refers to the step of adding and mixing 0.01 to 10 mg of nicotine and 0.001 to 10 mg of food gel HA. At this time, in the present invention, the "food gel" may include locust bean gum, xanthan gum, glucose, agar, tamarind gum, carrageenan, or potassium chloride, and the food gel HA of the present invention is a complex agent containing a thickening agent. , Locust bean gum 50%, xanthan gum 30%, glucose 10%, agar 5%, and tamarind gum 5% may be included, but is not limited thereto. When the amount of the food gel is less than 0.001 mg, the gel is too thin to form a jelly, and when the amount exceeds 10 mg, the gel becomes hard and excessive masticatory movements may be required.

In the present invention, “(2) warming step” refers to a step of warming the mixture to 80 to 90° C., preferably 85° C., after transferring the mixture to a stirring tank. When heated below 80°C, gel is not formed because it is not sufficiently dissolved, and when heated above 90°C, solids may be formed in the form of dots in the gel.

After transferring the mixture to a stirring tank, the sugar content may be adjusted to Brix 30 to 50 by selectively adding fructooligosaccharide or ovarian activated maltodextrin to the mixture before heating. In the present invention, “fructooligosaccharide” refers to a mixture of saccharides in which 1 to 3 fructose are bonded to a fructose residue. Unlike general sugar or glucose, “fructooligosaccharide” is a polysaccharide, so digestion and absorption take a long time to slowly increase blood sugar, and stomach acid It reaches the small intestine directly without being decomposed by digestive enzymes in the small intestine, and after reaching the large intestine without being hydrolyzed by digestive enzymes in the large intestine, it is metabolized by beneficial bacteria in the large intestine and converted into short-chain fatty acids, so it has effects on intestinal health, prevention of constipation, and promotion of mineral absorption. have In the present invention, “indigestible maltodextrin” is a component obtained by dry hydrolysis of corn starch, which can control blood sugar by slowing down the absorption of sugar in the intestine, and lowers visceral fat, blood sugar, triglyceride and cholesterol, so it is useful for metabolic syndrome. There is an improvement effect.

In the present invention, after adding fructooligosaccharide or ovarian-activated maltodextrin, adding a thickener to the stirring tank, and stirring at 50 to 60 rpm, preferably 50 to 55 rpm until the thickener is dissolved, is optionally performed. can include In the present invention, "thickening agent" is an additive for improving the physical stability of a mixture, and can increase aesthetic value by imparting hardness, smoothness, softness, etc. There are semi-synthetic materials such as methyl cellulose and methyl cellulose, and synthetic polymers include carboxyvinyl polymers, but are not limited thereto. In the present invention, the thickener is included in the food gel HA, and the stability can be controlled by additionally administering the thickener.

In addition, after adding the thickener and stirring, sodium citrate or calcium lactate may be added for pH control and then mixed.

In the present invention, “(3) adding fruit juice and stirring step” is to add fruit juice, vitamins, caffeine, or GABA to the stirring tank, and stir at 40 to 50 rpm for 5 to 10 minutes, preferably 40 to 45 rpm. Additives may further include ingredients for adding various nutrients, flavors, or colors other than fruit juice, vitamins, caffeine, or GABA.

In the present invention, "(4) sterilization step" is 80 to 90 ℃, preferably 82 ℃ for 20 to 60 minutes, preferably 30 minutes under a reduced pressure of 0.01 to 1 MPa, preferably 0.05 MPa 20 to 30 After stirring at rpm, preferably 20 to 25 rpm, it refers to the step of sterilizing to produce a concentrate.

In the present invention, "(5) additional stirring step" refers to the step of stirring at 25 rpm under the above-described reduced pressure condition. After additional stirring, anhydrous citric acid or fruit flavor may be added, purified water may be added, and the sugar content may be corrected using agave syrup. In the present invention, "purified water" means purified water that has been sterilized to remove dissolved minerals, dissolved organic matter, microparticles, or microorganisms by distilling constant water or purifying through an ion exchange resin. Agave syrup may be added one or more times during steps (1) to (5) of the present invention, which is to increase consumer preference by imparting appropriate sugar content.

