KR20190115873A - Manufacturing method of alkarine mineral water - Google Patents

Abstract

The present invention relates to a method of manufacturing alkaline mineral water, and more specifically, to a method of manufacturing alkaline mineral water, which comprises: a mineral firing step of firing mineral; a mineral mixing step of mixing the mineral fired through the mineral firing step and an additive with purified water to prepare a mixture; a carbonate injection step of injecting a carbonate into the mixture prepared through the mineral mixing step to obtain a carbonate-injected mixture; a mineral extraction step of applying pressure to the carbonate-injected mixture obtained through the carbonate injection step while heating and stirring the carbonate-injected mixture, thereby obtaining a mineral-extracted mixture; a centrifuging step of centrifuging the mineral-extracted mixture obtained through the mineral extraction step and separating solids to obtain a solid-separated mixture; and an aging step of aging the solid-separated mixture obtained through the centrifuging step. The alkaline mineral water manufactured through the foregoing processes exhibits excellent absorption rate with respect to animals and plants by containing large amounts of mineral components of a colloidal phase, and exhibits effects beneficial to the interior of the body even when the alkaline mineral water is taken for a long period of time by showing weak alkalinity.

Description

Method of producing alkaline mineral water {MANUFACTURING METHOD OF ALKARINE MINERAL WATER}

The present disclosure relates to a method for preparing alkaline mineral water, and more particularly, alkaline minerals, which contain a large amount of mineral components in colloidal form, exhibit excellent absorption rate for animals and plants, and have weak alkalinity, and thus have a beneficial effect in the body even when taken for a long time. It relates to a method for producing water.

Minerals play an important role in regulating and maintaining various physiological functions in the body, affecting water balance, equilibrium of acids and alkalis, neurotransmission and endocrine system, and generating, consuming, growing and maintaining health. It is involved in all metabolic actions of our body.

Since mineral components are not made through synthesis in the body, they must be consumed through food, etc. As plants grow, they absorb minerals contained in seawater or soil, and animals can obtain minerals by ingesting plants.

The extent to which minerals are used in our bodies is influenced by many factors in the body, such as the interaction between minerals and minerals, and the interaction between vitamins and minerals.

Magnesium, iron, calcium, and copper are all divalent ions, which are similar in size and charge, so they compete with each other when absorbed, affecting their mutual utilization and metabolism. Vitamin D also helps to absorb calcium. , Vitamin C enhances the absorption of iron.

Minerals can be divided into two types according to their needs. Generally, minerals that require more than 100 mg per day are classified into macro minerals and ordinary minerals that do not require large amounts. Magnesium, sodium, potassium, sulfur and chlorine.

As described above, since minerals play an important role in the body of animals and plants, efforts to extract and utilize minerals through artificial methods continue.

Conventionally, the technique related to the mineral extraction method was first developed by Dr. Kawada of Japan in the 1990s. The method of extracting natural rocks at high temperature and high pressure using inorganic acids such as sulfuric acid, and the number of minerals extracted by the above method It is diluted with and is used for various animals and plants.

However, the mineral water extracted by the above method proceeds with the activation of strong acidic ions, so that when the animals and plants take edible organic acid for a long time, the minerals that have undergone the activation of strong acidic ions on a principle similar to that of releasing various heavy metals into the body When water is taken for a long time, various mineral components in the body are discharged in the form of sulphate and the like, and there is a problem in that the actual body mineral absorption rate is low.

Korean Patent Registration No. 10-1239540 (2013.02.26) Korea Patent Registration No. 10-1658352 (2016.09.12)

Disclosed is a method for producing an alkaline mineral water containing a large amount of the mineral component of the colloidal phase shows an excellent absorption rate for animals and plants, and weak alkalinity, which shows a beneficial effect in the body even when taken for a long time.

