KR20230036762A - Ethanol free cosmetic composition having matte felling - Google Patents
Ethanol free cosmetic composition having matte felling Download PDFInfo
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- KR20230036762A KR20230036762A KR1020210119620A KR20210119620A KR20230036762A KR 20230036762 A KR20230036762 A KR 20230036762A KR 1020210119620 A KR1020210119620 A KR 1020210119620A KR 20210119620 A KR20210119620 A KR 20210119620A KR 20230036762 A KR20230036762 A KR 20230036762A
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- cosmetic composition
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- ethanol
- polyol
- cellulose powder
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- 239000000203 mixture Substances 0.000 title claims abstract description 32
- 239000002537 cosmetic Substances 0.000 title claims abstract description 28
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 title claims abstract description 22
- 210000002374 sebum Anatomy 0.000 claims abstract description 17
- 230000000694 effects Effects 0.000 claims abstract description 16
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 20
- 229920005862 polyol Polymers 0.000 claims description 15
- 150000003077 polyols Chemical class 0.000 claims description 15
- 239000002562 thickening agent Substances 0.000 claims description 14
- 238000003756 stirring Methods 0.000 claims description 12
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 10
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 9
- 239000008346 aqueous phase Substances 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 235000011187 glycerol Nutrition 0.000 claims description 5
- 229920001495 poly(sodium acrylate) polymer Polymers 0.000 claims description 5
- 239000008213 purified water Substances 0.000 claims description 5
- NNMHYFLPFNGQFZ-UHFFFAOYSA-M sodium polyacrylate Chemical compound [Na+].[O-]C(=O)C=C NNMHYFLPFNGQFZ-UHFFFAOYSA-M 0.000 claims description 5
- 229920001577 copolymer Polymers 0.000 claims description 4
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 claims description 3
- OMIGHNLMNHATMP-UHFFFAOYSA-N 2-hydroxyethyl prop-2-enoate Chemical compound OCCOC(=O)C=C OMIGHNLMNHATMP-UHFFFAOYSA-N 0.000 claims description 3
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 3
- 229910019142 PO4 Inorganic materials 0.000 claims description 3
- 239000002202 Polyethylene glycol Substances 0.000 claims description 3
- 229920002125 Sokalan® Polymers 0.000 claims description 3
- NIXOWILDQLNWCW-UHFFFAOYSA-M acrylate group Chemical group C(C=C)(=O)[O-] NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 3
- 125000005250 alkyl acrylate group Chemical group 0.000 claims description 3
- BQMNFPBUAQPINY-UHFFFAOYSA-N azane;2-methyl-2-(prop-2-enoylamino)propane-1-sulfonic acid Chemical compound [NH4+].[O-]S(=O)(=O)CC(C)(C)NC(=O)C=C BQMNFPBUAQPINY-UHFFFAOYSA-N 0.000 claims description 3
- 229960001631 carbomer Drugs 0.000 claims description 3
- 239000001913 cellulose Substances 0.000 claims description 3
- 229920002678 cellulose Polymers 0.000 claims description 3
- 229920006037 cross link polymer Polymers 0.000 claims description 3
- SZXQTJUDPRGNJN-UHFFFAOYSA-N dipropylene glycol Chemical compound OCCCOCCCO SZXQTJUDPRGNJN-UHFFFAOYSA-N 0.000 claims description 3
- 239000001341 hydroxy propyl starch Substances 0.000 claims description 3
- 235000013828 hydroxypropyl starch Nutrition 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 239000002245 particle Substances 0.000 claims description 3
- 239000010452 phosphate Substances 0.000 claims description 3
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 3
- 229920001223 polyethylene glycol Polymers 0.000 claims description 3
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical compound CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 2
- 229910052708 sodium Inorganic materials 0.000 claims description 2
- 239000011734 sodium Substances 0.000 claims description 2
- 230000000052 comparative effect Effects 0.000 description 22
- 239000000843 powder Substances 0.000 description 7
- 238000011156 evaluation Methods 0.000 description 5