In the present invention, “(6) filtration step” lowers the stirring speed to 10 to 20 rpm, preferably 10 to 15 rpm, maintains 75 to 85 ° C, preferably 80 ° C, and the concentrate is 30 to 50 ° C. It refers to the step of filtering with a mesh, preferably 40 mesh, and then transferring to a service tank.

In the present invention, "(7) jelly manufacturing step" refers to the step of manufacturing nicotine jelly using the contents of the service tank. After manufacturing jelly, it can be subjected to process inspection through transport and filtering. At this time, the jelly is stored in a low-humidity and low-temperature warehouse, and may be vacuum-packed by sealing treatment.

According to the manufacturing method of the present invention, nicotine jelly can be uniformly formed, and the nicotine jelly contains 7% nicotine, 1.6% food gel HA, 5% fructooligosaccharide, 3% ovarian active maltodextrin, 1% agave syrup, Sodium citrate 0.5%, calcium lactate 0.5%, fruit juice 0.1-10%, vitamins, caffeine 0.1-10%, GABA 0.1-10%, anhydrous citric acid 0.2%, fruit flavor 0.2%, purified water 30-50% It can be prepared by mixing.

Terms used in the examples are used only for the purpose of explanation and should not be construed as limiting. Singular expressions include plural expressions unless the context clearly dictates otherwise. In this specification, terms such as "include" or "have" are intended to designate that there is a feature, number, step, operation, component, part, or combination thereof described in the specification, but one or more other features It should be understood that the presence or addition of numbers, steps, operations, components, parts, or combinations thereof is not precluded.

Unless defined otherwise, all terms used herein, including technical or scientific terms, have the same meaning as commonly understood by a person of ordinary skill in the art to which the embodiment belongs. Terms such as those defined in commonly used dictionaries should be interpreted as having a meaning consistent with the meaning in the context of the related art, and unless explicitly defined in the present application, they should not be interpreted in an ideal or excessively formal meaning. don't

In the following, various changes may be made to the embodiments, so the scope of rights of the patent application is not limited or limited by these embodiments. It should be understood that all changes, equivalents or substitutes to the embodiments are included within the scope of rights.

In describing the embodiment, if it is determined that a detailed description of a related known technology may unnecessarily obscure the gist of the embodiment, the detailed description will be omitted.

[Example]

Example 1: Manufacturing method of nicotine jelly

0.01 to 10 mg of nicotine was added to the AZ mixer and mixed, and 0.001 to 10 mg of food gel HA was further added to disperse the mixture without clumping. Thereafter, fructooligosaccharide and ovarian active maltodextrin were added to adjust the sugar content to Brix 30 to 50.

The mixture dispersed in the AZ mixer was added to the stirring tank and heated to 85°C. The thickener was added, and the stirring blade was operated at 50 to 55 rpm and stirred until the thickener was dissolved. Sodium citrate and calcium lactate were further mixed in the stirring tank. Fruit juice, vitamins, caffeine, GABA, etc. were added to the stirring tank and stirred at 40 to 45 rpm for 5 to 10 minutes. A nicotine concentrate was produced by lowering the stirring speed to 20 to 25 rpm and sterilizing at 82 ° C. for 30 minutes under reduced pressure of 0.05 MPa. Further stirring was performed at 25 rpm under reduced pressure. Anhydrous citric acid and fruit flavor were added, purified water was added, and the sugar content was corrected using agave syrup, followed by stirring.

The stirring speed was further reduced to 10 to 15 rpm and the temperature was maintained at 80° C. while filtering through 40 mesh. After transferring the filtrate to a service tank, nicotine jelly was prepared.

