KR20190003160A - Perfume Composition for Enhancing the Long-lasting Effects of Fragrance, and Cosmetic Composition Containing the Same - Google Patents

Abstract

The present invention relates to a perfume composition which enhances persistence of fragrance and a cosmetic composition comprising the same. More particularly, the present invention relates to a perfume composition comprising at least one selected from the group consisting of Clearwood^tm, Dartanol, Heliotropine and Polysantol, which enhances similarity to a main fragrance by specific perfume(s) contained in conventional cosmetic compositions and the persistence of the main fragrance, Galaxolide 70 MIP, Helvetolide and Muscenone delta as active ingredients, and to a cosmetic composition comprising the perfume composition.

Description

TECHNICAL FIELD [0001] The present invention relates to a perfume composition for enhancing perseverance, and a cosmetic composition comprising the same. [0002]

The present invention relates to a perfume composition which improves the perseverance of fragrance and a cosmetic composition containing the fragrance composition. More specifically, the present invention relates to a perfume composition which is similar to the main fragrance of a specific perfume (s) At least one member selected from the group consisting of Clearwood tm, Dartanol, Heliotropine and Polysantol, which improve the durability, and at least one member selected from the group consisting of Galaxolide 70 MIP, A perfume composition comprising Helvalolide and Muscenone Delta as an active ingredient, and a cosmetic composition comprising the perfume composition.

Generally, consumers who use shampoo, body cleanser and soap want to keep the fragrance soft and long lasting. However, domestic shampoos, body cleansers and soaps use a lot of fragrance which is not long-lasting fragrance or fruity fragrance, and it is insufficient to meet consumer's desire in fragrance persistence. Therefore, there is a desperate need for a technique to maintain a certain tendency, for example, a pleasant fragrance, while maintaining the same.

The only way to keep the streak longer is simply to combine it with high-volatility (bp) fragrances, but since the fragrance is too heavy, the fragrance of the product is refreshed and the feeling of coolness can not be felt at all . In order to solve this problem, there is a method of increasing the sustainability by capturing the fragrance which is volatilized by using a fragrant holding agent (fixative), but this also causes the fragrance of the fragrance to be deteriorated. There is also a way to increase the fragrance's uptake rate, but this is not a fundamental solution because it increases the cost of the product and most of the products are flushed with water.

On the other hand, the persistency of the specific fragrance (s) by the method of selecting a substance that increases the persisting power of the specific fragrance (s) contained in the cosmetic composition based on the solubility (LogP) of the fragrance to water and the degree of volatility (Korean Patent Registration No. 10-1230933). However, the composition is different from the fragrance ingredients contained in the perfume composition of the present invention.

Under these technical backgrounds, the inventors of the present invention have found that 80 kinds of fragrance (s) known to be strong in the continuity of the existing fragrance series that improve the similarity with the fragrance (scent) and the persistence of the fragrance At least one selected from the group consisting of Clearwood tm, Dartanol, Heliotropine and Polysantol selected from the group consisting of Galaxolide 70 MIP, A perfume composition comprising Helvetolide and Muscenone Delta as an active ingredient and a cosmetic composition comprising the perfume composition may be used when the incidence of specific perfume (s) contained in a cosmetic composition (e.g., shampoo) (Reverberation effect) of the specific fragrance (s) without a large change in the flavor (s) of the fragrance (s) to improve the palatability of the specific fragrance (s) Group, while the sustainability of the strike was also found that to obtain the effect of improving and completing the present invention.

It is an object of the present invention to provide a perfume composition which improves the sustaining power of the perfume.

Another object of the present invention is to provide a cosmetic composition comprising the perfume composition.

It is still another object of the present invention to provide a cosmetic product made from the cosmetic composition.

In order to attain the above object, the present invention provides a method for producing a microcapsule comprising at least one selected from the group consisting of Clearwood tm, Dartanol, Heliotropine and Polysantol, Galaxolide 70 MIP), Helvetolide, and Muscenone Delta as active ingredients.