As an example, the contents of the present disclosure are a mineral firing step of calcining minerals, a mineral mixing step of mixing minerals and additives calcined through the mineral firing step with purified water, and a carbonate salt in the mixture prepared through the mineral mixing step. Injecting the carbonate injection step, the mineral extraction step of applying pressure while heating and stirring the mixture in which the carbonate is injected through the carbonate injection step, the centrifugal separation to filter the solids by centrifuging the mixture extracted minerals through the mineral extraction step It describes a method for producing alkaline mineral water, characterized in that consisting of a step of aging step of aging the mixture filtered solids through the centrifugation step.

Preferably, the mineral firing step may be performed for 2 to 4 hours at a temperature of 1100 to 1300 ℃.

More preferably, the mineral mixing step is mixed with 1 to 20 parts by weight of minerals and 0.1 to 2 parts by weight of additives calcined through the mineral firing step to 100 parts by weight of purified water and for 20 to 30 hours at a temperature of 70 to 90 ℃ Can be done.

More preferably, the mineral may be made of one or more selected from the group consisting of mica, germanium, illite, zeolite, clay and heavy soil.

Even more preferably, the additive may be at least one selected from the group consisting of magnesium, phosphoric acid, calcium oxide, borax, molybdenum, potassium chloride and potassium.

Even more preferably, the carbonate injection step may be performed by injecting 5 to 30 parts by weight of carbonate to 100 parts by weight of the mixture prepared through the mineral mixing step and stirring for 8 to 12 hours at a temperature of 70 to 90 ℃.

Even more preferably, the carbonate may be at least one selected from the group consisting of sodium carbonate, calcium carbonate, sodium bicarbonate and potassium bicarbonate.

Even more preferably, the mineral extraction step may be performed for 90 to 150 minutes at a pressure of 1 to 5kgf at a temperature of 70 to 90 ℃.

Alkaline mineral water production method as described above has a large amount of the mineral component of the colloidal phase shows an excellent absorption rate for animals and plants, and because it shows weak alkalinity, it shows an excellent effect showing a beneficial effect in the body even if taken for a long time.

1 is a flowchart illustrating a method of preparing the disclosed alkaline mineral water.

In the following, preferred embodiments of the present invention and the physical properties of each component will be described in detail, which is intended to explain in detail enough to be able to easily carry out the invention by one of ordinary skill in the art, This does not mean that the technical spirit and scope of the present invention is limited.

The disclosed method for producing alkaline mineral water includes a mineral firing step (S101) of firing minerals, a mineral mixing step (S103) of mixing minerals and additives calcined through the mineral firing step (S101) with purified water (S103), and the mineral mixing step ( Carbonate injection step (S105) of injecting carbonate into the mixture prepared through S103), mineral extraction step (S107) of applying pressure while heating and stirring the mixture into which the carbonate is injected through the carbonate injection step (S105), the mineral extraction A centrifugation step (S109) of filtering the solids by centrifuging the mixture from which the mineral is extracted through step (S107) and a maturing step (S111) of aging the mixture of the solids filtered through the centrifugation step (S109).

The mineral firing step (S101) is a step of firing a mineral that serves to supply mineral components to the mineral water produced through the disclosed method, and after washing the mineral to remove impurities remaining on the surface and put in the firing furnace 1100 to Heating at a temperature of 1300 ° C. for 2-4 hours.

When the calcination process is performed for the above temperature and time, impurities and heavy metal components contained in the minerals are removed, and impurities are removed and a fine pore layer is formed in the remaining space, so that the specific surface area is improved. Improve efficiency

If the firing temperature is less than 1100 ℃ or the firing time is less than 2 hours, the above effects are insignificant, and if the firing temperature exceeds 1300 ℃ or the firing time exceeds 4 hours, a temperature range and time sufficient to sinter minerals It is not preferable in terms of energy saving.

At this time, the mineral is preferably made of one or more selected from the group consisting of mica, germanium, illite, zeolite, clay and heavy soil, mica 100 parts by weight, germanium 90 to 110 parts by weight, illite 50 to 100 parts by weight, More preferably, the zeolite consists of 50 to 100 parts by weight, 20 to 100 parts by weight of clay and 20 to 100 parts by weight of heavy soil, and preferably has a particle size of 150 to 325 mesh.