Example 2: Physicochemical properties of nicotine jelly

The nicotine jelly prepared through the manufacturing method of the present invention had a pH of 2 to 5 and a sugar content of Brix 30 to 70. More specifically, pH 2.58, identified as Brix 64.

Although the embodiments have been described as above, those skilled in the art may apply various technical modifications and variations based on the above. For example, the described techniques may be performed in an order different from the method described, and/or components of the described system, structure, device, circuit, etc. may be combined or combined in a different form than the method described, or other components may be used. Or even if it is replaced or substituted by equivalents, appropriate results can be achieved.

Therefore, other implementations, other embodiments, and equivalents of the claims are within the scope of the following claims.

Claims (16)

(1) adding and mixing nicotine and food gel HA;
(2) transferring the mixture of step (1) to a stirring tank and then warming it;
(3) after step (2), further adding at least one selected from the group consisting of fruit juice, vitamins, caffeine, and GABA to the stirring tank and then stirring;
(4) stirring and sterilizing under reduced pressure to produce a concentrate;
(5) further agitating the concentrate of step (4);
(6) lowering the stirring speed, filtering, and transferring to a service tank; and
(7) preparing jelly using the contents of the service tank in step (6);
Method for producing a nicotine jelly comprising.
According to claim 1,
In step (1), the food gel HA is dispersed so as not to clump, a method for producing nicotine jelly.
According to claim 1,
The step (1) is a method for producing nicotine jelly, characterized in that by adding and mixing 0.01 to 10 mg of nicotine and 0.001 to 10 mg of food gel HA.
According to claim 1,
The step (2) is a method for producing nicotine jelly, characterized in that warming to 80 to 90 ℃.
According to claim 1,
Step (2) is a method for producing nicotine jelly, characterized in that the mixture is transferred to a stirring tank, the sugar content is adjusted by adding fructooligosaccharide or ovarian-active maltodextrin, and then heated.
According to claim 1,
After step (2) and before step (3), a method for producing nicotine jelly, further comprising the step of mixing sodium citrate or calcium lactate in the stirring tank.
According to claim 1,
The step (3) is a method for producing nicotine jelly, characterized in that stirring at 40 to 50 rpm for 5 to 10 minutes.
According to claim 1,
The step (4) is a method for producing nicotine jelly, characterized in that stirring at 20 to 30 rpm under a reduced pressure of 0.01 to 1 MPa for 20 to 60 minutes at 80 to 90 ° C.
According to claim 1,
The step (5) is a method for producing nicotine jelly, characterized in that additional stirring at 20 to 30 rpm under reduced pressure.
According to claim 1,
After step (5) and before step (6), adding anhydrous citric acid or fruit flavor, administering purified water, and further comprising adjusting the sugar level using agave syrup, nicotine jelly Manufacturing method.
According to claim 1,
The step (6) is a method for producing nicotine jelly, characterized in that the filtering after stirring at 10 to 20 rpm at 75 to 85 ° C.
According to claim 1,
The step (6) is a method for producing nicotine jelly, characterized in that filtering with 30 to 50 mesh.
A nicotine jelly prepared by the method of any one of claims 1 to 12.
According to claim 13,
The nicotine jelly is pH 2 to 5, characterized in that the sugar content Brix 30 to 70, nicotine jelly.
According to claim 13,
The nicotine jelly is characterized in that the stick form, nicotine jelly.
According to claim 13,
The nicotine jelly includes nicotine 5-10%, food gel HA 1-2%, fructooligosaccharide 3-6%, ovarian active maltodextrin 1-5%, agave syrup 0.1-2%, sodium citrate 0.3-0.6%, lactic acid Calcium 0.3~0.6%, fruit juice 0.1~10%, vitamins, caffeine 0.1~10%, GABA 0.1~10%, anhydrous citric acid 0.05~0.5%, fruit flavor 0.05~0.5%, purified water 30~50% Characterized in that it is prepared by mixing, nicotine jelly.