The present invention also provides a cosmetic composition comprising the perfume composition.

The present invention also provides cosmetics made from the cosmetic composition.

When the long-lasting fragrance base prepared using the perfume composition according to the present invention is incorporated into a cosmetic composition containing a specific perfume (s), the propensity of the specific perfume (s) contained in the cosmetic composition (Reverberation effect) of the specific fragrance (s) can be improved while maintaining the similarity of the fragrance (s), and the effect of improving the persistence of the fragrance can be obtained while satisfying the preference for the specific fragrance (s) contained in the cosmetic composition .

Unless otherwise defined, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. In general, the nomenclature used herein is well known and commonly used in the art.

In one embodiment of the present invention, a shampoo (cosmetic composition) containing 80 kinds of fragrance ingredients known to have strong durability of existing fragrance series was subjected to the olfactory sensory test of a professional steamer, and 13 kinds of different fragrance ingredients (Such as Acropal, Clearwood, Cyclogalbanate, Dartanol, Fruitate, Galaxolide 70 MIP, Heliotropine, Helvetolide, Koumalactone, Muscenone Delta, Polysantol, Undecalactone Gamma and Verdyl Propionate) were selected (see, for example, Test Examples 1 and 2).

In another embodiment of the present invention, the thirst of the specific fragrance (s) contained in the shampoo is maintained, and the sustaining ability of the fragrance (Dexanol), which contains seven different flavor components (Clearwood tm, Dartanol, Galaxolide 70 MIP, Heliotropine, Helvetolide, Muscenone Delta and Polysantol) were selected (see Test Example 3).

In another embodiment of the present invention, when the selected seven different fragrance ingredients are mixed as a combination fragrance in a specific blending ratio, the fragrance or fragrance of the fragrance (s) contained in the shampoo is similar to that of the fragrance The optimal mixing ratio was confirmed by the sensory evaluation of the olfactory senses of the professional and ordinary people. As a result, as a result of verifying seven kinds of fragrance component candidates based on the olfactory sensory evaluation, it was found that the persistency of the specific fragrance (s) contained in the shampoo was excellent in the range of 3 to 10% by weight, , And the similarity of the specific fragrance (s) contained in the shampoo was found to be excellent in the range of 1 to 5 wt%, and lower than 7 wt% (see Test Example 4).

In another embodiment of the present invention, when the selected seven different fragrance ingredients are used as combined fragrance, the effect of improving the similarity of the fragrance (s) of the fragrance (s) regardless of the fragrance series of the fragrance Was confirmed by the sensory evaluation of the olfactory sensibility of the professional and ordinary people. As a result, in the shampoo containing the perfume showing the floral fragrance, the perfume showing the oriental fragrance or the perfume showing the chypre fragrance, (See Test Example 5).

Accordingly, the present invention provides, in one aspect, at least one selected from the group consisting of Clearwood tm, Dartanol, Heliotropine and Polysantol, and at least one selected from the group consisting of Galaxolide 70 MIP), Helvetolide, and Muscenone Delta as active ingredients.

In the present invention, the scent includes citrus fragrance (for example, citrus flavor such as orange, lemon and grapefruit), Floral Fragrance (such as roses, jasmine, lily of the valley) Fruity fragrance (for example, fragrance of apples, pears, peaches, etc.), Oriental fragrance (e.g. spice, balsam, resin and animalic combined flavor), Chypre Fragrance , Aromatherapy fragrance (for example, a herb flavor such as lavender, rosemary, eucalyptus, etc.), a citrus top note, an osmosis, a resin and a flavor combined with a base component) , Preferably a perfume (flavor) exerted in a cosmetic composition containing an aroma-based component well known and commonly used in the art, In that the perfume (fragrance) is exerted in a cosmetic oil it may be characterized.

In the present invention, the total weight of the active ingredient may be 0.1 to 99.9% by weight, based on the total weight of the perfume composition, and the total weight of the active ingredient may be less than 0.1% ), It is impossible to obtain an effect of improving the sustaining ability of the specific perfume (s).

