KR20210095832A - A method for producing inorganic salt crystals by burning rice bran by direct burning - Google Patents

A method for producing inorganic salt crystals by burning rice bran by direct burning Download PDF

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KR20210095832A
KR20210095832A KR1020210098016A KR20210098016A KR20210095832A KR 20210095832 A KR20210095832 A KR 20210095832A KR 1020210098016 A KR1020210098016 A KR 1020210098016A KR 20210098016 A KR20210098016 A KR 20210098016A KR 20210095832 A KR20210095832 A KR 20210095832A
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rice bran
inorganic salt
direct
molding
salt crystals
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김광수
김찬승
한상국
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주식회사 엘앤더블유
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    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01FCOMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F5/00Compounds of magnesium
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/30Active carbon
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    • C01B32/318Preparation characterised by the starting materials

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Abstract

The present invention relates to a method for producing inorganic salt crystals through the direct combustion of rice bran, including the steps of: agitating rice bran powder with water to prepare a plurality of circular molded rice bran products, introducing the molded rice bran products into a direct combustion container, carrying out first direct heating with a heating means to carbonize the black-colored molded rice bran products into dark brown-colored molded rice bran products, and carrying out first cooling; carrying out second direct heating so that the dark brown-colored molded rice bran products may be molten into purple-colored molded rice bran products, and carrying out second cooling; carrying out third direct heating so that the molten purple-colored molded rice bran products may be molten into cobalt-colored inorganic salt, and carrying out third cooling to produce inorganic salt crystals. In this manner, it is possible to reduce the time required for producing inorganic salt crystals through the direct combustion of rice bran powder, and to obtain eco-friendly inorganic salt crystals by removing agricultural chemicals contained in rice bran. In addition, the inorganic salt crystals can be mixed with purified water so that it may be used as cosmetic water, makeup water, sterilizing water, a medical aid, a fertilizer additive, or the like, and as a deodorizing agent, bad odor diffusion-interrupting agent, fertilizer additive, agricultural chemical-decomposing agent, flame retardant, or the like.

Description

쌀겨를 직화연소시켜 무기염류결정체를 생성하는 제조방법{A method for producing inorganic salt crystals by burning rice bran by direct burning}A manufacturing method for producing inorganic salt crystals by direct burning of rice bran {A method for producing inorganic salt crystals by burning rice bran by direct burning}

본 발명은 쌀겨를 직화연소시켜 무기염류결정체를 생성하는 제조방법에 관한 것으로서, 더욱 상세하게는, 쌀겨분말을 직화연소시켜 무기염류결정체를로 생성제조하는 시간을 단축시키고, 쌀겨에 함유된 농약성분이 제거되어 친환경적인 무기염류결정체를를 얻을 수 있으며, 이러한 무기염류결정체를를 정제수와 혼합하여 미용수, 화장수, 살균수, 의료보조재, 비료첨가제 등과 악취제거 및 악취확산차단제와, 비료첨가제, 농약분해제, 난연제로 사용하도록 한 쌀겨를 직화연소시켜 무기염류결정체를 생성하는 제조방법에 관한 것이다.The present invention relates to a method for producing inorganic salt crystals by direct fire burning of rice bran, and more particularly, to shorten the time for producing and manufacturing inorganic salt crystals by direct fire burning of rice bran powder, and pesticide components contained in rice bran This can be removed to obtain eco-friendly inorganic salt crystals, and by mixing these inorganic salt crystals with purified water, odor removal and odor diffusion blocking agents, fertilizer additives, pesticide decomposers, etc. , It relates to a manufacturing method for producing inorganic salt crystals by direct combustion of rice bran to be used as a flame retardant.

일반적으로 쌀겨의 활용에 대해 살펴보면, 현미의 무게비율 6∼8%의 쌀겨가 생기는데, 현미의 도정도(搗精度)를 높이면 그 양이 증가되고, 또 도정도에 따라서 그 성분도 달라진다In general, looking at the use of rice bran, rice bran with a weight ratio of 6 to 8% of brown rice is produced. If the degree of milling of brown rice is increased, the amount increases, and the composition also changes depending on the degree of milling.

그리고 도정도가 높아지면 현미의 내층에 포함된 성분이 다량 포함되어 지방, 비타민 B1,인(燐)이 증가하고 섬유는 감소된다.And when the degree of grinding increases, the inner layer of brown rice contains a large amount of fat, vitamin B1, phosphorus, and fiber decreases.

그리고 쌀겨의 표준 화학조성은 수분 13.5%, 단백질 13.2%, 지방 18.3%, 당질 38.3%, 섬유 7.8%, 회분(灰分)8.9%이다.The standard chemical composition of rice bran is water 13.5%, protein 13.2%, fat 18.3%, sugar 38.3%, fiber 7.8%, and ash 8.9%.

그리고 쌀겨는 대부분이 사료나 비료로 사용되며, 유지원료(油脂原料)로서 쌀겨기름을 짜는 데도 이용되고, 쌀겨는 저장 중 변질되기 쉬우며 기온이 높고 습도가 클 때는 더욱 심한데, 이는 쌀겨에 함유되어 있는 리파아제(lipase)의 작용이 강하여 지방의 산값(酸價)이 높아지기 때문이다.Most of the rice bran is used as feed or fertilizer, and it is also used to squeeze rice bran oil as a raw material for oil and fat. This is because the acid value of fat is increased due to the strong action of lipase.

