KR20210062413A - W/S Type Cosmetic Composition Containing High-Content Potassium Lactate and Silicon Oil - Google Patents
W/S Type Cosmetic Composition Containing High-Content Potassium Lactate and Silicon Oil Download PDFInfo
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- KR20210062413A KR20210062413A KR1020190150622A KR20190150622A KR20210062413A KR 20210062413 A KR20210062413 A KR 20210062413A KR 1020190150622 A KR1020190150622 A KR 1020190150622A KR 20190150622 A KR20190150622 A KR 20190150622A KR 20210062413 A KR20210062413 A KR 20210062413A
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- 239000000203 mixture Substances 0.000 title claims abstract description 155
- 239000002537 cosmetic Substances 0.000 title claims abstract description 56
- PHZLMBHDXVLRIX-UHFFFAOYSA-M potassium lactate Chemical compound [K+].CC(O)C([O-])=O PHZLMBHDXVLRIX-UHFFFAOYSA-M 0.000 title claims description 17
- 239000001521 potassium lactate Substances 0.000 title claims description 17
- 235000011085 potassium lactate Nutrition 0.000 title claims description 17
- 229960001304 potassium lactate Drugs 0.000 title claims description 17
- 239000003921 oil Substances 0.000 title description 8
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 title description 3
- 239000010703 silicon Substances 0.000 title description 3
- 229910052710 silicon Inorganic materials 0.000 title description 3
- 150000003839 salts Chemical class 0.000 claims abstract description 41
- 229910052751 metal Inorganic materials 0.000 claims abstract description 37
- 239000002184 metal Substances 0.000 claims abstract description 37
- JVTAAEKCZFNVCJ-UHFFFAOYSA-M Lactate Chemical compound CC(O)C([O-])=O JVTAAEKCZFNVCJ-UHFFFAOYSA-M 0.000 claims abstract description 36
- 229920002545 silicone oil Polymers 0.000 claims abstract description 27
- 230000003020 moisturizing effect Effects 0.000 claims abstract description 21
- 229940001447 lactate Drugs 0.000 claims description 33
- 229940008099 dimethicone Drugs 0.000 claims description 19
- 239000004205 dimethyl polysiloxane Substances 0.000 claims description 19
- 235000013870 dimethyl polysiloxane Nutrition 0.000 claims description 19
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims description 19
- XMSXQFUHVRWGNA-UHFFFAOYSA-N Decamethylcyclopentasiloxane Chemical compound C[Si]1(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O1 XMSXQFUHVRWGNA-UHFFFAOYSA-N 0.000 claims description 10
- 239000004480 active ingredient Substances 0.000 claims description 6
- 230000007794 irritation Effects 0.000 claims description 6
- 229940086555 cyclomethicone Drugs 0.000 claims description 5
- 238000000034 method Methods 0.000 claims description 5
- 229920006037 cross link polymer Polymers 0.000 claims description 3
- 230000004044 response Effects 0.000 claims description 3
- CYDQOEWLBCCFJZ-UHFFFAOYSA-N 4-(4-fluorophenyl)oxane-4-carboxylic acid Chemical compound C=1C=C(F)C=CC=1C1(C(=O)O)CCOCC1 CYDQOEWLBCCFJZ-UHFFFAOYSA-N 0.000 claims description 2
- 239000004251 Ammonium lactate Substances 0.000 claims description 2
- 229940059265 ammonium lactate Drugs 0.000 claims description 2
- 235000019286 ammonium lactate Nutrition 0.000 claims description 2
- RZOBLYBZQXQGFY-HSHFZTNMSA-N azanium;(2r)-2-hydroxypropanoate Chemical compound [NH4+].C[C@@H](O)C([O-])=O RZOBLYBZQXQGFY-HSHFZTNMSA-N 0.000 claims description 2
- 239000001540 sodium lactate Substances 0.000 claims description 2
- 235000011088 sodium lactate Nutrition 0.000 claims description 2
- 229940005581 sodium lactate Drugs 0.000 claims description 2
- ZQTYRTSKQFQYPQ-UHFFFAOYSA-N trisiloxane Chemical compound [SiH3]O[SiH2]O[SiH3] ZQTYRTSKQFQYPQ-UHFFFAOYSA-N 0.000 claims description 2
- 230000036556 skin irritation Effects 0.000 abstract description 37
- 231100000475 skin irritation Toxicity 0.000 abstract description 37
- 206010040880 Skin irritation Diseases 0.000 abstract description 35
- 235000019645 odor Nutrition 0.000 abstract description 30
- 229920001296 polysiloxane Polymers 0.000 abstract description 5
- 230000003247 decreasing effect Effects 0.000 abstract description 2
- 230000002708 enhancing effect Effects 0.000 abstract description 2
- 230000000052 comparative effect Effects 0.000 description 48
- 210000003491 skin Anatomy 0.000 description 44
- 230000000694 effects Effects 0.000 description 23
- 238000009472 formulation Methods 0.000 description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 20
- 238000000926 separation method Methods 0.000 description 18
- 230000001877 deodorizing effect Effects 0.000 description 13
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 12
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N squalane Chemical compound CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 description 12
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 10
- 230000015572 biosynthetic process Effects 0.000 description 9
- 238000011156 evaluation Methods 0.000 description 7
- 238000004945 emulsification Methods 0.000 description 6
- JXTPJDDICSTXJX-UHFFFAOYSA-N n-Triacontane Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCC JXTPJDDICSTXJX-UHFFFAOYSA-N 0.000 description 6
- 239000011780 sodium chloride Substances 0.000 description 6
- 229940032094 squalane Drugs 0.000 description 6
- 239000006071 cream Substances 0.000 description 5
- 235000011187 glycerol Nutrition 0.000 description 5
- 229940075529 glyceryl stearate Drugs 0.000 description 5
- 239000004615 ingredient Substances 0.000 description 5
- 235000019198 oils Nutrition 0.000 description 5
- 229940100460 peg-100 stearate Drugs 0.000 description 5
- 238000002360 preparation method Methods 0.000 description 5
- 239000008213 purified water Substances 0.000 description 5
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 description 5
- 235000010234 sodium benzoate Nutrition 0.000 description 5
- 239000004299 sodium benzoate Substances 0.000 description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 208000003251 Pruritus Diseases 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 239000002781 deodorant agent Substances 0.000 description 4
- 239000000839 emulsion Substances 0.000 description 4
- LADGBHLMCUINGV-UHFFFAOYSA-N tricaprin Chemical compound CCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCC)COC(=O)CCCCCCCCC LADGBHLMCUINGV-UHFFFAOYSA-N 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 3
- 239000003995 emulsifying agent Substances 0.000 description 3
- 239000006210 lotion Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- IUMSDRXLFWAGNT-UHFFFAOYSA-N Dodecamethylcyclohexasiloxane Chemical compound C[Si]1(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O1 IUMSDRXLFWAGNT-UHFFFAOYSA-N 0.000 description 2
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 description 2
- 206010064503 Excessive skin Diseases 0.000 description 2