- 238000009472 formulation Methods 0.000 description 5
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
- 230000007794 irritation Effects 0.000 description 4
- 230000014759 maintenance of location Effects 0.000 description 4
- 239000004615 ingredient Substances 0.000 description 3
- 229940015975 1,2-hexanediol Drugs 0.000 description 2
- 229940048053 acrylate Drugs 0.000 description 2
- 239000000284 extract Substances 0.000 description 2
- FHKSXSQHXQEMOK-UHFFFAOYSA-N hexane-1,2-diol Chemical compound CCCCC(O)CO FHKSXSQHXQEMOK-UHFFFAOYSA-N 0.000 description 2
- 230000005923 long-lasting effect Effects 0.000 description 2
- 230000007774 longterm Effects 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- 238000004321 preservation Methods 0.000 description 2
- 239000000377 silicon dioxide Substances 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 229940104261 taurate Drugs 0.000 description 2
- PQUXFUBNSYCQAL-UHFFFAOYSA-N 1-(2,3-difluorophenyl)ethanone Chemical compound CC(=O)C1=CC=CC(F)=C1F PQUXFUBNSYCQAL-UHFFFAOYSA-N 0.000 description 1
- WTFUTSCZYYCBAY-SXBRIOAWSA-N 6-[(E)-C-[[4-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]piperazin-1-yl]methyl]-N-hydroxycarbonimidoyl]-3H-1,3-benzoxazol-2-one Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)N1CCN(CC1)C/C(=N/O)/C1=CC2=C(NC(O2)=O)C=C1 WTFUTSCZYYCBAY-SXBRIOAWSA-N 0.000 description 1
- 206010039792 Seborrhoea Diseases 0.000 description 1
- 206010040880 Skin irritation Diseases 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 239000002250 absorbent Substances 0.000 description 1
- 230000002745 absorbent Effects 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 239000003974 emollient agent Substances 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 230000037312 oily skin Effects 0.000 description 1
- 239000003002 pH adjusting agent Substances 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 230000037307 sensitive skin Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 229920002545 silicone oil Polymers 0.000 description 1
- 229920002379 silicone rubber Polymers 0.000 description 1
- 230000036556 skin irritation Effects 0.000 description 1
- 231100000475 skin irritation Toxicity 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 229940047670 sodium acrylate Drugs 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 239000000454 talc Substances 0.000 description 1
- 229910052623 talc Inorganic materials 0.000 description 1
Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/48—Thickener, Thickening system
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Emergency Medicine (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
Description
본 발명은 매트한 사용감의 화장료 조성물에 관한 것으로, 보다 구체적으로는 에탄올을 함유하지 않으면 끈적임이 없으며 피지 컨트롤 효과가 우수할 뿐만 아니라 메이크업 지속력도 유지시켜 주고 매트한 사용감을 갖는 에탄올 프리 화장료 조성물에 관한 것이다. The present invention relates to a cosmetic composition with a matte feeling of use, and more specifically, to an ethanol-free cosmetic composition that is non-sticky if it does not contain ethanol, has an excellent sebum control effect, maintains makeup durability, and has a matte feeling of use. will be.
최근 피지에 대한 관심이 늘어나면서 다양한 피지 케어 성분들이 출시되고 있다. 이러한 제품들은 피지 컨트롤 효능이 있는 추출물을 함유하거나 오일을 흡유하는 실리카 등의 파우더 성분을 함유하고 있다. 추출물 성분의 경우 즉각적인 효과를 보이기 어렵고, 실리카 등의 파우더는 광물 파우더 특유의 이물감이 있어 사용성이 좋지 않다. Recently, as interest in sebum has increased, various sebum care ingredients have been released. These products contain extracts with a sebum control effect or powder ingredients such as silica that absorb oil. In the case of extract components, it is difficult to show an immediate effect, and powders such as silica have a peculiar foreign body feeling, which is not good for usability.
또한, 피지 케어 제품들은 지성 피부들이 많이 선호하기 때문에 끈적임 없이 산뜻한 사용감을 나타내기 위해 에탄올 등의 휘발 성분을 함유하고 있다. 하지만 에탄올의 경우 피부 자극에 대한 이슈가 대두되고 있고 민감성 피부의 경우 선호하지 않는다. In addition, since sebum care products are preferred by oily skin, they contain volatile components such as ethanol to give a refreshing feeling without stickiness. However, in the case of ethanol, the issue of skin irritation is emerging, and it is not preferred in the case of sensitive skin.
