KR20220104503A - Viscoelastic soup composition and manufacturing method thereof - Google Patents

Viscoelastic soup composition and manufacturing method thereof Download PDF

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KR20220104503A
KR20220104503A KR1020210006898A KR20210006898A KR20220104503A KR 20220104503 A KR20220104503 A KR 20220104503A KR 1020210006898 A KR1020210006898 A KR 1020210006898A KR 20210006898 A KR20210006898 A KR 20210006898A KR 20220104503 A KR20220104503 A KR 20220104503A
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soap composition
viscoelastic
weight
mixing
oil
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Korean (ko)
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한봉숙
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한봉숙
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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/38—Products in which the composition is not well defined
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
    • C11D13/22—Cutting
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/225—Polymers
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/26—Organic compounds, e.g. vitamins containing oxygen
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/26—Organic compounds, e.g. vitamins containing oxygen
    • C11D9/265—Organic compounds, e.g. vitamins containing oxygen containing glycerol

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Seeds, Soups, And Other Foods (AREA)

Abstract

A method for producing a viscoelastic soap composition includes: a plant oil mixture preparation step of heating and maintaining a plant oil mixture containing 20 to 40 wt% of coconut oil, 20 to 40 wt% of palm oil, and 20 to 40 wt% of camellia oil at 35 to 50℃; a caustic soda aqueous solution preparation step of mixing 98% pure caustic soda with purified water in a sealed state to make a caustic soda aqueous solution, and then maintaining the same at 35 to 50℃; a first mixing step of mixing the plant oil mixture and the caustic soda aqueous solution in a wt% ratio of 67-69 to 31-33; a saponification step of stirring the mixture after the first mixing step at 30 to 45℃ to produce a liquid soap composition; a hard soap making step of sealing the liquid soap composition and maintaining the same for 12 to 24 hours to generate a viscoelastic soap composition; and a neutralization step of sealing and packaging the viscoelastic soap composition and maintaining the same for 2 to 3 weeks. The viscoelastic soap composition is suitable for health (especially skin health) as chemical additives are not added.

Description

점탄성 비누조성물 및 그 제조방법{VISCOELASTIC SOUP COMPOSITION AND MANUFACTURING METHOD THEREOF}Viscoelastic soap composition and manufacturing method thereof

본 발명은 점탄성 비누조성물 및 그 제조방법에 관한 것으로서, 특히 친환경적이고 건강에 이로우며 입체(3D) 성형성을 지닌 점탄성 비누조성물 및 그 제조방법에 관한 것이다.The present invention relates to a viscoelastic soap composition and a method for manufacturing the same, and more particularly, to a viscoelastic soap composition that is environmentally friendly, beneficial to health, and has three-dimensional (3D) moldability and a method for manufacturing the same.

점탄성(viscoelasticy)을 가진 비누조성물은 기존에 유아완구나 미술공예재료 등으로 사용되어 온 플라스틱제 점토완구나 액체괴물(slime)이라 불리는 점액질 완구를 천연재료로 유사하게 구현하여 대체제로 사용할 수 있도록 개발된 것이다.A soap composition with viscoelasticity is developed so that it can be used as a substitute for plastic clay toys or slime toys called liquid monsters, which have been used as infant toys and art craft materials, by implementing them as natural materials similarly. it has become

여기서 점탄성이란 점성과 탄성을 함께 지닌 성질을 말한다. 점탄성을 가진 물체는 액체와 고체의 중간 정도의 성질을 갖고 있어서 적절한 점성과 탄성에 의해 원하는 디자인으로 다양한 맞춤형 입체(3D) 성형이 가능하다는 특징을 갖고 있다.Here, viscoelasticity refers to the property of having both viscosity and elasticity. Objects with viscoelasticity have properties that are intermediate between liquid and solid, and have the characteristic that various customized three-dimensional (3D) molding is possible with a desired design by appropriate viscosity and elasticity.

이러한 점탄성 비누조성물은 비누로서 저자극 고보습의 세정효과와 함께 완구나 미술공예재료로서 적절한 점탄성을 가져야 함은 물론이고, 친환경적이고 건강(특히 피부건강)에 적합해야 한다는 과제를 안고 있다.Such a viscoelastic soap composition has the task of being environmentally friendly and suitable for health (especially skin health), as well as having appropriate viscoelasticity as a toy or art craft material with a mild, high moisturizing cleaning effect as a soap.

일반적으로 중화비누의 제조방법은 지방산과 알칼리금속염의 비누화반응으로 고온의 열반응으로 진행되는데, 건강에 이로운 아로마오일 성분이나 비타민 성분은 열에 약한 특성으로 인해 첨가하더라도 손실이 커서 제 효능을 발휘하기 어렵다는 문제점이 있다.In general, the manufacturing method of neutralized soap proceeds with a high-temperature thermal reaction due to the saponification reaction of fatty acids and alkali metal salts. There is a problem.