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 description 2
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 2
- 206010054786 Skin burning sensation Diseases 0.000 description 2
- 239000012190 activator Substances 0.000 description 2
- 239000002671 adjuvant Substances 0.000 description 2
- 229940081733 cetearyl alcohol Drugs 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000004332 deodorization Methods 0.000 description 2
- 239000003974 emollient agent Substances 0.000 description 2
- 230000007803 itching Effects 0.000 description 2
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical group CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 2
- KWGKDLIKAYFUFQ-UHFFFAOYSA-M lithium chloride Chemical compound [Li+].[Cl-] KWGKDLIKAYFUFQ-UHFFFAOYSA-M 0.000 description 2
- 230000014759 maintenance of location Effects 0.000 description 2
- 229910021645 metal ion Inorganic materials 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 230000002688 persistence Effects 0.000 description 2
- -1 potassium lactate Chemical class 0.000 description 2
- 239000003755 preservative agent Substances 0.000 description 2
- 230000035807 sensation Effects 0.000 description 2
- 235000019615 sensations Nutrition 0.000 description 2
- 239000003381 stabilizer Substances 0.000 description 2
- 239000002562 thickening agent Substances 0.000 description 2
- UNTXZFOXVBGXGZ-UHFFFAOYSA-N 1,3,5,7,9,11,13-heptaoxa-2$l^{2},4$l^{2},6$l^{2},8$l^{2},10$l^{2},12$l^{2},14$l^{2}-heptasilacyclotetradecane Chemical compound O1[Si]O[Si]O[Si]O[Si]O[Si]O[Si]O[Si]1 UNTXZFOXVBGXGZ-UHFFFAOYSA-N 0.000 description 1
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 description 1
- 241001237961 Amanita rubescens Species 0.000 description 1
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 206010015946 Eye irritation Diseases 0.000 description 1
- 206010016322 Feeling abnormal Diseases 0.000 description 1
- 206010020751 Hypersensitivity Diseases 0.000 description 1
- 235000018330 Macadamia integrifolia Nutrition 0.000 description 1
- 240000000912 Macadamia tetraphylla Species 0.000 description 1
- 235000003800 Macadamia tetraphylla Nutrition 0.000 description 1
- 230000007815 allergy Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 239000001110 calcium chloride Substances 0.000 description 1
- 229910001628 calcium chloride Inorganic materials 0.000 description 1
- 239000002738 chelating agent Substances 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- DDJSWKLBKSLAAZ-UHFFFAOYSA-N cyclotetrasiloxane Chemical compound O1[SiH2]O[SiH2]O[SiH2]O[SiH2]1 DDJSWKLBKSLAAZ-UHFFFAOYSA-N 0.000 description 1
- JJRDHFIVAPVZJN-UHFFFAOYSA-N cyclotrisiloxane Chemical compound O1[SiH2]O[SiH2]O[SiH2]1 JJRDHFIVAPVZJN-UHFFFAOYSA-N 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- DLAHAXOYRFRPFQ-UHFFFAOYSA-N dodecyl benzoate Chemical compound CCCCCCCCCCCCOC(=O)C1=CC=CC=C1 DLAHAXOYRFRPFQ-UHFFFAOYSA-N 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 239000000686 essence Substances 0.000 description 1
- 239000010696 ester oil Substances 0.000 description 1
- 231100000013 eye irritation Toxicity 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000004088 foaming agent Substances 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 239000000499 gel Substances 0.000 description 1
- 239000003349 gelling agent Substances 0.000 description 1
- JEGUKCSWCFPDGT-UHFFFAOYSA-N h2o hydrate Chemical compound O.O JEGUKCSWCFPDGT-UHFFFAOYSA-N 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 230000000774 hypoallergenic effect Effects 0.000 description 1
- 230000005722 itchiness Effects 0.000 description 1
- 239000004310 lactic acid Substances 0.000 description 1
- 235000014655 lactic acid Nutrition 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 229910001629 magnesium chloride Inorganic materials 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 239000010466 nut oil Substances 0.000 description 1
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 description 1
- 235000008390 olive oil Nutrition 0.000 description 1
- 239000004006 olive oil Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000003002 pH adjusting agent Substances 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 229920005862 polyol Polymers 0.000 description 1
- 150000003077 polyols Chemical class 0.000 description 1
- 239000001103 potassium chloride Substances 0.000 description 1
- 235000011164 potassium chloride Nutrition 0.000 description 1
- 229910001414 potassium ion Inorganic materials 0.000 description 1
- 239000003352 sequestering agent Substances 0.000 description 1
- 230000037384 skin absorption Effects 0.000 description 1
- 231100000274 skin absorption Toxicity 0.000 description 1
- 230000036548 skin texture Effects 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 210000000434 stratum corneum Anatomy 0.000 description 1
- 239000000516 sunscreening agent Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 239000000375 suspending agent Substances 0.000 description 1
- 238000010257 thawing Methods 0.000 description 1
- 150000003626 triacylglycerols Chemical class 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 239000004034 viscosity adjusting agent Substances 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
- A61K8/064—Water-in-oil emulsions, e.g. Water-in-silicone emulsions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
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- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Dermatology (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Dispersion Chemistry (AREA)
- Emergency Medicine (AREA)
- Cosmetics (AREA)
Abstract
Description
본 발명은 고함량의 락테이트 금속염 및 실리콘계 오일의 혼합물을 포함하는 W/S형 화장료 조성물에 관한 것으로, 보다 구체적으로는 고함량의 락테이트 금속염과 함께 실리콘계 오일을 포함함으로써 락테이트 금속염으로부터 유래되는 자극취 및 불쾌취를 소취시켜 사용감을 현저하게 개선시키고, 피부 보습력의 증강 및 피부 자극의 강하로 피부의 상태를 개선시키는 효과를 발휘하는 W/S형 화장료 조성물에 관한 것이다.The present invention relates to a W/S type cosmetic composition comprising a mixture of a high content lactate metal salt and a silicone oil, and more specifically, a lactate metal salt derived from a lactate metal salt by including a silicone oil together with a high content lactate metal salt. It relates to a W/S type cosmetic composition that significantly improves the feeling of use by deodorizing irritating odors and unpleasant odors, and exhibits an effect of improving the condition of the skin by enhancing skin moisturizing power and decreasing skin irritation.
통상적으로 유화 화장료 조성물 형태는 수중유(Oil in water, O/W) 유화 타입, 유중수(Water in oil, W/O) 유화 타입 및 실리콘중수(Water in silicone, W/S) 유화 타입으로 크게 대별된다. Typically, the types of emulsified cosmetic compositions are largely divided into oil in water (O/W) emulsification type, water in oil (W/O) emulsification type, and water in silicone (W/S) emulsification type. It is roughly different.