따라서, 에탄올이 없으면서 끈적이지 않고 즉각적인 피지 컨트롤 효과가 있는 매트한 제품이 제공될 경우 소비자의 니즈를 충족하면서 새로운 타입의 제품군으로의 발전 가능성이 기대된다. Therefore, if a matte product that is non-sticky without ethanol and has an immediate sebum control effect is provided, the possibility of developing into a new type of product line is expected while satisfying consumer needs.
한국등록특허 제10-2177424호에서는 성형 안정성이 높은 매트 타입의 압축분말상의 화장료 조성물을 개시한다. 상기 화장료 조성물은 무기 분체, 메탈 소프 및 오일 바인더를 포함하고, 탈크와 계면활성제를 포함하지 않는 것을 특징으로 한다.Korean Patent Registration No. 10-2177424 discloses a cosmetic composition in the form of a compressed powder of a matte type having high molding stability. The cosmetic composition includes an inorganic powder, a metal soap, and an oil binder, and is characterized in that it does not contain talc and a surfactant.
한국등록특허 제10-2032115호에서는 유상에 실리콘 엘라스토머와 실리콘 오일을 포함하고, 수상에는 흡수성 파우더와 폴리올을 함유한 매트 타입 리퀴드 립을 개시한다.Korean Patent Registration No. 10-2032115 discloses a matte type liquid lip containing silicone elastomer and silicone oil in the oil phase and absorbent powder and polyol in the aqueous phase.
이에 본 발명자들은 끈적임 없이 피지 컨트롤 효과가 우수한 매트한 사용감의 에탄올 프리 제품을 개발하고자 하였다. 본 발명의 목적은 오일을 흡유하는 특성을 지닌 셀룰로오스 파우더를 함유하여 피지 컨트롤 효과는 물론 메이크업 지속력도 우수한 매트한 사용감의 에탄올 프리 화장료 조성물 및 그 제조방법을 제공하는 것이다. Accordingly, the inventors of the present invention attempted to develop an ethanol-free product with a matte feeling of use that has excellent sebum control effect without stickiness. An object of the present invention is to provide an ethanol-free cosmetic composition with a matte feeling of use and a method for producing the same, which contains cellulose powder having oil-absorbing properties and has excellent sebum control effect as well as long-lasting makeup.
상기 목적을 달성하기 위하여, 본 발명은 폴리올, 점증제 및 셀룰로오스 파우더를 포함하며, 에탄올을 포함하지 않고 즉각적인 피지 조절 효과를 갖는 화장료 조성물을 제공한다. In order to achieve the above object, the present invention provides a cosmetic composition comprising a polyol, a thickener and a cellulose powder, and having an immediate sebum control effect without containing ethanol.
바람직하게는 상기 화장료 조성물은 화장료 조성물 총 중량 대비 폴리올 0.1 중량% 내지 5.0 중량%, 점증제 0.1 중량% 내지 2.0 중량% 및 셀룰로오스 파우더 0.1 중량% 내지 2.0 중량%를 포함한다.Preferably, the cosmetic composition includes 0.1% to 5.0% by weight of a polyol, 0.1% to 2.0% by weight of a thickener, and 0.1% to 2.0% by weight of a cellulose powder, based on the total weight of the cosmetic composition.
또한 바람직하게는, 상기 폴리올은 글리세린, 부틸렌글리콜, 프로필렌글리콜, 디프로필렌글리콜, 폴리에틸렌글리콜 및 프로판디올로 이루어진 군으로부터 선택된 하나 이상일 수 있다.Also preferably, the polyol may be at least one selected from the group consisting of glycerin, butylene glycol, propylene glycol, dipropylene glycol, polyethylene glycol, and propanediol.
또한 바람직하게는, 상기 점증제는 아크릴레이트/C10-30알킬아크릴레이트크로스폴리머, 소듐 폴리아크릴레이트, 카보머, 암모늄아크릴로일디메칠타우레이트/브이피코폴리머, 하이드록시에칠아크릴레이트/소듐아크릴로일디메칠타우레이트코폴리머 및 하이드록시프로필스타치포스페이트로 이루어진 군으로부터 선택된 하나 이상일 수 있다.Also preferably, the thickener is acrylate/C10-30 alkyl acrylate crosspolymer, sodium polyacrylate, carbomer, ammonium acryloyldimethyltaurate/Vpicopolymer, hydroxyethyl acrylate/sodium acrylate It may be at least one selected from the group consisting of royl dimethyl taurate copolymer and hydroxypropyl starch phosphate.