In the present invention, the perfume composition contains 5 to 10% by weight, preferably 5% by weight, of clearwood (Clearwood tm) based on the total weight of the composition, preferably 5 to 40% (Galaxolide 70 MIP) containing 10 to 30% by weight, preferably 20 to 30% by weight, and 5 to 10% by weight, preferably 10 to 30% by weight, of Dartanol, (Helvetolide) containing 5 to 30% by weight, preferably 5 to 30% by weight and preferably 15 to 20% by weight, of Heliotropin, And 20% by weight of Muscenone Delta, and 5% to 10% by weight, preferably 5% by weight, of Polysantol.

In the present invention, the perfume composition may be incorporated into a fragrance, deodorant, oil, gel, beads, plug-in, or the like including a diffuser, a candle, and a room spray, but is not limited thereto.

In the present invention, the perfume composition may be used as a long-lasting fragrance base of the cosmetic composition.

In another aspect, the present invention relates to a cosmetic composition comprising the perfume composition.

In the present invention, the cosmetic composition may be used in combination with a citrus flavor (for example, a citrus flavor such as orange, lemon or grapefruit), a floral fragrance (such as a rose, a jasmine or a lily of the valley) (Fruity Fragrance) (for example, an apple, a pear, a peach, etc.), an Oriental Fragrance (for example, a spice, a balsam, a resin and an animal combined with a basic component), a Chypre Fragrance (For example, fragrance of a citrus top note, an oak musk, a resin and a flavor combined with a base component) and an aromatic flavor (e.g., a herb flavor such as lavender, rosemary, eucalyptus, etc.) , Preferably a cosmetic composition containing a flavor-based ingredient which is well known and commonly used in the art A it can be characterized.

In the present invention, when the content of the perfume composition is less than 1% by weight based on the total weight of the cosmetic composition, it is impossible to obtain the effect of improving the sustaining ability of the specific perfume (s) contained in the cosmetic composition. %, The fragrance composition of the specific fragrance (s) contained in the cosmetic composition may be changed, so that the fragrance composition may be used in an amount of 1 to 10% by weight, preferably 3 to 20% by weight, 5% by weight, and most preferably 5% by weight.

In the present invention, the cosmetic composition containing the perfume composition is not particularly limited in formulation, but may be perfume, softener, astringent lotion, nutritional lotion, eye cream, nutritional cream, massage cream, cleansing cream, cleansing foam, Cleansing Water, Powder, Essence, Shampoo, Rinse, Pack, Ointment, Lotion, Burnable, Suspension, Emulsion, Cream, Gel, Spray, Puffing Agent, Warning Agent, Patch Agent, Water Paste, Hair Tonic, Hair Nourishing Lotion, Scalp Treat Hair lotions, hair shampoos, hair lotions, pomades, and the like. The cosmetic composition of each of these formulations may contain various components that are formulated in a conventional cosmetic composition according to the above-described various formulations or for a final purpose, and the kind and amount of these components can be easily selected by those skilled in the art.

Representative base components and additives will be described below taking as an example a typical shampoo composition of the cosmetic composition containing the above-mentioned perfume composition.

For example, in the case of a shampoo formulation, in a shampoo composition composed of a synthetic surfactant, a cleaning component, a preservative, a thickener and a viscosity adjusting agent, a pH adjusting agent, a perfume, a dye, a hair conditioning agent and water, The surfactant may be any selected from anionic, amphoteric, and nonionic surfactants. The synthetic surfactant may be contained in an amount of 10 to 70% by weight, preferably 10 to 30% by weight, based on the total weight of the composition.

Examples of the synthetic anionic surfactant include alkyl and alkyl ether sulfates. Specific examples thereof include sodium lauryl sulfate, ammonium lauryl sulfate, triethanolamine lauryl sulfate, sodium polyoxyethylene lauryl sulfate and polyoxyethylene lauryl sulfate. have.