수중유(O/W) 유화 타입은 친수성 타입으로서, 사용감이 촉촉하고 부드러우나, 화장의 지속성과 내수성이 떨어지는 단점이 있다. 이러한 단점을 개선하기 위하여 친유성 타입인 유중수(W/O) 유화 타입이 개발되었다. 그러나 유중수(W/O) 유화 타입은 화장 지속성과 내수성은 매우 우수하지만, 끈적임, 유분감, 왁시(waxy)감 등으로 인하여 피부에 부담을 주며 발림성, 퍼짐성 등의 사용감이 불량하다는 단점이 있다. 특히, 종래의 유화 조성물에는 스쿠알란 등의 탄화수소계 오일, C12-C15 알킬벤조에이트 등의 에스테르계 오일, 올리브유, 마카다미아 넛 오일 등의 식물성 오일 등이 다량 함유되는데, 이러한 오일들은 피부 자극성이 있는 것으로 알려져 있어 소비자의 저자극 화장품에 대한 욕구를 만족시키지 못하고 있다.The oil-in-water (O/W) emulsification type is a hydrophilic type and has a moist and soft feeling of use, but has a disadvantage in that the persistence of makeup and water resistance are poor. In order to improve these disadvantages, a lipophilic water-in-oil (W/O) emulsification type was developed. However, the water-in-oil (W/O) emulsifying type has excellent makeup persistence and water resistance, but has a disadvantage in that it puts a burden on the skin due to stickiness, oily, waxy, etc., and the feeling of use such as spreadability and spreadability is poor. In particular, conventional emulsion compositions contain a large amount of hydrocarbon oils such as squalane, ester oils such as C12-C15 alkylbenzoate, vegetable oils such as olive oil and macadamia nut oil, and these oils are known to have skin irritation. It is not satisfying the consumer's desire for hypoallergenic cosmetics.
실리콘중수(Water in silicone, W/S) 유화 타입은 실리콘 오일이 물을 감싸면서 유화가 된 제형으로 실키(silky)한 질감으로 피부결을 개선하고 피부 보호 효과가 있다.Water in silicone (W/S) emulsification type is an emulsified formulation with silicone oil enveloping water and has a silky texture that improves skin texture and protects the skin.
또한, 실리콘 오일은 탄력적이며 입체적인 특유의 구조로 인하여 매우 가볍고 퍼짐성 등의 사용감 및 피부 안정성이 우수할 뿐만 아니라 뛰어난 내수성과 에몰리언트(emollient) 효과를 지니고 있으므로, 이를 화장료에 이용하려는 노력이 계속되어 왔으며, 실리콘 오일을 외상으로 이용한 실리콘중수(W/S) 유화형 화장료 조성물에 대한 개발이 지속적으로 이루어지고 있다.In addition, silicone oil is very light due to its elastic and three-dimensional structure, and has excellent feeling of use and skin stability such as spreadability, as well as excellent water resistance and emollient effect.Therefore, efforts to use it in cosmetics have been continued. Development of a water-in-silicone (W/S) emulsion-type cosmetic composition using silicone oil as an external wound has been continuously made.
락테이트 금속염, 예컨대 포타슘 락테이트(Potassium Lactate)는 유화제(Emulsifier), pH 조절제, 보존제, 발색제, 피부 유연제 및 각질 제거제로서 화장품 제형에 많이 활용되고 있고, 특히 포타슘 락테이트는 피부에 안전하면서 피부 침투 효과 및 각질층의 수분보유 및 수분유지 능력을 촉진하고, 피부에 함께 도포되는 다른 보습 성분의 침투를 촉진하는 등의 작용이 있는 물질로서 많은 기능성 화장품 제형에서 사용되어 왔다(특허문헌 1, 비특허문헌 1 참조). 그러나 락테이트 금속염은 제형화된 화장품에 특히 고함량으로 포함될 경우 시간이 지남에 따라 불안정한 제형으로 변하게 되고, 자극취의 발생으로 사용감이 저하되는 문제점이 있었다.Lactate metal salts, such as potassium lactate, are widely used in cosmetic formulations as emulsifiers, pH adjusters, preservatives, coloring agents, skin softeners and exfoliating agents.In particular, potassium lactate is safe to the skin and penetrates the skin. It has been used in many functional cosmetic formulations as a substance that has an effect, promotes the moisture retention and moisture retention ability of the stratum corneum, and promotes penetration of other moisturizing ingredients applied to the skin (
조성물에 포함되는 유효성분에 의한 자극취의 저감 방법 및 피부 자극감을 감소시키는 방법에 관한 종래 기술을 살펴보면, 조성물에서의 아세테이트 계열 화합물로부터 유래되는 자극취를 소취(消臭, Deodorizing)시키는데 적절한 산-염기성의 성분, 예컨대 락테이트 금속염을 혼합해 아세테이트 계열 화합물을 화학적으로 중화시켜 아세테이트 계열 화합물로 인한 자극취를 감소시키는 화학적 중화 방법이 알려져 있고(특허문헌 2 참조), 조성물에서의 금속 이온, 예컨대, 포타슘 이온 등으로 피부 자극감을 저감시키는 효과를 밝힌 문헌은 개시된 바 있으나(특허문헌 3 참조), 피부 보습을 목적으로 하는 화장품에서 고함량의 락테이트 금속염으로 인해 발생되는 자극취를 소취시키고, 피부 자극감을 저감시키는 방법에 관한 내용은 개시된 바 없다.Looking at the prior art related to the method for reducing irritation odor by the active ingredient contained in the composition and the method for reducing skin irritation, the acid-basic property suitable for deodorizing the irritating odor derived from the acetate-based compound in the composition. A chemical neutralization method is known to reduce the irritating odor caused by the acetate-based compound by chemically neutralizing the acetate-based compound by mixing a component such as a lactate metal salt (see Patent Document 2), and a metal ion in the composition, such as potassium ions, etc. Although the literature revealing the effect of reducing skin irritation has been disclosed (see Patent Document 3), a method of deodorizing irritating odors caused by a high content of lactate metal salts in cosmetics intended for skin moisturization and reducing skin irritation. No information has been disclosed.
따라서, 피부 보습 개선 효과가 우수한 락테이트 금속염을 고함량으로 포함하는 화장료 조성물의 자극취를 소취시키고, 피부 자극감을 감소시킬 수 있는 수단에 대한 필요성이 존재한다.Accordingly, there is a need for a means capable of deodorizing the irritating odor of a cosmetic composition containing a high content of lactate metal salt having an excellent skin moisturizing improvement effect and reducing the skin irritation sensation.
본 발명자들은 화장료 조성물 속에 배합된 고함량의 락테이트 금속염 성분으로부터 유래되는 자극취 또는 불쾌한 냄새를 소취하는 효과가 우수한 물질(들)을 포함하는 조성물을 개발하고자 예의 노력한 결과, 고함량의 락테이트 금속염과 실리콘계 오일을 혼합하여 제조한 W/S 제형(Water in silicon. W/S emulsion)의 조성물은 락테이트 금속염으로부터 유래되는 자극취 또는 불쾌한 냄새를 소취시켜 사용감을 개선시키는 효과와, 피부 보습력을 증가시키는 효과 및 피부 자극 반응을 완화시키는 효과가 탁월함을 발견하였다.The present inventors have made diligent efforts to develop a composition containing material(s) having excellent effect of deodorizing irritating odor or unpleasant odor derived from a high content lactate metal salt component incorporated in a cosmetic composition. As a result, a high content lactate metal salt and The composition of the W/S formulation (Water in silicon.W/S emulsion) prepared by mixing silicone oil improves the feeling of use by deodorizing irritating odors or unpleasant odors derived from lactate metal salts, and increasing skin moisturizing power. And it was found that the effect of alleviating the skin irritation reaction was excellent.