또한 바람직하게는, 상기 셀룰로오스 파우더는 평균 30 μm의 입자 크기를 갖는 무정형 다공성 셀룰로오스일 수 있다.Also preferably, the cellulose powder may be amorphous porous cellulose having an average particle size of 30 μm.
또한, 본 발명의 목적은 실온의 정제수에 폴리올을 투입하고 아지믹서(Agi mixer)로 균일하게 교반시켜 수상을 제조하는 단계; 상기 수상에 아지믹서를 교반하면서 점증제를 투입하고 균일하게 분산시키는 단계; 및 상기 수상에 호모믹서를 교반하면서 셀룰로오스 파우더를 투입하고 균일하게 분산시키는 단계;를 포함하는 매트한 사용감의 에탄올 프리 화장료 조성물의 제조방법에 의해 달성된다.In addition, an object of the present invention is to prepare a water phase by adding a polyol to purified water at room temperature and uniformly stirring with an Agi mixer; Adding a thickening agent to the aqueous phase while stirring with an azimixer and uniformly dispersing it; It is achieved by a method for producing an ethanol-free cosmetic composition with a matte feeling of use including; and adding cellulose powder to the aqueous phase while stirring with a homomixer and uniformly dispersing it.
본 발명에 의한 매트한 사용감의 에탄올 프리 화장료 조성물은 끈적임이 없고 매트한 사용감을 가지며 에탄올이 함유되지 않아 피부에 마일드하다.The ethanol-free cosmetic composition having a matte feeling of use according to the present invention is non-sticky and has a matte feeling of use and is mild to the skin because it does not contain ethanol.
또한, 본 발명의 매트한 사용감의 에탄올 프리 화장료 조성물은 즉각적인 피지 컨트롤 효과는 물론 장시간 메이크업 지속력 효과를 제공한다. In addition, the ethanol-free cosmetic composition of the present invention having a matte feeling of use provides an immediate sebum control effect as well as a long-lasting makeup effect.
본 발명에서 사용되는 모든 기술용어는, 달리 정의되지 않는 이상, 하기의 정의를 가지며 본 발명의 관련 분야에서 통상의 당업자가 일반적으로 이해하는 바와 같은 의미에 부합된다. 또한 본 명세서에는 바람직한 방법이나 시료가 기재되나, 이와 유사하거나 동등한 것들도 본 발명의 범주에 포함된다.All technical terms used in the present invention, unless otherwise defined, have the following definitions and correspond to the meanings commonly understood by those of ordinary skill in the art related to the present invention. In addition, although preferred methods or samples are described in this specification, those similar or equivalent thereto are also included in the scope of the present invention.
용어 "약"이라는 것은 참조 양, 수준, 값, 수, 빈도, 퍼센트, 치수, 크기, 양, 중량 또는 길이에 대해 30, 25, 20, 15, 10, 9, 8, 7, 6, 5, 4, 3, 2 또는 1% 정도로 변하는 양, 수준, 값, 수, 빈도, 퍼센트, 치수, 크기, 양, 중량 또는 길이를 의미한다.The term "about" means a reference amount, level, value, number, frequency, percentage, dimension, size, amount, weight or length of 30, 25, 20, 15, 10, 9, 8, 7, 6, 5, means an amount, level, value, number, frequency, percentage, dimension, size, quantity, weight or length that varies by 4, 3, 2 or 1%.
본 명세서를 통해, 문맥에서 달리 필요하지 않으면, "포함하다" 및 "포함하는"이란 말은 제시된 단계 또는 구성요소, 또는 단계 또는 구성요소들의 군을 포함하나, 임의의 다른 단계 또는 구성요소, 또는 단계 또는 구성요소들의 군이 배제되지는 않음을 내포하는 것으로 이해하여야 한다.Throughout this specification, unless the context requires otherwise, the terms "comprise" and "comprising" include a given step or element, or group of steps or elements, but any other step or element, or It is to be understood that steps or groups of components are not excluded.