When the particle size of the mineral is less than 150 mesh, minerals are easily scattered and workability is lowered. When the particle size of the mineral exceeds 325 mesh, the elution efficiency of minerals contained in the mineral is lowered.

The mineral mixing step (S103) is a step of mixing the mineral fired through the mineral firing step (S101) with purified water, 1 to 20 parts by weight of minerals fired through the mineral firing step (S101) to 100 parts by weight of purified water And 0.1 to 2 parts by weight of the additive and stirred at a temperature of 70 to 90 ° C. for 20 to 30 hours.

In addition, the mineral mixing step (S103) is made by mixing 100 parts by weight of purified water and 1 to 20 parts by weight of minerals in a mixing device equipped with a stirrer, if the mineral content is less than 1 part by weight, the minerals are not sufficiently extracted, When the content of the mineral exceeds 20 parts by weight, the stirring process may not proceed properly, and the amount of the mineral to be extracted is not large compared to the amount of the mineral to be injected, which is not economically desirable.

At this time, the additive is made of one or more selected from the group consisting of magnesium, phosphoric acid, calcium oxide, borax, molybdenum, potassium chloride and potassium, and when the additive consisting of the above components are mixed, not only minerals, but also a large amount of beneficial components to the human body The mineral water contained is provided.

The carbonate injection step (S105) is a step of injecting carbonate to the mixture prepared through the mineral mixing step (S103), 5 to 30 parts by weight of carbonate to 100 parts by weight of the mixture prepared through the mineral mixing step (S103) Inject and agitate at a temperature of 70-90 ° C. for 8-12 hours.

The carbonate injected through the carbonate injection step (S105) serves to extract the minerals contained in the mineral. As described above, the mixture containing 5 to 30 parts by weight of the carbonate is adjusted to a pH of 7.5 to 8.5 to about It will show alkalinity.

When the content of the carbonate is less than 5 parts by weight, the amount of extraction of minerals contained in the minerals is reduced, and when the content of the carbonate exceeds 30 parts by weight, the extraction efficiency of the minerals contained in the minerals is not greatly improved and the manufacturing cost is reduced. Is increased.

At this time, the carbonate is preferably made of one or more selected from the group consisting of sodium carbonate, potassium carbonate, sodium bicarbonate and potassium bicarbonate.

If the temperature in the carbonate injection step (S105) is less than 70 ℃ or stirring time is less than 8 hours, the extraction efficiency of minerals contained in the mineral is lowered, if the temperature exceeds 90 ℃ or stirring time exceeds 12 hours The extraction efficiency of minerals contained in minerals is undesirable because it increases the manufacturing cost without significantly improving.

The mineral extraction step (S107) is a step of extracting the minerals contained in the mineral by applying pressure while heating and stirring the mixture in which the carbonate is injected through the carbonate injection step (S105), through the carbonate injection step (S105) The mixture into which the carbonate is injected is heated for a temperature of 70 to 90 ° C. while applying a pressure of 1 to 5 kgf for 90 to 150 minutes.

In the mineral extraction step (S107) made of the above conditions, a large amount of the mineral contained in the mineral is eluted. When the pressure is less than 1 kgf in the mineral extraction step (S107), the elution efficiency of the mineral contained in the mineral is lowered, and the mineral If the pressure exceeds 5 kgf in the extraction step (S107), the dissolution efficiency of the minerals contained in the mineral is not preferable because a separate device for maintaining excessive pressure should be provided.

The centrifugation step (S109) is a step of filtering solids by centrifuging the mixture from which minerals are extracted through the mineral extraction step (S107), and centrifuging the mixture from which minerals are extracted through the mineral extraction step (S107). It is added to and centrifuged for 30 to 40 minutes to remove the solids contained in the mixture.

After the centrifugation step (S109) consisting of the above process, the mixture is removed and solids are removed.