따라서, 본 발명의 목적은 고함량의 락테이트 금속염 및 실리콘계 오일의 혼합물을 유효성분으로 포함하는 화장료 조성물, 바람직하게는 락테이트 금속염으로부터 유래되는 자극취 또는 불쾌취를 소취시켜 사용감이 개선되고, 우수한 피부 상태 개선 효과, 특히 피부 보습력 개선 효과, 피부 자극 반응 완화 효과를 발휘하는 W/S형 화장료 조성물을 제공하는 데 있다.Accordingly, an object of the present invention is a cosmetic composition comprising a mixture of a high content of lactate metal salt and silicone oil as an active ingredient, preferably by deodorizing irritating or unpleasant odors derived from lactate metal salts to improve the feeling of use, and excellent skin It is to provide a W/S type cosmetic composition that exhibits a condition improving effect, particularly a skin moisturizing effect, and a skin irritation response alleviating effect.
상기 목적을 달성하기 위하여, 본 발명은 고함량의 락테이트 금속염 및 실리콘계 오일의 혼합물을 유효성분으로 포함하는 W/S형 화장료 조성물, 바람직하게는 자극취 소취용 W/S형 화장료 조성물, 피부 보습용 W/S형 화장료 조성물 및 피부 자극 완화용 W/S형 화장료 조성물을 제공한다.In order to achieve the above object, the present invention is a W/S type cosmetic composition comprising a mixture of a high content lactate metal salt and a silicone oil as an active ingredient, preferably a W/S type cosmetic composition for deodorizing irritation odor, and for moisturizing the skin. It provides a W/S type cosmetic composition and a W/S type cosmetic composition for relieving skin irritation.
본 발명에 따른 락테이트 금속염 및 실리콘계 오일의 혼합물을 유효성분으로 포함하는 W/S형 화장료 조성물은 락테이트 금속염으로부터 발생되는 자극취 및 불쾌취를 소취시켜 사용감이 개선되고, 우수한 피부 상태 개선 효과, 특히 피부 보습력 개선 효과 및 피부 자극 반응 완화 효과를 제공할 수 있다.The W/S-type cosmetic composition comprising a mixture of lactate metal salt and silicone oil according to the present invention as an active ingredient deodorizes irritating odors and unpleasant odors generated from lactate metal salts, thereby improving the feeling of use and improving skin condition, especially It can provide an effect of improving skin moisturizing ability and relieving skin irritation response.
도 1은 본 발명의 실시예 8에 따른 W/S형 화장료 조성물에 의한 피부 소취 효과를 나타낸 그래프이다.
도 2는 본 발명의 실시예 8에 따른 W/S형 화장료 조성물의 피부 도포 후, 피부 자극감 완화 효과를 나타낸 그래프이다.1 is a graph showing the skin deodorant effect by the W/S type cosmetic composition according to Example 8 of the present invention.
2 is a graph showing the effect of reducing skin irritation after applying the W/S type cosmetic composition according to Example 8 of the present invention to the skin.
다른 식으로 정의되지 않는 한, 본 명세서에서 사용된 모든 기술적 및 과학적 용어들은 본 발명이 속하는 기술분야에서 숙련된 전문가에 의해서 통상적으로 이해되는 것과 동일한 의미를 갖는다. 일반적으로 본 명세서에서 사용된 명명법은 본 기술분야에서 잘 알려져 있고 통상적으로 사용되는 것이다.Unless otherwise defined, all technical and scientific terms used herein have the same meaning as commonly understood by an expert skilled in the art to which the present invention belongs. In general, the nomenclature used in this specification is well known and commonly used in the art.
이하, 본 발명에 대하여 보다 구체적으로 설명한다.Hereinafter, the present invention will be described in more detail.
본 명세서에서 길이, 면적, 부피, 시간(기간), 농도, 함량, 온도 등을 표현하는데 사용된 용어 "약"은 해당 수치 또는 수치 범위에서 최대 10%의 허용오차가 존재한다는 것을 의미한다.In the present specification, the term "about" used to express length, area, volume, time (period), concentration, content, temperature, etc. means that there is a tolerance of up to 10% in the corresponding value or numerical range.
본 발명은 일 관점에서, 락테이트 금속염 및 실리콘계 오일의 혼합물을 유효성분으로 포함하는 W/S형(Water in silicon. W/S emulsion, W/S Type) 화장료 조성물, 바람직하게는 고함량의 락테이트 금속염으로부터 유래되는 자극취 소취용 W/S형 화장료 조성물, 피부 보습용 W/S형 화장료 조성물 및 피부 자극 반응 완화용 W/S형 화장료 조성물에 관한 것이다.In one aspect, the present invention is a W/S type (Water in silicon.W/S emulsion, W/S Type) cosmetic composition comprising a mixture of a lactate metal salt and a silicone oil as an active ingredient, preferably a high content lock It relates to a W/S-type cosmetic composition for deodorizing irritation odor derived from tate metal salt, a W/S-type cosmetic composition for moisturizing skin, and a W/S-type cosmetic composition for relieving skin irritation reaction.
상기 락테이트 금속염(Lactate Metallic Salts)은 젖산(Lactic Acid)에 금속이온이 결합된 형태로 생성 또는 합성될 수 있는 화합물, 바람직하게는 포타슘 락테이트(Potassium Lactate), 소듐 락테이트(Sodium Lactate), 암모늄 락테이트(Ammonium Lactate), 또는 이들의 혼합물일 수 있으나, 이에 한정되는 것은 아니다. The lactate metal salts are compounds that can be produced or synthesized in a form in which metal ions are bound to lactic acid, preferably potassium lactate, sodium lactate, It may be ammonium lactate, or a mixture thereof, but is not limited thereto.
상기 포타슘 락테이트는 피부에 존재하는 자연보습인자(Natural Moisturing Factor, NMF)의 일종으로, 수분과 결합하여 피부에서 수분이 건조되는 것을 억제한다. 포타슘 락테이트는 독성이 없고, 알레르기를 일으키지 않으며, 무색의 특성을 가진다. The potassium lactate is a kind of natural moisturing factor (NMF) that exists in the skin, and it binds with moisture to inhibit drying of moisture in the skin. Potassium lactate is non-toxic, does not cause allergies, and is colorless.
상기 락테이트 금속염의 함량은 화장품 안전에 관한 규칙에 의거한 사용 제한량을 고려하여, 조성물의 총 중량을 기준으로, 7.0~25.0중량%, 바람직하게는 7.0~20.0중량%, 더 바람직하게는 7.0~12.0중량%, 가장 바람직하게는 11.0~12.0중량%일 수 있으며, 상기 락테이트 금속염의 함량이 조성물의 총 중량을 기준으로 7.0중량% 미만일 경우 화장료로서 목적하는 피부 보습력 개선 효능을 충분히 나타낼 수 없고, 상기 조성물 중 락테이트 금속염의 함량이 조성물의 총 중량을 기준으로 25.0중량%를 초과할 경우 화장료 제형 중에 충분히 용해될 수 없어 화장료 제형의 다른 성분들과 안정적으로 배합될 수 없고, 또 피부에 적용시 과도한 피부 자극 등 안정성에서 문제가 있을 수 있다. The content of the lactate metal salt is 7.0 to 25.0% by weight, preferably 7.0 to 20.0% by weight, more preferably 7.0, based on the total weight of the composition, in consideration of the usage limit according to the rules on cosmetic safety. It may be ~12.0% by weight, most preferably 11.0 to 12.0% by weight, and when the content of the lactate metal salt is less than 7.0% by weight based on the total weight of the composition, the desired skin moisturizing power improvement effect as a cosmetic cannot be sufficiently exhibited. , When the content of the lactate metal salt in the composition exceeds 25.0% by weight based on the total weight of the composition, it cannot be sufficiently dissolved in the cosmetic formulation, so it cannot be stably blended with other ingredients of the cosmetic formulation, and is applied to the skin. There may be a problem with stability, such as excessive skin irritation.