본 발명에 따른 매트한 사용감의 에탄올 프리 화장료 조성물은 폴리올, 점증제 및 셀룰로오스 파우더를 함유한다. The ethanol-free cosmetic composition having a matte feeling of use according to the present invention contains a polyol, a thickener, and a cellulose powder.
본 발명에서 사용되는 폴리올은 글리세린, 부틸렌글리콜, 프로필렌글리콜, 디프로필렌글리콜, 폴리에틸렌글리콜, 프로판디올 등의 다가 알코올 등일 수 있다. 폴리올은 화장료 조성물 총 중량에 대하여 0.1 내지 5 중량%로 포함되는 것이 바람직하다. 폴리올이 0.1 중량% 미만으로 포함되면 건조함을 느끼게 되며 5 중량%를 초과하면 폴리올 특유의 끈적한 사용감이 강하게 느껴져 적합하지 않다. Polyols used in the present invention may be polyhydric alcohols such as glycerin, butylene glycol, propylene glycol, dipropylene glycol, polyethylene glycol, and propanediol. Polyol is preferably included in 0.1 to 5% by weight based on the total weight of the cosmetic composition. If the polyol is included in less than 0.1% by weight, dryness is felt, and if it exceeds 5% by weight, a sticky feeling peculiar to polyol is strongly felt, which is not suitable.
본 발명에서 사용되는 점증제는 아크릴레이트/C10-30알킬아크릴레이트크로스폴리머, 소듐 폴리아크릴레이트, 카보머, 암모늄아크릴로일디메칠타우레이트/브이피코폴리머, 하이드록시에칠아크릴레이트/소듐아크릴로일디메칠타우레이트코폴리머, 하이드록시프로필스타치포스페이트 등일 수 있다. 상기 점증제는 화장료 조성물 총 중량에 대하여 0.1 내지 2 중량%를 함유한다. 점증제가 0.1 중량% 미만이면 점도가 형성되지 않아 제형이 형성되지 않고 셀룰로오스 파우더가 가라앉아 안정도에 영향을 줄 수 있으며 2 중량%를 초과하면 점도가 높아져 발림성이 좋지 않고 점증제 특유의 끈적임이 느껴져 적합하지 않다. The thickener used in the present invention is acrylate/C10-30 alkyl acrylate crosspolymer, sodium polyacrylate, carbomer, ammonium acryloyldimethyltaurate/Vpicopolymer, hydroxyethyl acrylate/sodium acrylo It may be 1 dimethyl taurate copolymer, hydroxypropyl starch phosphate, etc. The thickener contains 0.1 to 2% by weight based on the total weight of the cosmetic composition. If the thickener is less than 0.1% by weight, the viscosity is not formed, so the formulation is not formed, and the cellulose powder sinks, which may affect the stability. don't
본 발명에서 사용되는 셀룰로오스 파우더는 평균 30 μm의 입자 크기를 갖는 무정형 다공성 셀룰로오스이며 물에 분산되는 타입으로 총 중량에 대하여 0.1 내지 2 중량%를 함유한다. 0.1 중량% 미만이면 피지 컨트롤 효과가 없고 끈적임이 생기며 2 중량%를 초과하면 파우더 특유의 이물감이 생기고 흡수 후 밀리는 형상이 생겨 적합하지 않다. The cellulose powder used in the present invention is an amorphous porous cellulose having an average particle size of 30 μm and is a water-dispersible type and contains 0.1 to 2% by weight based on the total weight. If it is less than 0.1% by weight, there is no sebum control effect and stickiness occurs, and if it exceeds 2% by weight, a foreign body feeling peculiar to the powder occurs and a shape that is pushed after absorption is not suitable.
본 발명에 의한 매트한 사용감의 에탄올 프리 화장료 조성물은 하기의 방법으로 제조된다. The ethanol-free cosmetic composition having a matte feeling of use according to the present invention is prepared by the following method.
1) 실온의 정제수에 폴리올을 투입하고 아지믹서(Agi mixer)로 균일하게 교반시켜 수상을 제조한다(제 1단계). 1) Add polyol to purified water at room temperature and uniformly stir with an Agi mixer to prepare an aqueous phase (first step).