The synthetic amphoteric surfactants are alkyl betaines and alkylamidopropyl betaines. Specific examples thereof include cocodimethylcarboxymethylbetaine, lauryldimethylcarboxymethylbetaine, lauryldimethyl alpha-carboxyethylbetaine, cetyldimethylcarboxymethyl Betaine, cocamidopropyl betaine, and the like.

Examples of the synthetic nonionic surfactant include alkanolamide and amine oxide. Specific examples thereof include lauryldiethylamine oxide, palm oil alkyldimethylamine oxide, lauric acid diethanolamide, palm oil fatty acid diethanolamide, palm oil fatty acid monoethanolamide .

The optional ingredients used in the cosmetic compositions according to the present invention are well known to those skilled in the art as conventional optional ingredients to maintain basic properties and quality. Such optional ingredients may include preservatives, thickeners, viscosity modifiers, pH adjusting agents, perfumes, dyes, hair conditioning agents, and the like.

The cosmetic composition according to the present invention can be used according to a conventional method of use, and the number of times of use may be varied depending on a user's hair condition, skin condition, or taste.

In another aspect, the present invention relates to cosmetics made from the cosmetic composition.

Hereinafter, the present invention will be described in more detail with reference to Examples. It is to be understood by those skilled in the art that these examples are for illustrative purposes only and that the scope of the present invention is not construed as being limited by these examples.

[ Test Example  One] Cosmetics  Of the perfume contained in the composition Inclinational  Screening of fragrance ingredients to improve persistence

A total of 80 commercially available fragrances were selected by a professional proprietor based on the following four odor evaluation criteria.

< Flavor Evaluation Standard >

(i) Neat: the fragrance state of the cosmetic composition containing the fragrance-sustaining fragrance (s) (the fragrance state of the shampoo contained in the container before application to the skin / hair);

(ii) Blooming: the fragrance state expressed upon application of the skin / hair of the cosmetic composition containing the fragrance-sustaining fragrance (s) (e. g., the sustained state of the hair when shampooed);

(iii) Swatch: A state in which the skin / hair to which the cosmetic composition containing the fragrance-sustaining fragrance (s) is applied contains excess water (for example, a state of being soaked in wet hair immediately after shampooing) ; And

(iv) Lasting: A state in which the skin / hair applied with the cosmetic composition containing the fragrance-sustaining fragrance (s) lasts after a certain time (for example, the fragrance state of the hair after 12 hours after shampooing).

More specifically, fragrance ingredients that prolong the persistence of fragrance (e.g., the fragrance contained in the cosmetic composition) were evaluated by a professional perfumer using the olfactory sensory evaluation (Survey criteria: Neat, Blooming, Swatch, and Lasting, but add up to a score of 10 on each scale to calculate a score of 40 on a 10-point scale. [1 point] Very low - [4 points] [10 points] very high ').

The content of each fragrance ingredient added to the shampoo (cosmetic composition) was 5 wt% based on the total weight of the shampoo, and the inversion rate was selected to be 0.5%.

As a result, as shown in Tables 1 and 2 below, based on the olfactory sensibility evaluation, it was found that the total of 13 fragrance components (i.e., Acropal, Clearwood, But are not limited to, Cyclogalbanate, Dartanol, Fruitate, Galaxolide 70 MIP, Heliotropine, Helvetolide, Koumalactone, (Muscenone Delta), Polysantol, Undecalactone Gamma and Verdyl Propionate) were selected.

The following Table 1 shows the results of the olfactory sensory evaluation of 80 kinds of fragrance components based on the four fragrance evaluation criteria on a scale of 10 points by the evaluator (professional vertebra) And the average value.