종래의 소성기술에 대해 살펴보면, 광물 처리 가공공업에서 널리 사용되는 고온처리의 한 방식으로서 소성 목적에는 열분해, 합성, 치환 등의 화학 반응, 소결 등을 들 수 있고, 이러한 소성과정은 형성하려는 광물질 이외의 불순물을 제거하고 용융된 물질 내부에서 열에 의한 화학반응을 통해 얻고자 하는 물질을 합성, 소결한다.Looking at the conventional calcination technology, as a method of high-temperature treatment widely used in the mineral processing industry, the purpose of calcination may include chemical reactions such as thermal decomposition, synthesis, substitution, sintering, etc., and this calcination process is It removes impurities from the molten material and synthesizes and sinters the material to be obtained through a chemical reaction by heat inside the molten material.

그러나, 쌀겨를 종래의 상기 소성기술에 적용하면 쌀겨를 종래의 상기 소성기술로 고온의 온도에서 진행하여 탄화된 쌀겨소성물을 얻기 위해서는 많은 장치로 이루어지고 이를 이용하여 얻어지는 탄화된 쌀겨소성물은 많은 시간을 들여 질좋은 탄화된 쌀겨소성물을 얻는데 많은 어려운 문제점이 있었다.However, when rice bran is applied to the conventional calcination technology, in order to obtain a carbonized rice bran calcined product by proceeding the rice bran at a high temperature with the conventional calcining technique, many devices are used, and the carbonized rice bran calcined product obtained using this is made of many There were many difficult problems in obtaining a good quality carbonized rice bran calcined product with time.

또한, 본 발명처럼 쌀겨분말을 물과 교반하여 원형의 쌀겨성형물을 다수개로 준비하여 직화용기의 내부에 수용하고 가열수단으로 1차 직화가열하여 쌀겨성형물이 검은색에서 진갈색으로 탄화시켜 1차냉각한 후, 진갈색의 쌀겨성형물을 보라색으로 용융되게 2차직화가열하고 2차냉각한 후, 보라색의 용융된 쌀겨성형물을 코발트색으로 용융시켜 무기염류로 생성되게 3차 직화가열하고 3차냉각하여서 얻은 무기염류결정체를를 생성하여 쌀겨분말을 직화연소시켜 무기염류결정체를로 생성제조하는 시간을 단축시키고, 쌀겨에 함유된 농약성분이 제거되어 친환경적인 무기염류결정체를를 얻을 수 있으며, 이러한 무기염류결정체를를 정제수와 혼합하여 미용수, 화장수, 살균수 이러한 무기염류결정체를를 정제수와 혼합하여 미용수, 화장수, 살균수 의료보조재, 비료첨가제 등과 난연제와 악취제거 및 악취확산차단제와 비료첨가제, 농약분해제로 사용하도록 한 쌀겨를 직화연소시켜 무기염류결정체를 생성하는 제조방법이 제공되지 못한 문제점이 있었다.In addition, as in the present invention, rice bran powder is stirred with water to prepare a plurality of circular rice bran moldings, accommodated in a direct fire container, and primary direct heating is performed using a heating means to carbonize the rice bran moldings from black to dark brown and first cooling. After that, the dark brown rice bran molding is heated by secondary direct heating to melt purple and secondary cooled, and then the purple molten rice bran molding is melted in cobalt color to produce inorganic salts. Inorganic obtained by direct heating and tertiary cooling By producing salt crystals and direct combustion of rice bran powder, the time for producing and manufacturing inorganic salt crystals is shortened, and pesticides contained in rice bran are removed to obtain eco-friendly inorganic salt crystals, and these inorganic salt crystals are mixed with purified water Rice bran made by mixing these inorganic salt crystals with purified water to be used as cosmetic water, lotion, sterilization water, medical aid, fertilizer additive, etc., flame retardant, odor removal, odor diffusion blocker, fertilizer additive, and pesticide decomposer. There was a problem in that a manufacturing method for producing inorganic salt crystals by direct fire combustion was not provided.

상기와 같은 문제점을 해결하기 위해서, 본 발명은 쌀겨분말을 물과 교반하여 원형의 쌀겨성형물을 다수개로 준비하여 직화용기의 내부에 수용하고 가열수단으로 1차 직화가열하여 쌀겨성형물을 검은색에서 진갈색으로 탄화시켜 1차냉각한후, 진갈색의 쌀겨성형물을 보라색으로 용융되게 2차직화가열하고 2차냉각한 후, 보라색의 용융된 쌀겨성형물을 코발트색으로 용융시켜 무기염류로 생성되게 3차 직화가열하고 3차냉각하여서 얻은 무기염류결정체를를 생성하여 쌀겨분말을 직화연소시켜 무기염류결정체를로 생성제조하는 시간을 단축시키고, 쌀겨에 함유된 농약성분이 제거되어 친환경적인 무기염류결정체를를 얻을 수 있으며, 이러한 무기염류결정체를를 정제수와 혼합하여 미용수, 화장수, 살균수, 의료보조재, 비료첨가제 등과 난연제와 악취제거 및 악취확산차단제와 비료첨가제, 농약분해제로 사용하도록 한 새로운 쌀겨를 직화연소시켜 무기염류결정체를 생성하는 제조방법을 제공하는데 그 목적이 있다.In order to solve the above problems, the present invention prepares a plurality of circular rice bran moldings by stirring rice bran powder with water, accommodates them in a direct fire container, and first directs heating with a heating means to change the rice bran moldings from black to dark brown After primary cooling by carbonization, the dark brown rice bran molding is heated by secondary direct heating to melt purple, and then cooled, then the purple molten rice bran molding is melted in cobalt color to produce inorganic salts by tertiary direct heating and produce inorganic salt crystals obtained by tertiary cooling, direct fire burning of rice bran powder to shorten the production time to produce inorganic salt crystals, and remove pesticides contained in rice bran to obtain eco-friendly inorganic salt crystals, By mixing these inorganic salt crystals with purified water, new rice bran, which is used as beauty water, lotion, sterilization water, medical aid, fertilizer additive, etc., as a flame retardant, odor removal, odor diffusion blocker, fertilizer additive, and pesticide decomposer, is directly burned to form inorganic salt crystals. An object of the present invention is to provide a manufacturing method for producing