또한, 수산화칼륨(가성가리)으로 만드는 연비누의 경우에는 원하는 점탄성을 얻기 위해 전분과 경화제를 첨가해야 하는데, 전분은 비누의 보관기간에 영향을 주어 유통기한이 짧아진다는 문제점이 있고, 경화제와 같은 화학첨가제는 피부건강에 좋지 않다는 문제점이 있다.In addition, in the case of fuel silk soap made of potassium hydroxide (caustic calcium), starch and a curing agent must be added to obtain the desired viscoelasticity. There is a problem that chemical additives are not good for skin health.

또한, 일반적으로 널리 사용되는 수산화나트륨(가성소다)으로 만드는 경비누는 단단해서 입체 성형에 적합한 점탄성을 확보하기 어려운 것으로 알려져 있다.In addition, it is known that it is difficult to secure viscoelasticity suitable for three-dimensional molding because the nasal soap made of sodium hydroxide (caustic soda), which is generally widely used, is hard.

이와 관련된 선행기술의 예로는 대한민국 특허등록 제10-2136774호 "폴리비닐알코올과 붕사를 사용하지 않는 신축성, 점탄성, 연성을 가진 천연비누조성물"(이하 '선행기술 1이라 함')과 대한민국 특허등록 제10-1129474호 "재성형 기능을 갖는 피부저자극 공작용 비누클레이의 제조방법"(이하 '선행기술 2라 함')이 있다.Examples of related prior art include Korean Patent Registration No. 10-2136774 "Natural soap composition with elasticity, viscoelasticity, and ductility that does not use polyvinyl alcohol and borax" (hereinafter referred to as 'prior art 1') and Korean patent registration There is a No. 10-1129474 "Method for Producing Skin Hypoallergenic Soap Clay with Reshaping Function" (hereinafter referred to as 'Prior Art 2').

하지만, 선행기술 1은 전분에 더하여 계면활성제, 농도조절제, 산도조절제, 경화제와 같은 화학첨가물을 첨가함으로써 상술한 유통기한 문제나 피부건강 문제를 해결하기 어렵고, 선행기술 2는 수산화나트륨과 수산화칼륨을 함께 사용하는 번거로움과 70℃ 이상의 고온 비누화공정으로 인해 건강에 이로운 아로마오일 성분이나 비타민 성분을 첨가하기 어렵다는 단점이 있다.However, in Prior Art 1, it is difficult to solve the above-mentioned shelf life problem or skin health problem by adding chemical additives such as surfactant, concentration adjusting agent, acidity adjusting agent, and hardener in addition to starch, and Prior Art 2 is sodium hydroxide and potassium hydroxide. There are disadvantages in that it is difficult to add aromatic oil or vitamin components beneficial to health due to the inconvenience of using together and the high-temperature saponification process at 70°C or higher.

1. 대한민국 특허등록 제10-2136774호1. Korean Patent Registration No. 10-2136774 2. 대한민국 특허등록 제10-1129474호2. Korean Patent Registration No. 10-1129474

본 발명은 상술한 과제 및 선행기술의 문제점을 해결하기 위하여 창안된 것으로서, 식물오일 혼합물과 수산화나트륨 수용액을 사용하고 식물오일의 배합비율과 비누화 온도와 교반시간 관리를 통해 원하는 점탄성을 얻을 수 있는 점탄성 비누조성물 및 그 제조방법을 제공하는 것이다.The present invention has been devised to solve the above problems and problems of the prior art. Viscoelasticity that can obtain desired viscoelasticity by using a vegetable oil mixture and an aqueous sodium hydroxide solution and managing the mixing ratio of plant oil, saponification temperature, and stirring time To provide a soap composition and a method for manufacturing the same.

본 발명의 다른 목적은 화학첨가물을 첨가하지 않아 건강(특히 피부건강)에 적합한 점탄성 비누조성물 및 그 제조방법을 제공하는 것이다.Another object of the present invention is to provide a viscoelastic soap composition suitable for health (especially skin health) and a method for manufacturing the same without adding chemical additives.

본 발명의 또 다른 목적은 저온 비누화공정을 채택함으로써 건강에 이로운 아로마오일 성분이나 비타민 성분을 첨가할 수 있는 점탄성 비누조성물 및 그 제조방법을 제공하는 것이다.Another object of the present invention is to provide a viscoelastic soap composition and a method for producing the same, in which an aromatic oil component or vitamin component beneficial to health can be added by adopting a low-temperature saponification process.