Sample number Name of sample neat
(neat) Buruming
(blooming) Swatch
(swatch) Lasting
(lasting) Control group Lilial 6.0 6.0 5.0 4.0 #One Acropal 7.4 7.5 5.6 4.6 #2 Aldehyde C11 Undecylenic 7.4 6.9 4.5 3.1 # 3 Aldehyde C11 Undecylic 6.6 6.7 5.8 3.6 #4 Aldehyde C-6 8.6 7.6 4.9 2.7 # 5 Allyl Amyl Glycolate 8.3 8.3 6.0 3.1 # 6 Aldehyde MNA 7.4 6.1 5.0 3.7 # 7 Anethol 8.1 7.3 5.7 3.3 #8 Anisaldehyde 7.2 6.4 5.4 3.5 # 9 Anysyl Acetate 5.7 5.6 5.0 3.0 # 10 Applinate 8.4 7.1 4.8 2.8 # 11 Bacdanol 6.4 6.3 5.3 3.8 # 12 Benzyldimethylcarbinol Acetate 6.4 6.1 5.9 2.9 # 13 Benzyldimethylcarbinol Butyrate 7.4 6.9 6.1 3.7 # 14 Ethyl Butyrate 8.8 8.0 5.6 2.8 # 15 Calone 6.2 6.2 5.6 4.2 # 16 Cashmeran 7.8 8.3 7.6 3.3 # 17 Centifolether 7.8 7.3 5.1 3.0 # 18 Cetalox 5.8 5.5 5.1 4.9 # 19 Cinnamic Alcohol 7.5 6.0 5.3 3.1 # 20 Cinnamyl Propionate 7.0 5.8 5.4 3.5 # 21 Cis Jasmon 6.3 5.9 5.1 3.3 # 22 Citronellol 7.7 7.4 5.4 4.0 # 23 Clearwood 6.9 7.4 6.3 5.5 # 24 Clonal 9.6 9.4 8.7 7.5 # 25 Coranol 6.4 5.7 4.6 2.8 # 26 Corps Racine 6.4 5.4 5.6 4.2 # 27 Coumarin 7.1 6.0 5.4 3.9 # 28 Cyclogalbanate 7.7 7.6 7.5 5.0 # 29 Cyclomethylene Citronellol 5.4 5.9 6.8 5.3 # 30 Cyclosal 6.8 6.8 6.0 4.0 # 31 Damascone Alpha 7.5 7.2 6.3 3.8 # 32 Dartanol 6.2 5.3 4.8 4.8 # 33 Decalactone Gamma 7.3 7.5 5.8 2.8 # 34 Decyl Acetate 7.3 6.8 6.3 2.5 # 35 Delphone 7.7 7.7 6.8 3.3 # 36 Damascone Delta 7.6 7.2 6.9 4.3 # 37 Dihydroestragole 8.6 7.8 6.1 2.9 # 38 Dihydro Linalol 7.0 5.8 5.4 2.4 # 39 Dihydromyrcenol 6.8 5.8 4.3 2.6 # 40 Doremox 8.0 7.4 6.9 3.4 # 41 Dynascone 7.8 7.0 6.9 3.4 # 42 Ethyl Linalol 7.1 6.4 5.2 3.2 # 43 Ethyl Methylphenylglycidate 7.1 6.1 4.9 3.4 # 44 Ethyl Maltol 7.5 7.2 6.4 2.2 # 45 Ethyl Vanillin 8.1 7.6 6.3 2.8 # 46 Eugenol 7.9 7.6 5.8 4.0 # 47 Floralozone 7.3 6.9 6.7 4.6 # 48 Fruitate 7.7 6.2 6.6 5.5 # 49 Galaxolide  70 MIP 6.4 6.6 6.7 6.3 # 50 Geraniol 7.7 6.4 5.7 2.8 # 51 Hedion 5.6 5.1 5.4 2.9 # 52 Heliopropanal 7.0 7.0 5.9 3.6 # 53 Heliotropin 6.8 5.5 7.2 5.2 # 54 Helvetolide 7.1 7.4 6.2 5.9 # 55 Hexylcinnamic Aldehyde 6.6 7.0 7.0 3.9 # 56 Indol 8.0 7.9 6.4 3.6 # 57 Isocyclocitral 7.9 6.0 5.9 3.4 # 58 Isoeugenol 8.3 7.6 6.6 4.0 # 59 Koumalactone 7.3 6.9 6.1 5.2 # 60 Lilial 6.0 6.0 5.0 4.0 # 61 Linalol 7.2 5.7 4.5 2.7 # 62 Methyl Anthranilate 7.3 7.0 5.5 4.2 # 63 methyllonone Alpha Iso 7.8 7.2 6.6 3.8 # 64 Mousse Cristal 5.3 5.1 5.1 4.0 # 65 Muscenone  Delta 7.3 7.3 6.4 5.5 # 66 Nonalactone Gamma 7.2 7.1 5.3 2.9 # 67 Norlimbanol 7.1 6.6 4.9 3.8 # 68 Phenylethyl Alcohol 7.0 6.6 4.9 2.7 # 69 Phenoxy 5.2 4.8 4.0 2.9 # 70 Pyrazobutyle 7.3 6.4 4.5 3.0 # 71 Hexenyl Acetate 8.4 7.4 4.8 3.0 # 72 Cis-3 Hexenol 7.6 5.7 6.5 4.5 # 73 Polysantol 6.3 6.5 5.6 5.9 # 74 Raspberry Ketone 5.6 5.4 4.5 3.3 # 75 Undecalactone  Gamma 7.9 8.0 7.5 6.1 # 76 Verdyl  Propionate 7.5 6.9 5.9 4.8 # 77 Zestover 8.1 6.9 4.3 3.1 # 78 Patchouli oil 8.7 8.2 6.1 4.8 # 79 Cedarwood oil Virginia 7.8 5.8 4.6 2.4 # 80 Lavandin Grosso ARR 7.9 7.2 4.7 2.9