이와 같은 목적을 달성하기 위해서, 본 발명에 따른 제조방법은 쌀겨분말에 물을 투입하고 교반기로 교반하여 쌀겨교반물을 생성하는 쌀겨교반물을 생성하는 단계(s100)와; 상기 쌀겨교반물을 원형의 형상으로 성형하여 쌀겨성형물로 다수개로 준비하는 쌀겨성형물을 성형하는 단계(s110)와; 상기 쌀겨성형물을 직화용기에 투입하고, 상기 쌀겨성형물을 가열수단으로 직접적으로 1차로 가열시켜 상기 쌀겨성형물을 검은색에서 진갈색으로 탄화시키는 쌀겨성형물에 1차 직화연소하는 단계(s120)와: 1차 직화연소시켜 생성된 쌀겨성형물을 1차로 냉각하는 쌀겨성형물 1차냉각단계(s130)와; 1차 냉각된 상기 쌀겨성형물을 가열수단으로 직접적으로 2차로 가열시켜 상기 쌀겨성형물이 보라색으로 용융되게 하는 쌀겨성형물에 2차 직화연소하는 단계(s140)와; 2차 직화연소시켜 용융된 쌀겨성형물을 2차로 냉각하는 쌀겨성형물 2차냉각단계(s150)와; 2차 냉각되어 용융된 상기 쌀겨성형물을 가열수단으로 직접적으로 3차로 가열시켜 용융된 쌀겨성형물이 코발트색으로 용융되어 상기 쌀겨성형물이 용융되어 최종적으로 무기염류로 생성되는 무기염류로 생성되게 3차 직화연소하는 단계(s160)와; 3차 직화연소시켜 용융된 무기염류를 3차로 냉각하여 무기염류결정체를로 생성되게 무기염류 3차냉각단계(s170)로 구성되는 것을 특징으로 한다.In order to achieve this object, the manufacturing method according to the present invention includes the steps of generating a rice bran stirred product to produce a rice bran stir by adding water to the rice bran powder and stirring with a stirrer (s100); Forming the rice bran agitated product into a circular shape to form a rice bran molding prepared in a plurality of rice bran moldings (s110); Putting the rice bran molded product into a direct fire container, and first directly heating the rice bran molded product with a heating means to carbonize the rice bran molded product from black to dark brown. First direct fire burning (s120) and: 1st A rice bran molding primary cooling step (s130) of primarily cooling the rice bran molding produced by direct fire combustion; Directly secondarily heating the firstly cooled rice bran molded product with a heating means to directly burn the rice bran molded product for a second time so that the rice bran molded product is melted in purple (s140); A secondary cooling step (s150) of the rice bran molded product secondary cooling the molten rice bran molded product by secondary direct fire combustion; The secondly cooled and molten rice bran molding is directly heated tertiarily with a heating means so that the molten rice bran molding is melted in cobalt color and the rice bran molding is melted to finally produce inorganic salts produced as inorganic salts. burning (s160); It is characterized in that it is composed of a tertiary cooling step (s170) of inorganic salts to produce inorganic salt crystals by tertiary cooling of the molten inorganic salts by tertiary direct fire combustion.

또한, 상기 쌀겨성형물에 다수개 통공을 형성하는 것을 특징으로 한다.In addition, it is characterized in that a plurality of through-holes are formed in the rice bran molding.

또한, 상기 쌀겨성형물에 1차 직화연소하는 단계의 가열온도는 400℃~600℃로 1~2시간 직화가열하고, 상기 쌀겨성형물에 2차 직화연소하는 단계의 가열온도는 400℃~600℃로 30~60분 직화가열하고, 무기염류로 생성되게 3차 직화연소하는 단계의 가열온도는 400℃~600℃로 1~2시간 직화가열하는 것을 특징으로 한다.In addition, the heating temperature of the first direct fire burning in the rice bran molding is 400 ° C to 600 ° C for 1 to 2 hours, and the heating temperature of the second direct fire burning to the rice bran molding is 400 ° C to 600 ° C. It is characterized by direct heating for 30 to 60 minutes, and direct heating for 1 to 2 hours at a heating temperature of 400 ° C to 600 ° C in the step of tertiary direct fire to produce inorganic salts.

또한, 상기 쌀겨교반물은 쌀겨분말 100중량부에 물 30중량부가 투입되어 교반되는 것을 특징으로 한다.In addition, the rice bran stirred product is characterized in that 30 parts by weight of water is added to 100 parts by weight of rice bran powder and stirred.

또한, 상기 쌀겨성형물에 2차 직화연소하는 단계에 송풍기를 구비하여 연소하는 것을 특징으로 한다.In addition, it is characterized in that the combustion is provided with a blower in the step of direct fire secondary combustion in the rice bran molding.