상기 목적을 달성하기 위하여, 본 발명의 일 측면에 따른 점탄성 비누조성물의 제조방법은 코코넛유 20~40중량%, 팜유 20~40중량%, 동백유(카멜리아유) 20~40중량%를 포함하는 식물오일 혼합물을 35~50℃로 가열 및 유지하는 식물오일 혼합물 준비단계; 정제수에 순도 98% 가성소다를 밀봉상태로 혼합하여 가성소다수용액을 만든 후 35~50℃로 유지하는 가성소다수용액 준비단계; 상기 식물오일 혼합물과 상기 가성소다수용액을 67~69 대 31~33의 중량% 비율로 혼합하는 1차 혼합단계; 상기 1차 혼합단계를 거친 혼합물을 30~45℃에서 교반하여 액상의 비누조성물을 생성하는 비누화 단계; 상기 액상의 비누조성물을 밀봉하여 12~24시간 유지하여 점탄성 비누조성물을 생성하는 경비누화 단계; 및 상기 점탄성 비누조성물을 밀봉 포장하여 2~3주간 유지하는 중화단계;를 포함하는 것을 특징으로 한다.In order to achieve the above object, the method for producing a viscoelastic soap composition according to an aspect of the present invention is coconut oil 20-40% by weight, palm oil 20-40% by weight, Camellia oil (Camellia oil) 20-40% by weight Plant comprising Plant oil mixture preparation step of heating and maintaining the oil mixture at 35 ~ 50 ℃; A caustic soda solution preparation step of mixing purified water with 98% purity caustic soda in a sealed state to make an aqueous caustic soda solution, and then maintaining the temperature at 35-50°C; A first mixing step of mixing the vegetable oil mixture and the caustic soda solution in a weight % ratio of 67 to 69 to 31 to 33; a saponification step of stirring the mixture that has undergone the first mixing step at 30 to 45° C. to produce a liquid soap composition; a non-cross-talk step of sealing the liquid soap composition and maintaining it for 12 to 24 hours to produce a viscoelastic soap composition; and a neutralization step of sealingly packaging the viscoelastic soap composition and maintaining it for 2-3 weeks.

상기 식물오일 혼합물은 해바라기씨유 10.5~15중량%를 더 포함할 수 있다.The plant oil mixture may further include 10.5 to 15% by weight of sunflower seed oil.

본 제조방법은 상기 경비누화 단계와 상기 중화단계 사이에, 상기 경비누화 단계를 거친 비누조성물을 소정의 형태 및 크기로 커팅하는 커팅 단계;를 더 포함하는 것이 바람직하다.Preferably, the manufacturing method further includes, between the non-crosstalk step and the neutralization step, a cutting step of cutting the soap composition that has undergone the non-crosstalk step to a predetermined shape and size.

본 제조방법은 상기 중화단계를 거친 비누조성물을 공기에 노출되지 않도록 포장하는 단계;를 더 포함하는 것이 바람직하다.Preferably, the method further comprises a step of packaging the soap composition that has undergone the neutralization step so as not to be exposed to air.

본 제조방법은 상기 1차 혼합단계를 거친 혼합물 100중량%에 대하여 라벤더 및 유칼립투스 중 적어도 어느 하나를 포함하는 아로마오일 0.5~1.0중량%와, 지용성비타민 0.5~2.0중량%와, 수용성비타민 0.5~2.0중량% 중 적어도 어느 하나를 혼합하는 2차 혼합단계;를 더 포함하는 것이 바람직하다.The present manufacturing method includes 0.5 to 1.0% by weight of an aroma oil containing at least one of lavender and eucalyptus, 0.5 to 2.0% by weight of fat-soluble vitamins, and 0.5 to 2.0% by weight of water-soluble vitamins with respect to 100% by weight of the mixture that has undergone the first mixing step It is preferable to further include; a secondary mixing step of mixing at least any one of weight %.

상기 지용성비타민은 비타민E이고, 상기 수용성비타민은 비타민B5인 것이 바람직하다.Preferably, the fat-soluble vitamin is vitamin E, and the water-soluble vitamin is vitamin B5.

본 발명의 다른 측면에 따른 점탄성 비누조성물은 상술한 제조방법에 의하여 제조된 점탄성 비누조성물로서, 자연적으로 생성된 글리세롤 15중량%를 포함하는 것을 특징으로 한다.The viscoelastic soap composition according to another aspect of the present invention is a viscoelastic soap composition prepared by the above-described manufacturing method, characterized in that it contains 15% by weight of naturally occurring glycerol.

본 발명에 따르면, 식물오일 혼합물에 수산화나트륨 수용액만을 사용하면서도 식물오일의 배합비율, 비누화 온도, 교반시간을 관리함으로써 자유로운 입체(3D) 성형성을 지닌 점탄성 비누조성물 및 그 제조방법을 제공할 수 있다.According to the present invention, it is possible to provide a viscoelastic soap composition having free three-dimensional (3D) moldability and a manufacturing method thereof by controlling the mixing ratio of plant oil, saponification temperature, and stirring time while using only an aqueous sodium hydroxide solution in a vegetable oil mixture. .