Table 2 shows thirteen kinds of fragrance components selected by the evaluator (professional steerer) of 80 kinds of fragrance components selected by the olfactory sensibility evaluation based on the four fragrance evaluation criteria.

Sample number Name of sample Flavor #A Acropal Aldehyde green #B Clearwood Woody (patchouli) #C Cyclogalbanate Green woody herbal #D Dartanol Ambery leathery musky #E Fruitate Aromatic herbal #F Galaxolide  70 MIP Musk #G Heliotropin Sweet, animalic #H Helvetolide Musk #I Koumalactone Coconut #J Muscenone  Delta Powdery #K Polysantol Woody (sandalwood) #L Undecalactone Gamma Fruity aldehyde #M Verdyl Propionate Fruity (pineapple) herbal

[ Test Example  2] Cosmetics  Screening of fragrance ingredients to improve the consistency and flavor similarity of the fragrance contained in the composition

The effect of the fragrance components on the maintenance (similarity) and persistence of the original fragrance (s) contained in the cosmetic composition when the conventional cosmetic composition contains the 13 fragrance components of Table 2 of the above Experimental Example 1 And the optimum fragrance components were selected.

More specifically, one kind of fragrance component is added to a shampoo (cosmetic composition) containing fragrance (s) of fragrance such as flower fragrance or fruit fragrance, and then, after 8 hours has elapsed, The optimum fragrance ingredients that maintain the original fragrance (s) of the fragrance (s) contained in the shampoo and prolong the persistence of the original fragrance (s) 10 point scale is evaluated as [10 points], [1 point] is very low - [4 points] is just - 10 point is very high ).

The content of each of the fragrance ingredients added to the shampoo (cosmetic composition) was 5% by weight based on the total weight of the shampoo, and the odds ratio was selected to be 1.0%.

As a result, as shown in Tables 3 and 4 below, thirteen flavor component candidates were verified based on the olfactory sensory evaluation, and as a result, Galaxolide 70 MIP, Helvetolide, The perfume composition containing Muscenone Delta as an active ingredient was excellent in improving the sustaining power and similarity of the perfume of the perfume (s) contained in the shampoo (cosmetic composition).