본 발명은 쌀겨분말을 물과 교반하여 원형의 쌀겨성형물을 다수개로 준비하여 직화용기의 내부에 수용하고 가열수단으로 1차 직화가열하여 쌀겨성형물이 검은색에서 진갈색으로 탄화시켜 1차냉각한 후, 진갈색의 쌀겨성형물을 보라색으로 용융되게 2차직화가열하고 2차냉각한 후, 보라색의 용융된 쌀겨성형물을 코발트색으로 용융시켜 무기염류로 생성되게 3차 직화가열하고 3차냉각하여서 얻은 무기염류결정체를를 생성하여 쌀겨분말을 직화연소시켜 무기염류결정체를로 생성제조하는 시간을 단축시키고, 쌀겨에 함유된 농약성분이 제거되어 친환경적인 무기염류결정체를를 얻을 수 있으며, 이러한 무기염류결정체를를 정제수와 혼합하여 미용수, 화장수, 살균수 의료보조재, 비료첨가제 등과 난연제와 악취제거 및 악취확산차단제와 비료첨가제, 농약분해제로 사용하는 효과가 있다.The present invention prepares a plurality of circular rice bran moldings by stirring rice bran powder with water, accommodates them in a direct fire container, and first directs heating with a heating means to carbonize the rice bran moldings from black to dark brown. Inorganic salt crystals obtained by secondary direct heating and secondary cooling of dark brown rice bran moldings to melt them in purple, and then tertiary direct heating and tertiary cooling to melt purple molten rice bran moldings in cobalt color to produce inorganic salts. It reduces the time to produce and manufacture inorganic salt crystals by direct combustion of rice bran powder by producing It has the effect of being used as a cosmetic water, lotion, sterilizing water, medical aid, fertilizer additive, etc., as a flame retardant, odor removal, odor diffusion blocker, fertilizer additive, and pesticide decomposing agent.

도 1은 본 발명에 따른 제조방법에 대한 개략도.1 is a schematic view of a manufacturing method according to the present invention.

본 발명을 충분히 이해하기 위해서 본 발명의 바람직한 실시예를 첨부 도면을 참조하여 설명한다.In order to fully understand the present invention, preferred embodiments of the present invention will be described with reference to the accompanying drawings.

본 발명의 실시예는 여러가지 형태로 변형될 수 있으며, 본 발명의 범위가 아래에서 상세히 설명하는 실시예로 한정되는 것으로 해석되어서는 안 된다. 본 실시예는 당업계에서 평균적인 지식을 가진 자에게 본 발명을 보다 안전하게 설명하기 위하여 제공되는 것이다.Embodiments of the present invention may be modified in various forms, and the scope of the present invention should not be construed as being limited to the embodiments described in detail below. This embodiment is provided to more safely explain the present invention to those of ordinary skill in the art.

따라서 도면에서의 요소의 형상 등은 보다 명확한 설명을 강조하기 위해서 과장되어 표현될 수 있다. 각 도면에서 동일한 부재는 동일한 참조부호로 도시한 경우가 있음을 유의하여야 한다.Accordingly, the shape of elements in the drawings may be exaggerated to emphasize a clearer description. It should be noted that the same members in each drawing are sometimes shown with the same reference numerals.

도 1은 본 발명에 따른 제조방법에 대한 개략도.1 is a schematic view of a manufacturing method according to the present invention.

본 발명에 따른 쌀겨를 직화연소시켜 무기염류로 생성하는 제조방법은 도 1을 참고하여 실시예를 들어 설명하면 다음과 같다.The manufacturing method for producing inorganic salts by direct combustion of rice bran according to the present invention will be described with reference to FIG. 1 by way of example.

[실시예][Example]

[쌀겨교반물을 생성하는 단계(s100)][Step of producing a rice bran stirred (s100)]

생산일자가 오래되지 않은 쌀겨분말을 준비하여 선별기를 통해 불순물을 제거하여 준다.Prepare rice bran powder whose production date is not old and remove impurities through a sorter.

이러한 상기 쌀겨분말에 물을 투입하고 교반기로 일정 시간 동안 교반하여 쌀겨교반물을 생성하여 준다.Water is added to the rice bran powder and stirred for a certain time with a stirrer to produce a rice bran stirred product.

상기와 같은 상기 쌀겨교반물은 쌀겨분말 100중량부에 물 25~35중량부가 투입되어 교반되는 것이 바람직하다.The rice bran stirred as described above is preferably stirred by adding 25 to 35 parts by weight of water to 100 parts by weight of rice bran powder.

쌀겨분말을 성형하기 위하여 쌀겨분말에 물을 투입하는 것으로 쌀겨분말의 건조상태에 따라 물을 투입하는 양을 다르게 하는 것으로 도정 후 오래되어 쌀겨분말의 건조가 많이 되었을 시는 물을 35중량부를 넣고 건조가 적은 경우에는 25중량부를 넣는다. Water is added to the rice bran powder to form the rice bran powder. The amount of water to be added varies according to the dry state of the rice bran powder. If there is little, add 25 parts by weight.

물을 35중량부 이상으로 많이 투입하는 경우에는 쌀겨분말의 성형은 용이하나 쌀겨성형물에 공간이 형성되지 않고 물을 많이 함유하고 있어 쌀겨분말성형물의 1차직화연소시간이 많이 소요되고 물을 35중량부를 투입하는 경우에는 물이 적게 투입되어 쌀겨분말이 뭉쳐지지 않아 쌀겨성형물이 형성되지 않거나 뭉쳐진 쌀겨성형물이 쉬게 부서져 쌀겨성형물을 연소하는데 1차직화연소시간을 필요로 하거나 연소되지 않게 된다.In the case of adding more than 35 parts by weight of water, the molding of rice bran powder is easy, but there is no space formed in the rice bran molding and contains a lot of water. In the case of adding wealth, little water is added and the rice bran powder is not agglomerated, so the rice bran molded product is not formed, or the agglomerated rice bran molded product is easily broken so that the first direct combustion time is required to burn the rice bran molding, or it does not burn.

따라서 쌀겨교반물 100중량부에 물 25~35중량부가 투입되게 하는 것이 좋다.Therefore, it is preferable to add 25 to 35 parts by weight of water to 100 parts by weight of the rice bran stirred.

[쌀겨성형물을 성형하는 단계(s110)][Step of molding the rice bran molding (s110)]

상기 쌀겨교반물을 작업자가 두 손으로 한 손 안에 넣을 수 있는 크기로 원형의 형상으로 성형하여 쌀겨성형물로 다수개로 준비하여 준다.The rice bran stirred product is molded into a circular shape to a size that the operator can put in one hand with both hands, and prepares a plurality of rice bran moldings.