상기 실리콘계 오일은 트리실록산(Trisiloxane), 디메치콘(Dimethicone), 사이클로메치콘(Cyclomethicone)(예컨대, 사이클로트리실록산(Cyclotrisiloxane), 사이클로테트라실록산(Cyclotetrasiloxane), 사이클로펜타실록산(Cyclopentasiloxane), 사이클로헥사실록산(Cyclohexasiloxane), 사이클로헵타실록산(Cycloheptasiloxane) 등), PEG/PPG-19/19 디메치콘(PEG/PPG-19/19 Dimethicone), 폴리실리콘-11(Polysilicone-11), 및 디메치콘 크로스폴리머(Dimethicone Crosspolymer), 또는 이들의 혼합물일 수 있으나, 이에 한정되는 것은 아니다. 상기 실리콘계 오일은 바람직하게는 사이클로메치콘, 디메치콘 및 이들의 혼합물, 더 바람직하게는 사이클로펜타실록산, 디메치콘 및 이들의 혼합물일 수 있으며, 가장 바람직하게는 사이클로펜타실록산 및 디메치콘의 혼합물이다. The silicone oils include Trisiloxane, Dimethicone, Cyclomethicone (e.g., Cyclotrisiloxane, Cyclotetrasiloxane, Cyclopentasiloxane), and Cyclohexasiloxane. Cyclohexasiloxane), Cycloheptasiloxane, etc.), PEG/PPG-19/19 Dimethicone (PEG/PPG-19/19 Dimethicone), Polysilicone-11, and Dimethicone Crosspolymer ), or a mixture thereof, but is not limited thereto. The silicone oil may be preferably cyclomethicone, dimethicone, and mixtures thereof, more preferably cyclopentasiloxane, dimethicone, and mixtures thereof, and most preferably a mixture of cyclopentasiloxane and dimethicone.
상기 사이클로메치콘 및 디메치콘의 혼합물은 사이클로메치콘 및 디메치콘을 2.0~30.0 : 1.0~15.0, 바람직하게는 7.0~25.0 : 3.5 ~12.5의 중량비로 혼합한 것일 수 있으며, 가장 바람직하게는 10.0~20.0 : 5.0~10.0의 중량비로 혼합한 것이다.The mixture of cyclomethicone and dimethicone may be a mixture of cyclomethicone and dimethicone in a weight ratio of 2.0 to 30.0: 1.0 to 15.0, preferably 7.0 to 25.0: 3.5 to 12.5, and most preferably 10.0 to It was mixed at a weight ratio of 20.0: 5.0-10.0.
상기 실리콘계 오일의 함량은 화장품 안전에 관한 규칙에 의거한 사용 제한량을 고려하여, 조성물의 총 중량을 기준으로, 2.9~52.1중량%, 바람직하게는 2.9~41.7중량%, 더 바람직하게는 2.9~25.0중량%, 가장 바람직하게는 5.0~25.0중량%일 수 있으며, 상기 실리콘계 오일의 함량이 조성물의 총 중량을 기준으로 2.9중량% 미만일 경우 화장료로서 목적하는 고함량의 락테이트 금속염으로부터 유래되는 자극취의 소취, 피부 보습력 개선 및 피부 자극 완화 효능을 나타낼 수 없고, 상기 실리콘계 오일의 함량이 조성물의 총 중량을 기준으로 52.1중량%를 초과할 경우 화장료 제형 중에 충분히 용해될 수 없어 화장료 제형의 다른 성분들과 안정적으로 배합될 수 없고, 또 피부에 적용시 과도한 피부 자극 등 안정성에서 문제가 있을 수 있다.The content of the silicone oil is 2.9-52.1% by weight, preferably 2.9-41.7% by weight, more preferably 2.9- It may be 25.0% by weight, most preferably 5.0 to 25.0% by weight, and when the content of the silicone oil is less than 2.9% by weight based on the total weight of the composition, irritation odor derived from the high content lactate metal salt intended as a cosmetic It cannot exhibit deodorization, skin moisturizing power and skin irritation alleviation effect, and when the content of the silicone-based oil exceeds 52.1% by weight based on the total weight of the composition, it cannot be sufficiently dissolved in the cosmetic formulation, and thus other ingredients of the cosmetic formulation and It cannot be formulated stably, and when applied to the skin, there may be problems in stability such as excessive skin irritation.
상기 락테이트 금속염 및 실리콘계 오일의 혼합물은 락테이트 금속염 및 실리콘계 오일을 1.0~12.0 : 1.0~50.0, 바람직하게는 6.0~12.0 : 5.0~30.0의 중량비로 혼합한 것일 수 있으며, 가장 바람직하게는 12.0 : 5.0~25.0의 중량비로 혼합한 것이다.The mixture of lactate metal salt and silicone oil may be a mixture of lactate metal salt and silicone oil in a weight ratio of 1.0 to 12.0: 1.0 to 50.0, preferably 6.0 to 12.0: 5.0 to 30.0, and most preferably 12.0: It is mixed at a weight ratio of 5.0 to 25.0.
상기 조성물은 염화나트륨, 염화칼륨, 염화리튬, 염화칼슘 및 염화마그네슘으로 이루어진 군에서 선택되는 1종 이상의 염을 유화 안정제로서 더 포함할 수 있고, 상기 염의 함량은 조성물의 총 중량을 기준으로, 0.01~20.0중량%, 바람직하게는 0.01~10.0중량%, 가장 바람직하게는 0.5~5.0중량%일 수 있다. 상기 염의 함량이 조성물의 총 중량을 기준으로 0.01중량% 미만일 경우 화장료로서 목적하는 고함량의 락테이트 금속염으로부터 유래되는 자극취의 소취, 피부 보습력 개선 및 피부 자극 완화 효능을 현저하게 향상시킬 수 없고, 상기 염의 함량이 조성물의 총 중량을 기준으로 20.0중량%를 초과할 경우 화장료 제형 중에 충분히 용해될 수 없어 화장료 제형의 다른 성분들과 안정적으로 배합될 수 없고, 또 피부에 적용시 과도한 피부 자극 등 안정성에서 문제가 있을 수 있다.The composition may further include one or more salts selected from the group consisting of sodium chloride, potassium chloride, lithium chloride, calcium chloride, and magnesium chloride as an emulsion stabilizer, and the content of the salt is 0.01 to 20.0 weight based on the total weight of the composition. %, preferably 0.01 to 10.0% by weight, most preferably 0.5 to 5.0% by weight. When the content of the salt is less than 0.01% by weight based on the total weight of the composition, it is not possible to remarkably improve the deodorization, skin moisturizing power and skin irritation alleviation effect of the irritation odor derived from the high content lactate metal salt intended as a cosmetic. If the salt content exceeds 20.0% by weight based on the total weight of the composition, it cannot be sufficiently dissolved in the cosmetic formulation, so it cannot be stably blended with other ingredients of the cosmetic formulation. There may be a problem.