The following Table 3 shows the results of the tendency of the fragrance (s) contained in the shampoo obtained from the olfactory sensory evaluation of 13 kinds of fragrance components (10 experts from professional and general people; S1 to S10) on a scale of 10 points (Blank: shampoo without flavor ingredients).

rater Blank #A #B #C #D #E #F #G #H #I #J #K #L #M S1 4 4 5 4 4 5 6 5 6 5 5 6 4 4 S2 4 4 5 5 5 5 7 6 6 5 5 7 5 5 S3 4 6 6 5 5 5 7 5 7 6 6 7 6 5 S4 4 4 5 4 5 6 7 5 7 5 7 6 4 4 S5 4 5 5 5 4 5 7 6 6 5 6 5 5 5 S6 4 4 5 5 4 5 6 5 6 6 6 5 5 4 S7 4 4 4 4 4 5 7 6 6 6 7 5 6 5 S8 4 5 6 5 5 6 6 5 7 6 7 6 5 5 S9 4 3 4 3 4 5 7 5 6 6 6 6 5 4 S10 4 4 5 4 4 5 6 5 6 5 6 5 4 4 Average 4.0 4.3 5 4.4 4.4 5.2 6.6 5.3 6.3 5.5 6.1 5.8 4.9 4.5

The following Table 4 shows the scent similarity results of fragrance (s) contained in the shampoo obtained by evaluating the flavor components of 13 kinds of fragrance components by the evaluator (professional irrigation and general person) on a scale of 10 points.

rater #A #B #C #D #E #F #G #H #I #J #K #L #M S1 2 5 2 6 One 6 4 5 3 6 5 One One S2 2 4 2 5 One 5 3 4 2 6 4 One 2 S3 2 5 One 6 One 6 4 6 One 5 4 One One S4 One 3 One 4 One 5 3 5 One 5 3 2 One S5 3 5 One 5 2 6 4 6 3 5 3 One 2 S6 2 5 2 5 One 6 4 5 2 6 5 One 2 S7 2 5 2 6 One 6 4 5 One 6 3 One One S8 3 6 4 6 2 6 3 5 3 6 4 One 2 S9 2 4 2 4 One 5 4 4 One 5 4 One 2 S10 2 4 One 4 One 6 4 5 2 5 4 One 2 Average 2.1 4.6 1.8 5.1 1.2 5.7 3.7 5 1.9 5.5 3.9 1.1 1.6

[ Test Example  3] Optimum flavor Combination ( Steering  evaluation

Based on the results of Test Example 2, seven kinds of fragrance components were selected from thirteen candidates to prepare fragrance combinations at different mixing weight ratios, and then the fragrance component (s) such as flower fragrance or fruit fragrance (Sweeteners) in the shampoo (cosmetic composition), the similarity and persistence of the flavor (s) contained in the shampoo by the combination at the elapsed time of 8 hours was evaluated by a professional irrigation sensory evaluation The evaluation criteria are as follows: 1) Very low - [4 points] Slightly - [10 points] Very high High ').

The content of each of the fragrance components added to the shampoo (cosmetic composition) was 5 to 40% by weight based on the total weight of the shampoo, and the odor sensitivity was evaluated to be 1.0%.

As a result, as shown in Tables 5 to 7 below, seven kinds of fragrance ingredient candidates were verified based on the olfactory sensory evaluation, and as a result, the persistence of the fragrance (s) contained in the shampoo (cosmetic composition) The combination of # 1, # 2, #, and # was superior in the order of combination, and the similarity of the perfume (s) contained in the shampoo (cosmetic composition) , Followed by the combination of #, #, and #.

Therefore, it was confirmed that the combination of # 1 was the most excellent in terms of the continuity of the perfume (s) contained in the shampoo (cosmetic composition) and the similarity of the propensity.

Table 5 below shows the composition of a fragrance combination comprising seven fragrance components (figure: weight%).