벼를 도정한 쌀겨는 분말이므로 열을 가해도 쌀겨를 연소하는 시간이 많이 소요되므로 쌀겨분말을 쌀겨성형물로 만들어 사용한다. Since rice bran that has been polished is a powder, it takes a lot of time to burn the bran even when heat is applied.

상기 쌀겨성형물의 크기는 한정하지 않는다.The size of the rice bran molding is not limited.

다만 쌀겨성형물의 크기가 너무 큰 경우에는 1차직화연소시간이 많이 소요되므로 두 손으로 한 손 안에 넣을 수 있는 주먹크기로 만들어 사용하는 것이 좋다.However, if the size of the rice bran molding is too large, it takes a lot of time for the first direct fire, so it is better to make it into a fist size that can be put in one hand with two hands.

쌀겨성형물의 성형은 힘을 가해 단단히 덩어리로 만들지 않고 쌀겨분말이 뭉쳐진 후에 부서지지 않은 정로도 만든다.The molding of the rice bran molding is not made into a solid lump by applying force, but is also made into an unbroken dough after the rice bran powder is agglomerated.

이와 같이 쌀겨분말이 뭉쳐진 후에 부서지지 않은 정도로 성형하는 것은 쌀겨성형물을 단단히 뭉쳐 성형하는 쌀겨성형물에는 미세한 공간이 없어 쌀겨성형물에 1차직화열이 전달되는 것을 방해하여 쌀겨성형물을 1차연소시간이 많이 소요하게 된다.In this way, forming the rice bran powder to such a degree that it is not broken after agglomeration of the rice bran molding does not have a fine space in the rice bran molding, which is tightly agglomerated and molded, and thus prevents the primary direct heat heat from being transmitted to the rice bran molding, and the primary combustion of the rice bran molding takes a lot of time. will do

또한, 상기 쌀겨성형물에 다수개 통공을 형성하여 준다.In addition, a plurality of through holes are formed in the rice bran molding.

상기와 같이, 상기 쌀겨성형물에 다수개 통공을 형성하는 것은, 상기 쌀겨성형물을 가열수단으로 직화로 가열 시 상기 쌀겨성형물이 상기 통공들을 통해 보다 용이하고 신속하게 열 소성되게 하기 위함이다.As described above, the formation of a plurality of through holes in the rice bran molding is to allow the rice bran molding to be more easily and quickly thermally fired through the through holes when the rice bran molding is heated by direct fire with a heating means.

[쌀겨성형물에 1차 직화연소하는 단계(s120)][Step of primary direct fire burning in the rice bran molding (s120)]

상기 쌀겨성형물을 직화용기에 투입하여 준다.The rice bran molding is put into a direct fire container.

상기 쌀겨성형물은 직화용기의 내부에 하부에서 상부로 피라미드형상으로 쌓아서 수용하는 것이 바람직하다.The rice bran molding is preferably stacked and accommodated in a pyramid shape from the bottom to the top inside the direct fire container.

이렇게 직화용기의 내부에 수용된 상기 쌀겨성형물들에 가열수단으로 직접적으로 1차로 가열시켜 상기 쌀겨성형물에 함유된 불순물과 유기물성분을 제거하여 상기 쌀겨성형물을 검은색에서 진갈색으로 탄화시켜준다.In this way, the rice bran moldings accommodated in the direct fire container are directly heated with a heating means to first remove impurities and organic components contained in the rice bran moldings, thereby carbonizing the rice bran moldings from black to dark brown.

이때, 상기 쌀겨성형물에 1차 직화연소하는 단계의 가열온도는 400℃~600℃로 1∼2시간 직화가열하는 것이 바람직하다.At this time, it is preferable that the heating temperature of the step of primary direct fire burning in the rice bran molding is direct heating at 400° C. to 600° C. for 1 to 2 hours.

가열온도는 400℃이하인 경우에는 불순물과 유기물성분을 제거하는 시간이 많이 소요되고 600℃이상인 경우에는 급격히 온도를 가해지므로 불순물과 유기물성분을 제거되면서 무기물도 같이 손실되어 무기염류결정체를의 양이 작아지므로 쌀겨성형물에 1차 직화연소하는 단계의 가열온도는 400℃~600℃에서 실시하는 것이 좋다. When the heating temperature is less than 400℃, it takes a lot of time to remove impurities and organic substances, and when it is more than 600℃, the temperature is rapidly applied. Therefore, it is recommended that the heating temperature of the first direct fire burning in the rice bran molding be carried out at 400°C to 600°C.

직화시간이 1시간 이하인 경우에는 쌀겨에 함유된 불순물과 유기물성분을 제거가 불충분하고 2시간 이상하는 경우에는 쌀겨에 함유된 불순물과 유기물성분 제거는 좋으나 연소하는데 많은 시간이 소비되므로 1차 직화연소하는 시간은 1∼2시간 직화가열하는 것이 바람직하다.If the direct fire time is less than 1 hour, it is insufficient to remove impurities and organic components contained in the rice bran. The time is preferably 1 to 2 hours by direct heating.

〔쌀겨성형물 1차냉각단계(s130)][Rice bran molding primary cooling step (s130)]

1차 직화연소시켜 생성된 쌀겨성형물을 1차로 냉각하여 준다.The rice bran molded product produced by primary direct fire combustion is first cooled.

상기 쌀겨성형물은 상온의 그늘에서 일정 시간 냉각시켜 준다.The rice bran molding is cooled for a certain time in the shade of room temperature.