상기 조성물은 보습제(폴리올 등), 왁스, 점도 조절제, 점증제, pH 조정제, 지방, 유기용매, 용해제, 농축제, 겔화제, 연화제, 항산화제, 현탁화제, 안정화제, 발포제(foaming agent), 방향제, 계면활성제, 이온형 유화제, 비이온형 유화제, 충전제, 금속이온봉쇄제, 킬레이트화제, 보존제(preservative), 비타민, 습윤화제, 염료, 안료, 친수성 활성제, 친유성 활성제, 지질 소낭 또는 화장품에 통상적으로 사용되는 임의의 다른 성분과 같은 화장품학 또는 피부과학 분야에서 통상적으로 사용되는 보조제를 포함할 수 있다. 상기 보조제는 화장품학 또는 피부과학 분야에서 일반적으로 사용되는 양으로 도입된다. 또한, 본 발명의 조성물은 피부 상태 개선 효과를 증가시키기 위하여 피부 흡수 촉진 물질을 포함할 수 있다.The composition includes a moisturizing agent (polyol, etc.), a wax, a viscosity modifier, a thickener, a pH adjuster, a fat, an organic solvent, a solubilizer, a thickening agent, a gelling agent, an emollient, an antioxidant, a suspending agent, a stabilizer, a foaming agent, Fragrances, surfactants, ionic emulsifiers, nonionic emulsifiers, fillers, sequestering agents, chelating agents, preservatives, vitamins, wetting agents, dyes, pigments, hydrophilic activators, lipophilic activators, lipid vesicles or cosmetics It may contain adjuvants commonly used in the field of cosmetics or dermatology, such as any other ingredients commonly used. The adjuvant is introduced in an amount generally used in the field of cosmetology or dermatology. In addition, the composition of the present invention may contain a substance that promotes skin absorption in order to increase the effect of improving the skin condition.
또한, 상기 조성물은 상술한 성분 이외에 통상적으로 물을 함유하고 있다. 물로서는, 이온 교환수, 증류수 등의 정제수를 이용하는 것이 바람직하고, 그 함유량은 특별히 한정되지 않으며, 상기 조성물에 함유되는 각 성분을 충분히 용해 또는 분산할 수 있는 양이면 무방하다.In addition, the composition usually contains water in addition to the above-described components. As water, it is preferable to use purified water such as ion-exchanged water or distilled water, and the content thereof is not particularly limited, and any amount capable of sufficiently dissolving or dispersing each component contained in the composition may be used.
상기 조성물은 유연 화장수, 영양 화장수, 에센스, 스프레이 타입, 미스트, 겔, 선크림, 메이크업베이스, 파운데이션, 비비크림, 컨실러, 립스틱, 립글로스, 립라이너, 투웨이케익, 프라이머, 팩트, 아이새도우, 블러셔, 아이라이너, 아이 마스카라, 로션, 아이 크림, 영양 크림, 마사지 크림 및 클렌징 크림으로 이루어진 군에서 선택되는 어느 하나로 제형화될 수 있으나, 이에 한정되는 것은 아니다.The composition is a flexible lotion, nourishing lotion, essence, spray type, mist, gel, sun cream, makeup base, foundation, BB cream, concealer, lipstick, lip gloss, lip liner, two-way cake, primer, pact, eye shadow, blusher, eye It may be formulated with any one selected from the group consisting of a liner, eye mascara, lotion, eye cream, nourishing cream, massage cream, and cleansing cream, but is not limited thereto.
이하, 실시예를 통하여 본 발명을 더욱 상세히 설명하고자 한다. 이들 실시예는 오로지 본 발명을 예시하기 위한 것으로서, 본 발명의 범위가 이들 실시예에 의해 제한되는 것으로 해석되지 않는 것은 당업계에서 통상의 지식을 가진 자에 있어서 자명할 것이다.Hereinafter, the present invention will be described in more detail through examples. These examples are for illustrative purposes only, and it will be apparent to those of ordinary skill in the art that the scope of the present invention is not construed as being limited by these examples.
[[ 제조예Manufacturing example 1] One] 고함량의High content 포타슘 Potassium 락테이트Lactate 및 실리콘계 오일의 혼합물을 포함하는 화장료 조성물의 제조 And Preparation of a cosmetic composition comprising a mixture of silicone oil
상업적으로 입수 가능한 포타슘 락테이트(Sigma, 60389), 스쿠알란(Sigma, 234311), 세틸아릴 알코올(Amazon, SZ Cetearyl Alcohol(50/50) 1Lb), 글리세릴 스테아레이트*PEG-100 스테아레이트, 카프릴릭/카프릭 트리글리세라이드(MakingCosmetics®, CreamMaker® BLEND), 사이클로펜타실록산(Dow Corning, XIAMETER® PMX-0245 Cyclopentasiloxane), 디메치콘(MakingCosmetics®, Dimethicone 500), 소듐 클로라이드(Sigma, S3014), 글리세린(Sigma, G2289), 소듐 벤조에이트(Sigma, 18106), EDTA(Sigma, E6758)를 이용하여, 실시예 1~8 및 비교예 1~8의 조성물을 하기 표 1~4의 조성으로 제조하였다(단위: 중량%).Commercially available potassium lactate (Sigma, 60389), squalane (Sigma, 234311), cetylaryl alcohol (Amazon, SZ Cetearyl Alcohol (50/50) 1Lb), glyceryl stearate*PEG-100 stearate, capryl Rick/Capric triglycerides (MakingCosmetics ® , CreamMaker ® BLEND), cyclopentasiloxane (Dow Corning, XIAMETER ® PMX-0245 Cyclopentasiloxane) , Dimethicone (MakingCosmetics ® , Dimethicone 500), sodium chloride (Sigma, S3014), glycerin ( Sigma, G2289), sodium benzoate (Sigma, 18106), and EDTA (Sigma, E6758) were used to prepare the compositions of Examples 1 to 8 and Comparative Examples 1 to 8 in the composition of Tables 1 to 4 below (unit : weight%).
[[ 시험예Test example 1] One] 고함량의High content 포타슘 Potassium 락테이트Lactate 및 실리콘계 오일의 혼합물을 포함하는 And a mixture of silicone oils 화장료Cosmetic 조성물의 Composition of 자극취에With irritating odor 대한 About 소취Deodorant 효과 평가 Effectiveness evaluation
제조예 1에서 제조한 실시예 1~8 및 비교예 1~8 각각의 조성물의 자극취의 정도를 Odor meter(OMX-GR, Shinyei, Japan)로 측정하였다. The degree of irritating odor of each of the compositions of Examples 1 to 8 and Comparative Examples 1 to 8 prepared in Preparation Example 1 was measured with an Odor meter (OMX-GR, Shinyei, Japan).