또한, 점탄성을 얻기 위한 화학첨가물을 첨가하지 않음으로써 건강(특히 피부건강)에 적합한 점탄성 비누조성물 및 그 제조방법을 제공할 수 있다.In addition, it is possible to provide a viscoelastic soap composition suitable for health (especially skin health) and a manufacturing method thereof by not adding chemical additives for obtaining viscoelasticity.

또한, 저온 비누화공정을 채택함으로써 건강에 이로운 아로마오일 성분이나 비타민 성분을 첨가할 수 있는 점탄성 비누조성물 및 그 제조방법을 제공할 수 있다.In addition, by adopting a low-temperature saponification process, it is possible to provide a viscoelastic soap composition and a method for producing the same, in which an aromatic oil component or vitamin component beneficial to health can be added.

상술한 본 발명의 효과 및 기타 효과는 후술하는 실시예를 통해 보다 명확하게 이해될 수 있을 것이다.The above-described effects and other effects of the present invention will be more clearly understood through the following examples.

본 발명은 도면을 참조하여 구체적으로 설명되지만, 도면은 본 발명의 예시적인 실시예를 나타낸 것이므로, 본 발명의 기술사상이 도면에만 한정되어 해석되어서는 아니 된다.
도 1은 본 발명의 실시예에 따른 점탄성 비누조성물의 제조방법을 설명하기 위한 순서도이다.The present invention will be described in detail with reference to the drawings, but the drawings show exemplary embodiments of the present invention, and thus the technical spirit of the present invention should not be construed as being limited only to the drawings.
1 is a flowchart for explaining a method of manufacturing a viscoelastic soap composition according to an embodiment of the present invention.

이하, 첨부된 도면을 참조하여 본 발명의 바람직한 실시예에 따른 점탄성 비누조성물 및 그 제조방법을 상세히 설명한다.Hereinafter, a viscoelastic soap composition and a manufacturing method thereof according to a preferred embodiment of the present invention will be described in detail with reference to the accompanying drawings.

도 1은 본 발명의 일 실시예에 따른 점탄성 비누조성물의 제조방법을 설명하기 위한 순서도이다.1 is a flowchart for explaining a method of manufacturing a viscoelastic soap composition according to an embodiment of the present invention.

도 1에 도시된 바와 같이, 본 실시예에 따른 점탄성 비누조성물의 제조방법은 식물오일 혼합물 준비단계(S1)와, 알칼리수용액 준비단계(S2)와, 1차 혼합단계(S3)와, 2차 혼합단계(S4)와, 비누화 단계(S5)와, 경비누화 단계(S6)와, 커팅 단계(S7)와, 중화단계(S8)와, 포장단계(S9)를 포함하여 이루어진다.As shown in FIG. 1, the method for preparing a viscoelastic soap composition according to this embodiment includes a plant oil mixture preparation step (S1), an alkaline aqueous solution preparation step (S2), a first mixing step (S3), and a second A mixing step (S4), a saponification step (S5), a non-crosstalk step (S6), a cutting step (S7), a neutralization step (S8), and a packing step (S9) are included.

식물오일 혼합물 준비단계(S1)는 식물오일 혼합물을 50℃ 이하로 가열하여 유지하는 단계이다.The plant oil mixture preparation step (S1) is a step of heating and maintaining the plant oil mixture at 50° C. or less.

식물오일 혼합물은 카멜리아유(동백유) 20~40중량%, 코코넛유 20~40중량%, 팜유 20~40중량%를 포함하여 이루어지며, 이에 더하여 해바라기씨유 10.5~15중량%를 더 포함할 수 있다.The plant oil mixture is made of 20 to 40% by weight of camellia oil (camellia oil), 20 to 40% by weight of coconut oil, and 20 to 40% by weight of palm oil, and may further include 10.5 to 15% by weight of sunflower seed oil. have.