2) 상기 수상에 아지믹서를 교반하면서 점증제를 투입하고 균일하게 분산시킨다(제2 단계). 2) Add a thickening agent to the aqueous phase while stirring with an azimixer and uniformly disperse (second step).
3) 상기 수상에 호모믹서(Homo Mixer)를 교반하면서 셀룰로오스 파우더를 투입하고 10분 이상의 충분한 시간 동안 균일하게 분산시킨다. 이때 호모믹서를 교반하지 않은 상태로 셀룰로오스 파우더를 투입하거나 10분 이상의 충분한 시간으로 교반하지 않으면 셀룰로오스 파우더가 뭉쳐 균일한 제형을 형성시킬 수 없다(제3 단계).3) Add cellulose powder to the aqueous phase while stirring with a homomixer and uniformly disperse for a sufficient time of 10 minutes or more. At this time, if the cellulose powder is added without stirring in the homomixer or stirred for a sufficient time of 10 minutes or more, the cellulose powder is agglomerated and a uniform formulation cannot be formed (third step).
본 발명에 따른 화장료 조성물은 본 발명의 목적을 저해하지 않는 범위 내에서 가용화제, 안정화제, 에몰리언트, 향, 방부제, pH 조절제 등을 추가로 포함할 수 있다.The cosmetic composition according to the present invention may further include a solubilizer, a stabilizer, an emollient, a fragrance, a preservative, a pH adjuster, and the like within a range that does not impair the object of the present invention.
이하, 실시예를 통하여 본 발명을 보다 상세히 설명하지만, 본 발명의 범위가 반드시 이들 예에만 한정되는 것은 아니다.Hereinafter, the present invention will be described in more detail through examples, but the scope of the present invention is not necessarily limited only to these examples.
실시예 및 비교예Examples and Comparative Examples
하기 표 1의 성분과 함량비로 화장료 조성물을 제조하였다. 보다 구체적으로 실온의 정제수에 글리세린과 1,2-헥산다이올을 투입하여 용해시켰다. 소듐폴리아크릴레이트를 교반하면서 분산시키고, 호모믹서를 교반하면서 셀룰로오스 파우더를 투입하였다. 이때 호모믹서 속도는 3,500rpm으로 유지시켜 10분 이상의 충분한 시간 동안 고르게 교반시켰다. 단, 비교예 5는 호모믹서를 교반하지 않은 상태에서 셀룰로오스 파우더를 투입하고 호모믹서 속도를 3500rpm으로 유지시켜 3분 동안만 교반시켰다. A cosmetic composition was prepared with the components and content ratios shown in Table 1 below. More specifically, glycerin and 1,2-hexanediol were added to purified water at room temperature and dissolved. Sodium polyacrylate was dispersed while stirring, and cellulose powder was added while stirring in a homomixer. At this time, the speed of the homomixer was maintained at 3,500 rpm and evenly stirred for a sufficient time of 10 minutes or more. However, in Comparative Example 5, the cellulose powder was added while the homomixer was not stirred, and the homomixer speed was maintained at 3500 rpm and stirred only for 3 minutes.
실험예 1: 사용성 평가Experimental Example 1: Usability evaluation
20~30대의 여성 30명을 대상으로 실시예 1 및 비교예 1~5의 샘플을 얼굴에 사용하게 한 후 다음 평가 기준에 따라 끈적임, 자극감, 피지 컨트롤 효과 및 메이크업 유지력의 사용성을 평가하여 그 결과를 하기 표 2에 나타내었다. After having 30 women in their 20s and 30s use the samples of Example 1 and Comparative Examples 1-5 on their faces, the usability of stickiness, irritation, sebum control effect, and makeup retention was evaluated according to the following evaluation criteria, and the results are shown in Table 2 below.