구체적으로, 각 조성물을 동일한 함량(0.1g)으로 60초간 Odor meter에서 3회 측정하여 평균값을 구하였다(Odor meter의 측정값(a.u.)이 높을수록 자극취/악취가 심한 것을 의미함).Specifically, each composition was measured three times in an Odor meter for 60 seconds at the same content (0.1 g) to obtain an average value (the higher the measured value (a.u.) of the Odor meter means that the irritating odor/odor is severe).
그 결과, 표 5 및 도 1에 나타낸 바와 같이, 실시예 8의 조성물은 비교예 1의 조성물 또는 비교예 2의 조성물보다 현저하게 자극취를 소취시키는 효과가 있음을 확인하였다. As a result, as shown in Table 5 and FIG. 1, it was confirmed that the composition of Example 8 has the effect of remarkably deodorizing irritating odors than the composition of Comparative Example 1 or the composition of Comparative Example 2.
구체적으로, 실시예 8의 조성물은 비교예 1의 조성물보다 약 2.7배 소취 효과가 높았고, 비교예 2의 조성물보다 약 1.4배 소취 효과가 높은 것을 확인하였다.Specifically, it was confirmed that the composition of Example 8 had about 2.7 times higher deodorant effect than the composition of Comparative Example 1, and about 1.4 times higher deodorant effect than the composition of Comparative Example 2.
그밖에 실시예 1 내지 7의 조성물은 실시예 8의 조성물과 동등한 정도의 소취 효과가 있음을 확인하였고, 비교예 3 내지 7의 조성물은 비교예 2의 조성물과 동등한 정도의 소취 효과가 있음을 확인하였다(데이터 미제시).In addition, it was confirmed that the compositions of Examples 1 to 7 had a deodorizing effect equivalent to that of the composition of Example 8, and the compositions of Comparative Examples 3 to 7 were confirmed to have a deodorizing effect equivalent to that of the composition of Comparative Example 2. (Data not shown).
[[ 시험예Test example 2] 2] 고함량의High content 포타슘 Potassium 락테이트Lactate 및 실리콘계 오일의 혼합물을 포함하는 And a mixture of silicone oils 화장료Cosmetic 조성물의 피부 Composition of the skin 자극감Irritation 평가 evaluation
제조예 1에서 제조한 실시예 1~8 및 비교예 1~8 각각의 조성물을 20명의 피검자 군을 대상으로 도포하여 피부 자극 정도를 확인하였다.The composition of each of Examples 1 to 8 and Comparative Examples 1 to 8 prepared in Preparation Example 1 was applied to a group of 20 subjects to check the degree of skin irritation.
구체적으로, 각 피검자는 먼저, 세안 후 약 15분간 휴식을 취한 후, 실시예 1~8 및 비교예 1~8 각각의 조성물을 양쪽 뺨과 눈가에 적당량(예컨대, 0.5g)으로 도포하고 약 10분간 기다린 다음, 피부 자극감의 정도, 즉 피부의 따가움, 화끈거림, 가려움 및 눈/눈가의 시림의 정도로 4가지 항목에서 총 6점 척도로 각 피검자별로 의견을 청취하여 점수화한 다음, 피검자 20명의 점수 결과를 평균값으로 계산하여 피부 자극감을 평가하였다. 여기서, 각 항목의 점수가 높으면 피부의 따가움, 화끈거림, 가려움, 눈/눈가의 시림의 정도가 높은 것을 의미하며, 아래 표 6의 평가 기준으로 피부 자극감을 평가하였다.Specifically, each subject first took a rest for about 15 minutes after cleansing, and then applied the composition of each of Examples 1 to 8 and Comparative Examples 1 to 8 in an appropriate amount (e.g., 0.5 g) to both cheeks and around the eyes, and then about 10 After waiting for a minute, the degree of skin irritation, that is, the degree of skin irritation, burning, itching, and aching in the eyes/eye area, was scored by listening to the opinions of each subject on a total of 6 points on a scale of 6 points, and then scored by 20 subjects. The result was calculated as an average value to evaluate skin irritation. Here, if the score of each item is high, it means that the degree of skin irritation, burning, itchiness, and eye/eye sensation is high, and skin irritation was evaluated according to the evaluation criteria in Table 6 below.
그 결과, 표 7 및 도 2에 나타낸 바와 같이, 실시예 8의 조성물은 비교예 1의 조성물 또는 비교예 2의 조성물보다 피부 자극감(또는 피부 통증감)의 정도가 낮아 사용감이 개선되는 효과가 있음을 확인하였다. 구체적으로, 실시예 8의 조성물은 피부의 따가움, 화끈거림, 가려움 및 눈/눈가의 시림의 정도가 평균적으로 1 이하의 점수를 얻어 피부 자극감이 거의 없는 것으로 평가된 반면, 비교예 1 및 비교예 2의 조성물은 모든 항목에서 피부 자극감에 대한 평가점수가 높게 나타나 피부 자극감이 높은 것으로 확인되었다. 특히, 실시예 8의 조성물은 비교예 1 및 비교예 2 각각의 조성물보다 피부 자극감 중 피부의 통증, 즉 피부의 따가움, 피부의 화끈거림 및 눈/눈가의 시림의 정도가 현저하게 낮은 것을 확인하였다. As a result, as shown in Table 7 and FIG. 2, the composition of Example 8 has an effect of improving the feeling of use because the degree of skin irritation (or skin pain) is lower than that of the composition of Comparative Example 1 or the composition of Comparative Example 2. Was confirmed. Specifically, the composition of Example 8 was evaluated as having little skin irritation by obtaining a score of 1 or less on average in the degree of skin irritation, burning, itching, and aching in the eyes/eye areas, whereas Comparative Example 1 and Comparative Example The composition of 2 showed a high evaluation score for skin irritation in all items, and it was confirmed that the skin irritation was high. In particular, it was confirmed that the composition of Example 8 significantly lowered the degree of skin pain, that is, skin irritation, skin burning, and eye/eye irritation than the respective compositions of Comparative Example 1 and Comparative Example 2. .
그밖에 실시예 1 내지 7의 조성물은 실시예 8의 조성물과 동등한 정도의 피부 자극(통증) 강하 효과로 사용감이 개선되는 것을 확인하였고, 비교예 3 내지 7의 조성물은 비교예 2의 조성물과 동등한 정도의 피부 자극감이 있는 것을 확인하였다(데이터 미제시).In addition, it was confirmed that the composition of Examples 1 to 7 improved the feeling of use with a skin irritation (pain) lowering effect equivalent to that of the composition of Example 8, and the compositions of Comparative Examples 3 to 7 were equivalent to those of the composition of Comparative Example 2. It was confirmed that there was a feeling of skin irritation (data not shown).
[[ 시험예Test example 3] 3] 고함량의High content 포타슘 Potassium 락테이트Lactate 및 실리콘계 오일의 혼합물을 포함하는 And a mixture of silicone oils 화장료Cosmetic 조성물의 피부 Composition of the skin 보습력Moisturizing power 개선 효능 평가 Evaluation of improvement efficacy
제조예 1에서 제조한 실시예 1~8 및 비교예 1~8 각각의 조성물의 피부 보습력 개선 효과를 20명의 피검자 군을 대상으로 확인하였다. The effect of improving skin moisturizing power of each of the compositions of Examples 1 to 8 and Comparative Examples 1 to 8 prepared in Preparation Example 1 was confirmed in a group of 20 subjects.