[쌀겨성형물에 2차 직화연소하는 단계(s140)][Step of direct fire burning in the rice bran molding (s140)]

1차 냉각된 상기 쌀겨성형물을 가열수단으로 직접적으로 2차로 가열시켜 상기 쌀겨성형물에 함유된 불순물과 유기물성분을 제거하여 상기 쌀겨성형물이 보라색으로 용융되게 하여 준다.The firstly cooled rice bran molded product is directly heated with a second heating means to remove impurities and organic components contained in the rice bran molded product, so that the rice bran molded product is melted in purple.

또한, 상기 쌀겨성형물에 2차 직화연소하는 단계의 가열온도는 400℃~600℃로 30분 직화가열하여준다.In addition, the heating temperature of the second direct fire burning in the rice bran molding is 400 ℃ ~ 600 ℃ direct heating for 30 minutes.

그리고 상기 쌀겨성형물에 2차 직화연소하는 단계에 송풍기를 구비하여 연소하여 준다.And a blower is provided in the step of secondary direct fire combustion in the rice bran molded product and combusted.

상기와 같이, 상기 쌀겨성형물에 2차 직화연소하는 단계에 송풍기를 구비하는 것은 상기 쌀겨성형물이 1차 탄화물에서 2차로 가열연소시켜 생성되는 상기 쌀겨성형물의 용융물에 상기 쌀겨성형물의 탄화재가 섞이지 않게 탄화재를 직화용기의 외부로 배출하여 순수한 상기 쌀겨성형물이 소성되어 얻어지는 용융물을 얻기 위함이다.As described above, the provision of a blower in the step of secondary direct fire burning in the rice bran molding is to prevent the char of the rice bran molding from being mixed with the melt of the rice bran molding produced by secondary heating and combustion of the rice bran molding in the primary carbide. This is to obtain a melt obtained by discharging the carbonized material to the outside of the direct fire container and firing the pure rice bran molding.

[쌀겨성형물 2차냉각단계(s150)][Rice bran molding secondary cooling step (s150)]

2차 직화연소시켜 용융된 쌀겨성형물을 2차로 냉각하여 준다.Secondary direct fire combustion gives the melted rice bran molding a second cooling.

상기 쌀겨성형물은 상온의 그늘에서 일정시간 냉각시켜 준다.The rice bran molding is cooled for a certain time in the shade of room temperature.

[무기염류로 생성되게 3차 직화연소하는 단계(s160)][Step of tertiary direct fire combustion to produce inorganic salts (s160)]

2차 냉각되어 용융된 상기 쌀겨성형물을 가열수단으로 직접적으로 3차로 가열시켜 용융된 쌀겨성형물이 코발트색으로 용융되어 상기 쌀겨성형물이 용융되어 최종적으로 무기염류로 생성되는 무기염류로 생성되게 하여준다.The secondly cooled and molten rice bran molded product is directly heated tertiarily with a heating means to melt the molten rice bran molded product in cobalt color so that the rice bran molded product is melted to finally produce inorganic salts produced as inorganic salts.

또한, 무기염류로 생성되게 3차 직화연소하는 단계의 가열온도는 400℃~600℃로 1 내지 2시간 직화가열하는 것이 바람직하다.In addition, it is preferable that the heating temperature of the third direct fire combustion step to be generated into inorganic salts is 400° C. to 600° C. for 1 to 2 hours.

[무기염류결정체를로 생성되게 무기염류 3차냉각단계(s170)][Inorganic salt tertiary cooling step (s170) to produce inorganic salt crystals]

3차 직화연소시켜 용융된 무기염류를 3차로 냉각하여 무기염류결정체를로 생성되게 하여준다.The tertiary direct fire burns the molten inorganic salts to the tertiary cooling to form inorganic salt crystals.

용융상태의 무기염류를 상온의 그늘에서 일정시간 냉각시켜 무기염류결정체를로 생성하여 준다.Inorganic salt crystals are produced by cooling the molten inorganic salts in the shade of room temperature for a certain period of time.

한편, 코발트색을 구비한 상기 무기염류결정체를를 정제수가 수용된 용기에 투입하고 난 다음에 상온에서 일정 기간 햇빛에 노출시켜 상기 무기염류결정체를가 정제수와 반응하여 무기염류수를 생성하여 준다.On the other hand, the inorganic salt crystals having a cobalt color are put into a container containing purified water, and then exposed to sunlight at room temperature for a certain period of time to react with the purified water to produce inorganic salt water.

한편 코발트색을 구비한 무기염류결정체를 3g과 정재수 20L를 수증기 증류추출기에 투입하여 105℃에서 2 내지 3 시간 가열하여 무기염류수를 생성하여 준다.Meanwhile, 3 g of inorganic salt crystals having cobalt color and 20 L of purified water are put into a steam distillation extractor and heated at 105° C. for 2 to 3 hours to produce inorganic salt water.

무기염류수와 일반용수를 용도에 따라 일정비율로 희석하여 사용하면, 저렴한 원재료비 및 가공비와 사용시 희석비율을 통한 원가경쟁력을 극대화 할 수 있다.If inorganic saline water and general water are diluted in a certain ratio according to the use, cost competitiveness can be maximized through low raw material cost and processing cost and dilution ratio when used.

또한, 악취 발생원에 분사하여 악취가스 제거 및 확산 차단 - 주요 악취가스와 독성물질 포름알데히드 등을 분해하여 제거; 추출액 내에 함유되어 있는 Mg, K, OH- 이온이 오염원과 반응하여 분해; 빠른 반응속도를 통한 악취제거 시간 단축한다.(참조: 첨부자료 3,6 탈취실험 결과, 배합전후에 따른 토양중금속 시험결과)In addition, it is sprayed to the source of odor to remove odor gas and block diffusion - decompose and remove major odor gas and toxic substance such as formaldehyde; Mg, K, OH- ions contained in the extract react with contaminants to decompose; Shorten odor removal time through fast reaction speed.