The aging step (S111) is a step of ripening the mixture of the solid content filtered through the centrifugation step (S109), the solid content filtered through the centrifugation step (S109) to stand at room temperature for 30 to 50 hours to mature It's a step

At this time, the mineral water containing the mineral having regular activity and adsorption power is provided through the aging step (S111), if the time of the aging step (S111) is less than 30 hours, the aging of the mineral water is not completely made, the aging If the time of step (S111) exceeds 50 hours to continue the aging process even after the aging of the mineral water is completed to reduce the efficiency of the manufacturing process.

After the aging step (S111), the production of homogeneous and stabilized alkaline mineral water is completed.

Hereinafter, the physical properties of the disclosed alkaline mineral water and the alkaline mineral water produced through the preparation method will be described with reference to Examples.

<Manufacture example 1>

100 g of mica, 100 g of germanium, 75 g of zeolite, 75 g of zeolite, 60 g of clay and 60 g of heavy soil were mixed and washed, and then charged into a kiln and fired at a temperature of 1200 ° C. for 3 hours to prepare a calcined mineral.

<Manufacture example 2>

100 g of heavy soil and 50 g of germanium were mixed and washed, and then charged into a kiln and calcined at a temperature of 1200 ° C. for 3 hours to prepare a calcined mineral.

<Manufacture example 3>

100 g of heavy soil and 100 g of germanium were mixed and washed, and then charged into a kiln and calcined at a temperature of 1200 ° C. for 3 hours to prepare a calcined mineral.

<Example 1>

8 parts by weight of calcined minerals prepared in Preparation Example 1 and 0.9 parts by weight of additives (0.3 parts by weight of potassium, 0.3 parts by weight of magnesium, 0.3 parts by weight of calcium oxide) of 100 parts by weight of purified water (manufactured by refined rock water) The mixture was stirred for 24 hours at a temperature of 80 ° C. to prepare a mixture, and carbonates (sodium carbonate, calcium carbonate, sodium bicarbonate and potassium bicarbonate were mixed at a weight portion of 1: 1: 1: 1 by weight to 100 parts of the prepared mixture). Inject parts by weight and stir for 10 hours at a temperature of 80 ℃ to prepare a mixture of carbonate injected, and extract the mineral contained in the mineral by applying a pressure of 3 kgf for 120 minutes while heating the mixture to a temperature of 80 ℃, The mixture from which minerals were extracted was put into a centrifuge and centrifuged for 35 minutes to remove solids, and the mixture from which the solids were removed was aged by standing for 40 hours at room temperature. To prepare a number of mineral province.

<Example 2>

2 parts by weight of calcined minerals prepared by Preparation Example 2 and 100 parts by weight of purified water and additives (0.3 part by weight of phosphoric acid, 0.03 part by weight of borax, 0.02 part by weight of molybdenum, 0.5 part by weight of calcium oxide, 0.6 part by weight of potassium chloride) The mixture was mixed to prepare a mixture by stirring at a temperature of 80 ° C. for 24 hours, and carbonates (sodium carbonate, calcium carbonate, sodium bicarbonate and potassium bicarbonate were mixed at a weight of 1: 1: 1: 1) by weight of the prepared mixture. 15 parts by weight was injected and stirred at a temperature of 80 ° C. for 10 hours to prepare a mixture in which carbonate was injected, and the mixture was heated to a temperature of 80 ° C. under a pressure of 3 kgf for 120 minutes to extract minerals contained in the mineral. The mixture was extracted with minerals, centrifuged for 35 minutes to remove solids, and the mixture was removed for 40 hours at room temperature. Turn to prepare a number of alkaline minerals.