가열 및 유지온도는 35~50℃인 것이 바람직하다. 온도를 50℃ 이하로 하는 이유는 온도가 높을수록 비누화반응의 속도가 빨라져서 탄성이 높은 단단한 경비누로 진행되기 쉬우므로 적절한 점탄성(입체 성형성)을 지닌 비누를 얻기 어렵기 때문이고, 또한 비누화가 진행되지 못한 채 젤화되거나 경화되는 불량율이 높아지기 때문이다. 또한, 열에 약한 식물오일의 유효성분들의 손실을 막기 위한 것이기도 하다. 온도를 35℃ 이상으로 하는 이유는 온도가 오일성분들의 녹는점보다 낮으면 식물오일 혼합물이 액체상태가 아닌 고체상태가 되어 비누화반응이 일어날 수 없기 때문이다. 이 단계는 히터를 장착한 교반기에 식물오일 혼합물을 투입한 후 상기한 온도범위에서 가열함으로써 이루어질 수도 있고, 일반 금속용기에 식물오일 혼합물을 담고 일반 전열기구로 가열함으로써 이루어질 수도 있다.The heating and holding temperature is preferably 35 to 50 °C. The reason that the temperature is set to 50° C. or less is that the higher the temperature, the faster the rate of the saponification reaction, so it is easy to proceed with a hard soap with high elasticity, so it is difficult to obtain a soap with appropriate viscoelasticity (stereoformability). This is because the defect rate that gels or hardens without progressing increases. In addition, it is also to prevent the loss of the active ingredients of the plant oil, which is weak to heat. The reason for setting the temperature to 35°C or higher is that, when the temperature is lower than the melting point of the oil components, the plant oil mixture becomes a solid state rather than a liquid state, so that the saponification reaction cannot occur. This step may be made by putting the plant oil mixture into a stirrer equipped with a heater and then heating it in the above temperature range, or it may be made by placing the plant oil mixture in a general metal container and heating it with a general electric heating device.

알칼리수용액 준비단계(S2)는 상온의 정제수에 순도 98% 가성소다(수산화나트륨: NaOH)을 밀봉상태로 혼합하여 가성소다수용액을 만든 후 50℃ 이하로 유지하는 단계이다.The alkaline aqueous solution preparation step (S2) is a step of mixing 98% pure caustic soda (sodium hydroxide: NaOH) with purified water at room temperature in a sealed state to make an aqueous caustic soda solution and then maintaining it at 50° C. or less.

가성소다수용액의 농도는 25~35%인 것이 바람직하다.The concentration of the aqueous caustic soda solution is preferably 25 to 35%.

가성소다와 물이 만나면 순간적으로 열이 발생하여 약 95℃까지 온도가 올라가므로 약 20~30분 간 온도가 내려오기를 기다린 다음(가성소다수용액을 만들 때 차가운 정제수를 사용하거나 얼음을 함께 사용하면 냉각시간을 줄일 수 있음), 상술한 식물오일 혼합물 준비단계(S1)의 온도와 비슷한 온도인 35~50℃로 유지하는 것이 바람직하다. 온도범위를 이렇게 설정한 것은 비누화반응의 속도를 늦추기 위함이고, 원하는 점탄성을 얻기 위함이다.When caustic soda and water meet, heat is instantaneously generated and the temperature rises to about 95°C, so wait for the temperature to drop for about 20-30 minutes (if you use cold purified water or use ice to make caustic soda solution) It is possible to reduce the cooling time), it is preferable to maintain the temperature at 35 ~ 50 ℃ similar to the temperature of the above-described plant oil mixture preparation step (S1). The temperature range was set in this way to slow down the saponification reaction and to obtain desired viscoelasticity.

또한, 가성소다와 물이 만나면 유독가스가 나오므로 밀봉 가능한 비닐 지퍼백 안에 가성소다수용액을 만들 계량용기를 넣고 정제수를 먼저 부은 다음 가성소다를 천천히 넣고 비닐 지퍼백을 잘 밀봉한 후 미리 넣어둔 저어주기용 도구로 섞으면서 녹인다.Also, when caustic soda and water meet, toxic gas is released, so put a measuring container to make caustic soda solution in a sealable plastic zipper bag, pour purified water first, then slowly add caustic soda, seal the plastic zipper bag well, and stir Melt while mixing with a tool.

1차 혼합단계(S3)는 식물오일 혼합물 준비단계(S1)에서 준비된 식물오일 혼합물에 알칼리수용액 준비단계(S2)에서 준비된 가성소다수용액을 투입하여 혼합하는 단계이다.The first mixing step (S3) is a step of mixing the caustic soda solution prepared in the alkaline aqueous solution preparation step (S2) into the plant oil mixture prepared in the plant oil mixture preparation step (S1) and mixing.

식물오일 혼합물과 가성소다수용액의 비율은 중량%로 67~69 대 31~33인 것이 바람직하다.The ratio of the vegetable oil mixture and the aqueous caustic soda solution is preferably 67 to 69 to 31 to 33 by weight.

1차 혼합단계(S3)는 식물오일 혼합물 준비단계(S1)와 마찬가지로 35~50℃에서 이루어지는 것이 바람직하다. 온도범위를 이렇게 설정한 것은 식물오일 혼합물 준비단계(S1)에서 설명한 바와 같다. 이 단계의 혼합은 1분 이내의 짧은 시간에 신속하게 이루어진다.The first mixing step (S3) is preferably made at 35 ~ 50 ℃ like the plant oil mixture preparation step (S1). Setting the temperature range in this way is the same as described in the plant oil mixture preparation step (S1). This step of mixing is done quickly and in a short time of less than 1 minute.