그리고 식품을 보관, 가공하기 전에 쌀겨로 무기염류결정체를의 추출액을 정제수와 일정비율로 희석하여 식품에 분사 - 유기인계, 카바 마이트계 농약 분해촉진; 농약 화합물보다 높은 반응성을 이용하여 제거가 용이한 단단위 화합물로 분해; 유기불소계, 유기염소계 농약 제거 촉진; 높은 침투력을 활용하여 식품 표면 및 내부에 잔류한 농약에 직접 작용한다.(참조: 첨부자료 5,7 세척 전후에 따른 농약분해 실험결과, 농약성분(원액) 분해에 대한 시험결과)And before storing and processing food, dilute the extract of inorganic salt crystals from rice bran with purified water at a certain ratio and spray it on food - Promotion of decomposition of organic phosphorus and carbamite pesticides; decomposition into monounit compounds that are easy to remove using higher reactivity than pesticide compounds; Promote removal of organic fluorine and organochlorine pesticides; It acts directly on the pesticide remaining on the surface and inside of the food by utilizing its high penetrating power.

또한, 액상 형태로 제조되어 사용이 편리하고 식품의 형태에 제한받지 않는 폭넓은 활용 가능하고 식품 생산, 보관, 유통, 가공 등 적정 사용 시기에 제한이 없다.In addition, it is manufactured in a liquid form, so it is convenient to use, can be used widely without being limited by the form of food, and there is no restriction on the appropriate use time such as food production, storage, distribution, and processing.

그리고 천연원료를 사용하여 기술의 안전성을 극대화하고 쌀겨를 순수하게 직화만으로 가열하여 순수한 무기염류결정체를를 만들어 물로 희석해서 추출액 제조하여 식품 첨가시 발생할 수 있는 위험성 제거할 수 있다. In addition, it is possible to maximize the safety of the technology by using natural raw materials and heat the rice bran purely by direct fire to form pure inorganic salt crystals and dilute it with water to prepare an extract, thereby eliminating the risk that may occur when adding food.

상술하는 본 발명은 쌀겨분말을 물과 교반하여 원형의 쌀겨성형물을 다수개로 준비하여 직화용기의 내부에 수용하고 가열수단으로 1차 직화가열하여 쌀겨성형물을 검은색에서 진갈색으로 탄화시켜 1차냉각한 후, 진갈색의 쌀겨성형물을 보라색으로 용융되게 2차직화가열하고 2차냉각한 후, 보라색의 용융된 쌀겨성형물을 코발색으로 용융시켜 무기염류로 생성되게 3차 직화가열하고 3차냉각하여서 얻은 무기염류결정체를를 생성하여 쌀겨분말을 직화연소시켜 무기염류결정체를로 생성제조하는 시간을 단축시키고, 쌀겨에 함유된 농약성분이 제거되어 친환경적인 무기염류결정체를를 얻을 수 있으며, 이러한 무기염류결정체를를 정제수와 혼합하여 미용수, 화장수, 살균수, 의료보조재, 식품첨가제, 비료첨가제 등과 악취제거 및 악취확산차단제와 비료첨가제, 농약분해제, 난연제로 사용하기 위함이다.In the present invention described above, rice bran powder is stirred with water to prepare a plurality of circular rice bran moldings, accommodated in a direct fire container, and primary direct heating is performed with a heating means to carbonize the rice bran moldings from black to dark brown and first cooling. After that, the dark brown rice bran molded product is heated by secondary direct heating to melt purple and secondary cooled, and then the purple molten rice bran molded product is melted to form an inorganic salt by tertiary direct heating and tertiary cooling. By producing salt crystals and direct combustion of rice bran powder, the time for producing and manufacturing inorganic salt crystals is shortened, and pesticides contained in rice bran are removed to obtain eco-friendly inorganic salt crystals, and these inorganic salt crystals are mixed with purified water It is intended to be used as a cosmetic water, lotion, sterilization water, medical aid, food additive, fertilizer additive, etc., by mixing it to remove odors, block the spread of odors, as a fertilizer additive, as a pesticide decomposer, and as a flame retardant.

이상에서 설명된 본 발명에 따른 실시예는 예시적인 것에 불과하며, 본 발명이 속하는 기술분야의 통상의 지식을 가진 자라면 이로부터 다양한 변형 및 균등한 타 실시예가 가능하다는 점을 잘 알 수 있을 것이다. 그러므로 본 발명은 상기의 상세한 설명에서 언급되는 형태로만 한정되는 것은 아님을 잘 이해할 수 있을 것이다.The embodiments according to the present invention described above are merely exemplary, and those of ordinary skill in the art to which the present invention pertains will appreciate that various modifications and equivalent other embodiments are possible therefrom. . Therefore, it will be well understood that the present invention is not limited to the form mentioned in the above detailed description.