[평가 기준] [Evaluation standard]
매우 우수함 - 5, 우수함 - 4, 보통 - 3, 나쁨 - 2, 매우 나쁨 - 1Excellent - 5, Excellent - 4, Fair - 3, Poor - 2, Very Poor - 1
상기 표 2에 나타낸 바와 같이, 실시예 1이끈적임과 자극이 없으면서 피지 컨트롤 효과와 메이크업 유지력이 우수하여 모든 항목에서 우수한 것으로 평가되었다. 비교예 1은 전반적으로 양호한 점수로 평가되었으나, 실시예 1 보다 건조하게 느껴져 자극으로 받아들이는 경향이 있었다. 비교예 2는 제형이 형성되지 않아 사용성을 평가하기가 어려웠고, 비교예 3은 셀룰로오스 파우더 성분이 없어 끈적임은 물론 효능 측면에서 전반적으로 매우 낮은 점수로 평가되었다. 비교예 4는 피지 컨트롤 효과와 메이크업 유지력이 전반적으로 높은 점수로 평가되었지만, 에탄올에서 오는 자극감이 강한 것으로 확인되었다. 비교예 5는 셀룰로오스 파우더가 고르게 분산되지 않아 사용성 평가가 어려웠고, 특히 파우더의 뭉침 현상으로 이물감이 느껴진다는 답변이 많았다. As shown in Table 2, Example 1 was evaluated as excellent in all items because it had excellent sebum control effect and makeup retention without stickiness and irritation. Comparative Example 1 was generally evaluated with good scores, but it felt drier than Example 1 and tended to be accepted as irritation. In Comparative Example 2, it was difficult to evaluate usability because the formulation was not formed, and in Comparative Example 3, since there was no cellulose powder component, it was evaluated as overall very low in terms of stickiness and efficacy. In Comparative Example 4, the sebum control effect and makeup retention were evaluated with high overall scores, but it was confirmed that the stimulation from ethanol was strong. In Comparative Example 5, it was difficult to evaluate the usability because the cellulose powder was not evenly dispersed, and in particular, many answered that a foreign body feeling was felt due to the agglomeration of the powder.
실험예 2: 제형 안정성 평가 Experimental Example 2: Formulation stability evaluation
상기에서 제조한 실시예 1 및 비교예 1 내지 5의 제형 안정성을 평가하였다.Formulation stability of Example 1 and Comparative Examples 1 to 5 prepared above was evaluated.
상기 화장료들에 대하여 4℃, 45℃, 50℃ 및 4℃-45℃ 사이클 (Cycle)의 항온조 및 실온에서 1주일, 1개월 및 3개월을 단위로 하여 장기 보전 안정성을 하기 표 3의 평가기준으로 평가하여 그 결과를 표 4에 나타내었다.For the above cosmetics, the long-term storage stability of 4 ℃, 45 ℃, 50 ℃ and 4 ℃ - 45 ℃ cycle (Cycle) in a constant temperature bath and room temperature in units of 1 week, 1 month and 3 months Evaluation criteria in Table 3 below It was evaluated and the results are shown in Table 4.
상기 표 4로부터, 본 발명에 의한 실시예 1은 장기 보관 안정성이 우수하게 나타났다. 비교예 2와 5를 제외한 나머지 비교예들도 안정도는 크게 이상이 없었다.From Table 4, Example 1 according to the present invention showed excellent long-term storage stability. Except for Comparative Examples 2 and 5, the stability of the other Comparative Examples was not significantly abnormal.
Claims (5)
상기 수상에 아지믹서를 교반하면서 점증제를 투입하고 균일하게 분산시키는 단계; 및
상기 수상에 호모믹서를 교반하면서 셀룰로오스 파우더를 투입하고 균일하게 분산시키는 단계;를 포함하고,
화장료 조성물 총 중량 대비 폴리올 0.1 중량% 내지 5.0 중량%, 점증제 0.1 중량% 내지 2.0 중량% 및 셀룰로오스 파우더 0.1 중량% 내지 2.0 중량%를 포함하는, 매트한 사용감의 에탄올 프리 화장료 조성물의 제조방법.Injecting polyol into purified water at room temperature and uniformly stirring with an Agi mixer to prepare an aqueous phase;
Adding a thickening agent to the aqueous phase while stirring with an azimixer and uniformly dispersing it; and
Including; adding cellulose powder to the aqueous phase while stirring with a homomixer and uniformly dispersing it;
0.1% to 5.0% by weight of polyol, 0.1% to 2.0% by weight of thickener and 0.1% to 2.0% by weight of cellulose powder, based on the total weight of the cosmetic composition, A method for producing an ethanol-free cosmetic composition with a matte feeling.
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