2차 혼합단계(S4)는 1차 혼합단계(S3)에서 생성된 1차 혼합물(식물오일 혼합물와 가성소다수용액의 혼합물)에 아로마오일 성분과 비타민 성분 중 적어도 어느 하나를 혼합하는 단계이다.The second mixing step (S4) is a step of mixing at least one of an aroma oil component and a vitamin component in the first mixture (a mixture of a vegetable oil mixture and a caustic soda solution) generated in the first mixing step (S3).

아로마오일 성분은 향기치료용으로 진정효과를 지닌 라벤더와 호흡기 개선효과를 지닌 유칼립투스 중 적어도 어느 하나를 포함할 수 있고, 필요에 따라 로즈마리, 카모마일, 티트리와 같은 다른 성분을 더 포함할 수 있다. 아로마오일 성분의 총 함량은 아로마오일의 농도가 100%일 때 혼합물 100중량%에 대해 0.5~1.5중량%인 것이 바람직하다.The aroma oil component may include at least one of lavender having a calming effect and eucalyptus having a respiratory improving effect for aroma therapy, and may further include other ingredients such as rosemary, chamomile, and tea tree, if necessary. The total content of the aroma oil component is preferably 0.5 to 1.5% by weight based on 100% by weight of the mixture when the concentration of the aroma oil is 100%.

비타민 성분은 지용성비타민과 수용성비타민 중 적어도 어느 하나를 포함할 수 있다. 지용성비타민은 비타민E인 것이 바람직하고, 수용성비타민은 비타민B5인 것이 바람직하다. 지용성비타민과 수용성비타민의 각 함량은 1차 혼합물 100중량%에 대해 0.5~2.0중량%인 것이 바람직하다.The vitamin component may include at least one of fat-soluble vitamins and water-soluble vitamins. The fat-soluble vitamin is preferably vitamin E, and the water-soluble vitamin is preferably vitamin B5. Each content of fat-soluble vitamins and water-soluble vitamins is preferably 0.5 to 2.0% by weight based on 100% by weight of the primary mixture.

배경기술에서 설명한 바와 같이, 아로마오일 성분이나 비타민 성분은 열에 약한 성질을 갖고 있어서 고온 비누화공정에서는 첨가하기 어려웠으나, 본 발명은 50℃ 이하의 저온 비누화공정을 채택함으로써 필요에 따라 건강(특히 피부건강)에 이로운 다양한 아로마오일 성분이나 비타민 성분을 선택하여 자유롭게 첨가할 수 있다.As described in the background art, aroma oil components or vitamin components have weak properties to heat, so it is difficult to add them in a high-temperature saponification process. ) can be added freely by selecting various aromatic oil components or vitamin components that are beneficial to

2차 혼합단계(S4)는 건강을 고려하여 선택적으로 행해지는 단계이고 완제품의 점탄성에 영향을 미치지 않으므로, 생략하더라도 본 발명의 범위에서 벗어나지 않는다.The secondary mixing step (S4) is a step performed selectively in consideration of health and does not affect the viscoelasticity of the finished product, so even if omitted, it does not depart from the scope of the present invention.

비누화 단계(S5)는 2차 혼합단계(S4)에서 생성된 2차 혼합물을 30~45℃에서 교반하는 단계이다. 2차 혼합단계(S4)를 생략하는 경우에는 1차 혼합단계(S3)에서 생성된 1차 혼합물을 교반하게 된다. 교반은 10~30분 간격으로 1분 정도 교반하면서 2~3시간 진행되는 것이 바람직하다.The saponification step (S5) is a step of stirring the secondary mixture produced in the secondary mixing step (S4) at 30 ~ 45 ℃. When the secondary mixing step (S4) is omitted, the primary mixture generated in the primary mixing step (S3) is stirred. Stirring is preferably performed for 2 to 3 hours while stirring for about 1 minute at intervals of 10 to 30 minutes.

이 단계를 거치면 액상의 비누 혼합물이 생성되고, 이 비누 혼합물은 자연 발생적으로 생성된 글리세롤을 함유하게 된다. 이 경우 글리세롤의 함량은 15중량% 정도가 된다. 글리세롤은 완성된 비누에서 피부보습의 역할을 한다.This step produces a liquid soap mixture, which contains naturally occurring glycerol. In this case, the content of glycerol is about 15% by weight. Glycerol plays the role of moisturizing the skin in the finished soap.