따라서 본 발명의 진정한 기술적 보호범위는 첨부된 특허청구범위의 기술적 사상에 의해 정해져야 할 것이다. 또한, 본 발명은 첨부된 청구범위에 의해 정의되는 본 발명의 정신과 그 범위내에 있는 모든 변형물과 균등물 및 대체물을 포함하는 것으로 이해되어야 한다.Therefore, the true technical protection scope of the present invention should be determined by the technical spirit of the appended claims. Moreover, it is to be understood that the present invention includes all modifications, equivalents and substitutions falling within the spirit and scope of the invention as defined by the appended claims.

s100: 쌀겨교반물을 생성하는 단계
s110: 쌀겨성형물을 성형하는 단계
s120: 쌀겨성형물에 1차 직화연소하는 단계
s130: 쌀겨성형물 1차냉각단계
s140: 쌀겨성형물에 2차 직화연소하는 단계
s150: 쌀겨성형물 2차냉각단계
s160: 무기염류로 생성되게 3차 직화연소하는 단계
s170: 무기염류결정체를로 생성되게 무기염류 3차냉각단계
s100: step of generating a rice bran stirred
s110: forming a rice bran molding
s120: Step of primary direct fire burning in the rice bran molding
s130: rice bran molding primary cooling step
s140: Secondary direct fire burning in the rice bran molding
s150: rice bran molding secondary cooling step
s160: a step of tertiary direct combustion to be produced as inorganic salts
s170: inorganic salt tertiary cooling step to produce inorganic salt crystals

Claims (1)

쌀겨를 직화연소시켜 무기염류결정체를 생성하는 제조방법에서, 상기 제조방법은
2차 냉각되어 용융된 상기 쌀겨성형물을 가열수단으로 직접적으로 3차로 가열시켜 용융된 쌀겨성형물이 코발트색으로 용융되어 상기 쌀겨성형물이 용융되어 최종적으로 무기염류로 생성되는 무기염류로 생성되게 3차 직화연소하는 단계(s160)와; 3차 직화연소시켜 용융된 무기염류를 3차로 냉각하여 무기염류결정체를로 생성되게 무기염류 3차냉각단계(s170)로 구성되고, 상기 쌀겨성형물에 1차 직화연소하는 단계의 가열온도는 400℃~600℃로 1~2시간 직화가열하고,
상기 쌀겨성형물에 2차 직화연소하는 단계의 가열온도는 400℃~600℃로 30~60분 직화가열하고, 무기염류로 생성되게 3차 직화연소하는 단계의 가열온도는 400℃~600℃로 1~ 2시간 직화가열하고,
쌀겨교반물은 쌀겨분말 100중량부에 물 30중량부가 투입되어 교반되고,
쌀겨성형물에 2차 직화연소하는 단계에 송풍기를 구비하여 연소하는 쌀겨를 직화연소시켜 무기염류결정체를 생성하는 제조방법에 있어서,
쌀겨분말에 물을 투입하고 교반기로 교반하여 쌀겨교반물을 생성하는 쌀겨교반물을 생성하는 단계(s100)와; 상기 쌀겨교반물을 원형의 형상으로 성형하여 쌀겨성형물로 다수개로 준비하는 쌀겨성형물을 성형하는 단계(s110)와;
상기 쌀겨성형물을 직화용기에 투입하고, 상기 쌀겨성형물을 가열수단으로 직접적으로 1차로 가열시켜 상기 쌀겨성형물이 검은색에서 진갈색으로 탄화시키는 쌀겨성형물에 1차 직화연소하는 단계(s120)와: 1차 직화연소시켜 생성된 쌀겨성형물을 1차로 냉각하는 쌀겨성형물 1차냉각단계(s130)와;
1차 냉각된 상기 쌀겨성형물을 가열수단으로 직접적으로 2차로 가열시켜 상기 쌀겨성형물이 보라색으로 용융되게 하는 쌀겨성형물에 2차 직화연소하는 단계(s140)와; 2차 직화연소시켜 용융된 쌀겨성형물을 2차로 냉각하는 쌀겨성형물 2차냉각단계(s150)와,
쌀겨성형물에 다수개 통공을 형성하는 것을 특징으로 하는 쌀겨를 직화연소시켜 무기염류결정체를 생성하는 제조방법.
In the production method for producing inorganic salt crystals by direct combustion of rice bran, the production method comprises:
The secondly cooled and molten rice bran molding is directly heated tertiarily with a heating means so that the molten rice bran molding is melted in cobalt color, and the rice bran molding is melted to finally produce inorganic salts produced as inorganic salts. burning (s160); It consists of a tertiary cooling step (s170) of inorganic salts to produce inorganic salt crystals by tertiary cooling of molten inorganic salts by tertiary direct fire combustion, and the heating temperature of the step of primary direct fire burning in the rice bran molding is 400 ° C. Direct heating at ~600℃ for 1-2 hours,
The heating temperature of the second direct fire burning in the rice bran molding is 400 ° C to 600 ° C for 30 to 60 minutes, and the heating temperature of the third direct fire burning to produce inorganic salts is 400 ° C to 600 ° C. ~ 2 hours direct heating,
Rice bran stirred product is stirred by adding 30 parts by weight of water to 100 parts by weight of rice bran powder,
In the manufacturing method of producing inorganic salt crystals by direct fire combustion of the burned rice bran by providing a blower in the step of secondary direct fire burning in the rice bran molding,
Adding water to the rice bran powder and stirring with a stirrer to produce a rice bran stirred product to produce a rice bran stirred (s100) and; Forming the rice bran agitated product into a circular shape to form a rice bran molded product prepared in a plurality of rice bran moldings (s110);
Putting the rice bran molded product into a direct fire container, and first directly heating the rice bran molded product with a heating means to carbonize the rice bran molded product from black to dark brown. A rice bran molding primary cooling step (s130) of primarily cooling the rice bran molding produced by direct fire combustion;
Directly secondarily heating the firstly cooled rice bran molded product with a heating means to burn the rice bran molded product by direct fire so that the rice bran molded product is melted in purple color (s140); A secondary cooling step (s150) of a rice bran molded product of secondary cooling of the molten rice bran molded product by secondary direct fire combustion;
A method for producing inorganic salt crystals by direct fire combustion of rice bran, characterized in that a plurality of through holes are formed in the rice bran molding.
KR1020210098016A 2018-07-31 2021-07-26 A method for producing inorganic salt crystals by burning rice bran by direct burning KR20210095832A (en)

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