구체적으로, 매일 2회씩 4주간 각 피검자의 오른팔에 실시예 1~8의 조성물을 도포하고, 왼팔에 비교예 1~8의 조성물을 도포한 다음, 도포 전과, 도포 후 1주, 2주, 4주가 경과한 시점, 및 도포를 중지한 후 2주가 경과한 시점(즉, 시험 개시 후, 총 6주가 경과된 시점)에 항온, 항습 조건(24℃, 상대습도 40%)에서 피부 수분량 측정기(Corneometer CM825, C+K Electronic Co, 독일)로 각 피검자의 피부 수분량을 측정한 다음, 피검자 20명의 피부 수분량을 평균값으로 계산하여 피부 보습력 개선 여부를 평가하였다.Specifically, the compositions of Examples 1 to 8 were applied to the right arm of each subject twice a day for 4 weeks, and the compositions of Comparative Examples 1 to 8 were applied to the left arm, and then before and after application, 1 week, 2 weeks, 4 The skin moisture level meter (Corneometer) under constant temperature and humidity conditions (24°C, 40% relative humidity) at the time when the week has elapsed, and at the time that 2 weeks have elapsed after the application is stopped (ie, 6 weeks have elapsed after the start of the test). CM825, C+K Electronic Co, Germany) was used to measure the skin moisture content of each subject, and then the skin moisture content of 20 subjects was calculated as an average value to evaluate whether the skin moisturizing ability was improved.
그 결과, 표 8에 나타낸 바와 같이, 각 조성물의 도포 전에 측정한 피부 수분량 값을 기준으로 1주, 2주, 4주 및 6주의 기간별로 증가분을 백분율로 표시하였을 때 실시예 8의 조성물은 도포 후 6주가 경과된 시점에서 비교예 1의 조성물 및 비교예 2의 조성물보다 현저하게 피부 보습 효과가 높은 것을 확인하였다. As a result, as shown in Table 8, the composition of Example 8 was applied as a percentage of the increase for each period of 1 week, 2 weeks, 4 weeks and 6 weeks based on the skin moisture value measured before application of each composition. After 6 weeks elapsed, it was confirmed that the skin moisturizing effect was significantly higher than the composition of Comparative Example 1 and the composition of Comparative Example 2.
그밖에 실시예 1 내지 7의 조성물은 실시예 8의 조성물과 동등한 정도의 피부 보습 효과를 나타내는 것을 확인하였고, 비교예 3 내지 7의 조성물은 비교예 2의 조성물과 동등한 정도로 피부 보습 효과가 거의 없는 것을 확인하였다(데이터 미제시).In addition, it was confirmed that the compositions of Examples 1 to 7 exhibited a skin moisturizing effect equivalent to that of Example 8, and the compositions of Comparative Examples 3 to 7 had almost no skin moisturizing effect to the same extent as the composition of Comparative Example 2. Confirmed (data not shown).
[[ 시험예Test example 4] 4] 고함량의High content 포타슘 Potassium 락테이트Lactate 및 실리콘계 오일의 혼합물을 포함하는 화장료 조성물의 제형 안정도 평가 And formulation stability evaluation of a cosmetic composition comprising a mixture of silicone oil
제조예 1에서 제조한 실시예 1~8 및 비교예 1~8 각각의 조성물의 제형 안정도를 확인하기 위해, 각각의 조성물 약 25mL를 100mL 시료 용기에 넣은 다음, -10℃~45℃의 온도범위에서 시간별로 온도가 변화하는 기기인 사이클 챔버(Cycle chamber)로 상기 온도범위에서 냉동/해동 과정을 반복하고, 약 185rpm의 속도로 1주일간 흔들어주면서 조성물 분리층 형성 여부를 육안으로 관찰하여 제형 안정도를 평가하였다.In order to check the formulation stability of each of the compositions of Examples 1 to 8 and Comparative Examples 1 to 8 prepared in Preparation Example 1, about 25 mL of each composition was placed in a 100 mL sample container, and then a temperature range of -10 °C to 45 °C. In the cycle chamber, which is a device whose temperature changes by time, the freezing/thawing process is repeated in the above temperature range, and shaken at a speed of about 185 rpm for 1 week to visually observe whether a composition separation layer is formed, and the formulation stability Evaluated.
그 결과, 표 9에 나타낸 바와 같이, 실시예 1~8의 조성물은 비교예 1, 비교예 2 및 비교예 3~8 각각의 조성물보다 제형 안정도가 높은 것을 확인하였다.As a result, as shown in Table 9, it was confirmed that the compositions of Examples 1 to 8 have higher formulation stability than the respective compositions of Comparative Examples 1, 2, and 3 to 8.
종합하면, 본 발명에 따른 고함량의 락테이트 금속염 및 실리콘계 오일의 혼합물을 포함하는 W/S형 화장료 조성물은 락테이트 금속염으로부터 유래되는 자극취 또는 불쾌취를 소취시켜 사용감을 개선시킬 뿐만 아니라, 화장학적 용도로서 피부 상태 개선 효과, 특히 피부 자극감을 저감시키고, 피부 보습력을 개선시키는 효과가 우수한 것을 확인하였다. In summary, the W/S-type cosmetic composition comprising a mixture of a high content lactate metal salt and a silicone oil according to the present invention not only improves the feeling of use by deodorizing irritating or unpleasant odors derived from lactate metal salts, but also cosmetic As a use, it was confirmed that the effect of improving skin condition, particularly, reducing skin irritation and improving skin moisturizing power, is excellent.
이상으로 본 발명 내용의 특정한 부분을 상세히 기술하였는바, 당업계의 통상의 지식을 가진 자에게 있어서, 이러한 구체적 기술은 단지 바람직한 실시양태일 뿐이며, 이에 의해 본 발명의 범위가 제한되는 것이 아닌 점은 명백할 것이다. 따라서 본 발명의 실질적인 범위는 첨부된 청구항들과 그것들의 등가물에 의하여 정의된다고 할 것이다. As described above, specific parts of the present invention have been described in detail, and for those of ordinary skill in the art, it is obvious that this specific description is only a preferred embodiment, and the scope of the present invention is not limited thereby. something to do. Therefore, it will be said that the practical scope of the present invention is defined by the appended claims and their equivalents.
Claims (9)
According to claim 1, wherein the composition is characterized in that to alleviate the irritation response of the skin, W / S type cosmetic composition.
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JP4758599B2 (en) | 2001-01-18 | 2011-08-31 | 太陽誘電株式会社 | Granular magnetic thin film and manufacturing method thereof, laminated magnetic film, magnetic component, electronic device |
EP2166875A1 (en) | 2007-06-07 | 2010-03-31 | PURAC Biochem BV | Method for removing odor from vinegar |
JP5756107B2 (en) | 2009-08-26 | 2015-07-29 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | Process for producing a crystalline solid having sufficiently low hygroscopicity from glycine-N, N-diacetic acid derivative I |
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