경비누화 단계(S6)는 비누화 단계(S5)에서 생성된 액상의 비누 혼합물을 밀봉하여 일정 시간 유지하여 원하는 점탄성을 지닌 비누를 생성하는 단계이다.The non-cross-talk step (S6) is a step of sealing the liquid soap mixture generated in the saponification step (S5) and maintaining it for a certain period of time to produce a soap having desired viscoelasticity.

경비누화 시간은 온도와 습도에 따라 달라지나 12~24시간인 것이 바람직하다. 밀봉은 비닐 지퍼백에 보관하여 행하는 것이 바람직하다. 이 단계를 거치면 본 발명이 의도하는 적절한 점성과 탄성을 함께 지닌 비누조성물, 즉 점탄성 비누조성물이 생성된다.The non-crosstalk time varies depending on temperature and humidity, but is preferably 12 to 24 hours. It is preferable to keep it sealed in a plastic zipper bag. Through this step, a soap composition having appropriate viscosity and elasticity intended by the present invention, that is, a viscoelastic soap composition is produced.

커팅 단계(S7)는 경비누화 단계(S6)를 거친 점탄성 비누조성물을 일정한 형태 및 커팅하는 단계이다.The cutting step (S7) is a step of cutting and forming the viscoelastic soap composition that has undergone the non-crosstalk step (S6).

중화단계(S8)는 커팅 단계(S7)에서 커팅된 점탄성 비누조성물을 밀봉 포장하여 일정 기간 유지함으로써 자연 중화하는 단계이다.The neutralization step (S8) is a step of natural neutralization by sealing the viscoelastic soap composition cut in the cutting step (S7) and maintaining it for a certain period of time.

중화기간은 2~3주인 것이 바람직하다. 밀봉은 밀봉 가능한 비닐 지퍼백에 수용하여 행하는 것이 바람직하다.The neutralization period is preferably 2-3 weeks. Sealing is preferably performed by being accommodated in a sealable plastic zipper bag.

이 단계를 거치면 pH7.0~8.5의 점탄성 비누조성물이 생성된다.Through this step, a viscoelastic soap composition with a pH of 7.0 to 8.5 is produced.

포장단계(S9)는 중화단계(S8)를 거친 점탄성 비누조성물 제품을 포장하는 단계이다.The packaging step (S9) is a step of packaging the viscoelastic soap composition product that has undergone the neutralization step (S8).

포장은 점탄성 비누조성물이 공기에 노출되어 수분이 손실되지 않도록 하기 위한 것이다. 이 포장상태에서 포장을 개봉하면, 점탄성 비누조성물은 상온에서 자연 건조되어 약 12~48시간 후에 경비누로 경화된다. 따라서 경화되기 전에는 완구나 미술공예재료로서 사용할 수 있고, 경화된 후에는 일반 경비누로서 사용할 수 있다. 이러한 이중의 효과는 가성소다수용액만을 사용하고 식물오일 혼합물의 배합비율, 비누화 온도, 교반시간을 관리함으로써 얻어지는 효과이다.Packaging is intended to prevent moisture loss due to exposure of the viscoelastic soap composition to air. When the package is opened in this packaging state, the viscoelastic soap composition is naturally dried at room temperature and cured with a soft soap after about 12 to 48 hours. Therefore, before hardening, it can be used as a toy or art craft material, and after hardening, it can be used as a general soap cloth. This double effect is obtained by using only the caustic soda solution and controlling the mixing ratio of the vegetable oil mixture, the saponification temperature, and the stirring time.

이상에서 본 발명을 실시예들과 첨부된 도면을 통해 구체적으로 설명하였으나, 본 발명의 기술적 사상은 특허청구범위에 기재된 사항에 의해 정해지는 것이며, 본 발명의 기술적 사상을 벗어나지 않는 범위 내에서 다양한 변형예와 균등예가 있을 수 있다.Although the present invention has been described in detail with reference to embodiments and the accompanying drawings in the above, the technical spirit of the present invention is defined by the matters described in the claims, and various modifications are made without departing from the technical spirit of the present invention. There may be examples and equivalent examples.

Claims (7)