<Example 3>

1 part by weight of the calcined mineral prepared in Preparation Example 3 and 1.5 parts by weight of an additive (0.3 part by weight of potassium oxide, 1.2 parts by weight of calcium oxide) were mixed with 100 parts by weight of purified water, and stirred at a temperature of 80 ° C. for 24 hours. 1 part by weight of carbonate (sodium carbonate) was added to 100 parts by weight of the prepared mixture and stirred at a temperature of 80 ° C. for 10 hours to prepare a mixture in which carbonate was injected, and the mixture was heated to a temperature of 80 ° C. of 3 kgf. Pressure was applied for 120 minutes to extract the minerals contained in the mineral, the mixture was extracted into the centrifuge and centrifuged for 35 minutes to remove the solids, and the solids-free mixture was left at room temperature for 40 hours. Aged by the method to prepare alkaline mineral water.

The components of the alkaline mineral water prepared through Examples 1 to 3 are shown in Table 1 below.

(However, the components of the alkaline mineral water prepared in Examples 1 to 3 were confirmed using ICP mass spectrometry using ICP equipment.)

TABLE 1

As shown in Table 1 above, it can be seen that the mineral water produced through the disclosed method of producing alkaline mineral water has excellent mineral content.

At this time, the mineral water prepared through Example 1 is suitable for drinking water because the content of calcium, magnesium, sodium, potassium, phosphorus, sulfur, germanium, iron, zinc and selenium is excellent, and prepared through Example 2 The prepared mineral water is suitable for use in plant cultivation, and the mineral water prepared in Example 3 is suitable for animal feed.

Therefore, the disclosed method for producing alkaline mineral water has a high content of colloidal mineral components, shows excellent absorption rate for animals and plants, and shows weak alkalinity.

S101; Mineral firing stage
S103; Mineral Mixing Step
S105; Carbonate injection stage
S107; Mineral extraction stage
S109; Centrifugation Step
S111; Ripening step

Claims (8)

Mineral firing step of firing minerals;
A mineral mixing step of mixing minerals and additives calcined through the mineral firing step with purified water;
A carbonate injection step of injecting carbonate into the mixture prepared through the mineral mixing step;
A mineral extraction step of applying pressure while heating and stirring the mixture into which the carbonate is injected through the carbonate injection step;
A centrifugal separation step of filtering solids by centrifuging the mixture from which minerals are extracted through the mineral extraction step; And
Method for producing an alkaline mineral water, characterized in that consisting of; a aging step of aging the mixture of the solid content filtered through the centrifugation step.
The method according to claim 1,
The mineral firing step is a method for producing alkaline mineral water, characterized in that for 2 to 4 hours at a temperature of 1100 to 1300 ℃.
The method according to claim 1,
The mineral mixing step is mixed with 1 to 20 parts by weight of minerals and 0.1 to 2 parts by weight of additives calcined through the mineral firing step to 100 parts by weight of purified water, characterized in that made for 20 to 30 hours at a temperature of 70 to 90 ℃ Method for producing alkaline mineral water.
The method according to any one of claims 1 to 3,
The mineral is a method of producing alkaline mineral water, characterized in that consisting of one or more selected from the group consisting of mica, germanium, illite, zeolite, clay and heavy soil.
The method according to claim 1 or 3,
The additive is a method of producing alkaline mineral water, characterized in that consisting of at least one selected from the group consisting of magnesium, phosphoric acid, calcium oxide, borax, molybdenum, potassium chloride and potassium.
The method according to claim 1,
The carbonate injection step is prepared by injecting 5 to 30 parts by weight of carbonate to 100 parts by weight of the mixture prepared by the mineral mixing step and the alkaline mineral water, characterized in that the mixture is stirred for 8 to 12 hours at a temperature of 70 to 90 ℃ Way.
The method according to claim 1 or 6,
The carbonate is a method of producing alkaline mineral water, characterized in that consisting of at least one selected from the group consisting of sodium carbonate, calcium carbonate, sodium bicarbonate and potassium bicarbonate.
The method according to claim 1,
The mineral extraction step is a method for producing alkaline mineral water, characterized in that made for 90 to 150 minutes at a pressure of 1 to 5kgf at a temperature of 70 to 90 ℃.