코코넛유 20~40중량%, 팜유 20~40중량%, 동백유(카멜리아유) 20~40중량%를 포함하는 식물오일 혼합물을 35~50℃로 가열 및 유지하는 식물오일 혼합물 준비단계;
정제수에 순도 98% 가성소다를 밀봉상태로 혼합하여 가성소다수용액을 만든 후 35~50℃로 유지하는 가성소다수용액 준비단계;
상기 식물오일 혼합물과 상기 가성소다수용액을 67~69 대 31~33의 중량% 비율로 혼합하는 1차 혼합단계;
상기 1차 혼합단계를 거친 혼합물을 30~45℃에서 교반하여 액상의 비누조성물을 생성하는 비누화 단계;
상기 액상의 비누조성물을 밀봉하여 12~24시간 유지하여 점탄성 비누조성물을 생성하는 경비누화 단계; 및
상기 점탄성 비누조성물을 밀봉 포장하여 2~3주간 유지하는 중화단계;를 포함하는 것을 특징으로 하는 점탄성 비누조성물의 제조방법.Coconut oil 20-40% by weight, palm oil 20-40% by weight, plant oil mixture preparation step of heating and maintaining a plant oil mixture containing 20-40% by weight of camellia oil (camellia oil) to 35-50 ℃;
A caustic soda solution preparation step of mixing purified water with 98% purity caustic soda in a sealed state to make an aqueous caustic soda solution, and then maintaining the temperature at 35-50°C;
A first mixing step of mixing the vegetable oil mixture and the caustic soda solution in a weight % ratio of 67 to 69 to 31 to 33;
a saponification step of stirring the mixture that has undergone the first mixing step at 30 to 45° C. to produce a liquid soap composition;
a non-cross-talk step of sealing the liquid soap composition and maintaining it for 12 to 24 hours to produce a viscoelastic soap composition; and
A method for producing a viscoelastic soap composition, comprising: a neutralization step of sealing the viscoelastic soap composition and maintaining it for 2 to 3 weeks. 제1항에 있어서,
상기 식물오일 혼합물은 해바라기씨유 10.5~15중량%를 더 포함하는 것을 특징으로 하는 점탄성 비누조성물의 제조방법.According to claim 1,
The plant oil mixture is a method for producing a viscoelastic soap composition, characterized in that it further comprises 10.5 to 15% by weight of sunflower seed oil. 제2항에 있어서,
상기 경비누화 단계와 상기 중화단계 사이에, 상기 경비누화 단계를 거친 비누조성물을 소정의 형태 및 크기로 커팅하는 커팅 단계;를 더 포함하는 것을 특징으로 하는 점탄성 비누조성물의 제조방법.3. The method of claim 2,
Between the non-crosstalk step and the neutralization step, a cutting step of cutting the soap composition that has undergone the non-crosstalk step to a predetermined shape and size; 제3항에 있어서,
상기 중화단계를 거친 비누조성물을 공기에 노출되지 않도록 포장하는 단계;를 더 포함하는 것을 특징으로 하는 점탄성 비누조성물의 제조방법.4. The method of claim 3,
Packaging the soap composition that has undergone the neutralization step so as not to be exposed to air; 제4항에 있어서,
상기 1차 혼합단계를 거친 혼합물 100중량%에 대하여 라벤더 및 유칼립투스 중 적어도 어느 하나를 포함하는 아로마오일 0.5~1.0중량%와, 지용성비타민 0.5~2.0중량%와, 수용성비타민 0.5~2.0중량% 중 적어도 어느 하나를 혼합하는 2차 혼합단계;를 더 포함하는 것을 특징으로 하는 점탄성 비누조성물의 제조방법.5. The method of claim 4,
With respect to 100% by weight of the mixture that has undergone the first mixing step, at least 0.5 to 1.0% by weight of an aroma oil containing at least one of lavender and eucalyptus, 0.5 to 2.0% by weight of fat-soluble vitamins, and 0.5 to 2.0% by weight of water-soluble vitamins A method for producing a viscoelastic soap composition further comprising; a secondary mixing step of mixing any one. 제5항에 있어서,
상기 지용성비타민은 비타민E이고, 상기 수용성비타민은 비타민B5인 것을 특징으로 하는 점탄성 비누조성물의 제조방법.6. The method of claim 5,
The fat-soluble vitamin is vitamin E, and the water-soluble vitamin is vitamin B5. 제1항 내지 제6항 중 어느 한 항의 방법으로 제조된 점탄성 비누조성물로서,
자연적으로 생성된 글리세롤 15중량%를 포함하는 것을 특징으로 하는 점탄성 비누조성물.As a viscoelastic soap composition prepared by the method of any one of claims 1 to 6,
A viscoelastic soap composition comprising 15% by weight of naturally occurring glycerol.
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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101129474B1 (en) 2009-07-20 2012-03-28 서울대학교산학협력단 Olfactory sensor for increasing olfactory reaction and method for increasing olfactory reaction using thereof
KR102136774B1 (en) 2020-02-17 2020-07-22 손지민 Natural soup composition with the effect of elasticity, viscoelasticity and ductility, without polyvinyl alcohol and borax

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101129474B1 (en) 2009-07-20 2012-03-28 서울대학교산학협력단 Olfactory sensor for increasing olfactory reaction and method for increasing olfactory reaction using thereof
KR102136774B1 (en) 2020-02-17 2020-07-22 손지민 Natural soup composition with the effect of elasticity, viscoelasticity and ductility, without polyvinyl alcohol and borax

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