Name of sample Combination Spice Number #end #I #All #la #hemp #bar #four Clearwood 10 5 5 5 5 10 10 Dartanol 20 20 5 30 10 40 40 Galaxolide 70 MIP 20 30 30 30 10 10 20 Heliotropin 5 5 5 5 10 10 5 Helvetolide 20 5 20 15 30 10 10 Muscenone Delta 20 30 30 10 30 10 10 Polysantol 5 5 5 5 5 10 5 Total content (% by weight) 100 100 100 100 100 100 100

Table 6 below shows the tenacity of the fragrance (s) contained in the shampoo obtained by evaluating the taste combination of the flavor combination comprising the seven flavor components (professional and general) .

rater #F #end #I #All #la #hemp #bar #four S1 6 9 8 7 8 8 8 7 S2 7 10 8 8 9 8 7 8 S3 7 9 9 7 8 8 8 8 S4 7 9 8 8 9 7 8 7 S5 7 10 7 8 8 8 7 7 S6 6 9 7 7 8 7 6 7 S7 7 10 8 8 7 8 8 7 S8 6 8 7 6 7 8 6 8 S9 7 9 8 8 9 7 7 7 S10 6 9 7 7 8 9 6 6 Average 6.6 9.2 7.7 7.4 8.1 7.8 7.1 7.2

The following Table 7 shows the scent similarity results of the fragrance (s) contained in the shampoo obtained by evaluating the odorant combination composed of seven kinds of fragrance components by the evaluator (professional irrigation and general public) on a scale of 10 points.

rater #F #end #I #All #la #hemp #bar #four S1 6 4 8 7 9 8 5 4 S2 5 5 8 8 8 8 5 5 S3 6 5 7 7 8 9 6 5 S4 5 4 7 7 9 6 4 4 S5 6 5 6 6 9 7 5 6 S6 6 5 7 7 7 8 5 5 S7 6 4 7 6 9 8 5 4 S8 6 6 6 7 8 7 7 6 S9 5 5 7 5 8 6 5 5 S10 6 6 7 7 8 7 6 5 Average 5.7 4.9 7 6.7 8.3 7.4 5.3 4.9

[ Test Example  4] Cosmetics  The fragrance in the composition Combination  Evaluation of optimum combination content

(Fragrance combination) is added to the cosmetic composition containing the fragrance (s) of the fragrance series such as the fragrance of flowers or the fragrance of the fruit and then the fragrance components added at the time of 8 hours elapse after the shampoo The optimum combination content of the fragrance ingredients required to maintain the original fragrance of the fragrance contained in the composition and to extend the persistence of the original fragrance was determined by a professional irrigation and general public using the olfactory sensibility evaluation 10 point scale is evaluated as [10 points], [1 point] is very low - [4 points] is just - 10 point is very high ).

Here, the mixing ratio of the combination was determined on the basis of Test Example 3 using the mixing ratio of the combination of #la.

The content of each of the fragrance ingredients added to the shampoo (cosmetic composition) was 1 to 10% by weight based on the total weight of the shampoo, and the odor sensitivity was evaluated to be 1.0%.

As a result, as shown in Tables 8 and 9 below, seven kinds of fragrance component candidates were verified based on the olfactory sensory evaluation, and as a result, the persistence of the fragrance (s) in the shampoo (cosmetic composition) 10% by weight and less than 1% by weight, and the similarity of the perfume (s) contained in the shampoo (cosmetic composition) was excellent in the range of 1 to 5% by weight, Respectively.

The following Table 8 shows the tenacity tenacity results of the fragrance (s) contained in the shampoo obtained from the olfactory sensory evaluation of the seven kinds of fragrance components by the evaluator (professional and general public) (Blank: Shampoo not included).

rater Shampoo with a combination of '#la' Blank 1 wt% 3 wt% 5 wt% 7 wt% 10 wt% S1 4 4 6 8 9 10 S2 4 5 6 9 9 9 S3 4 5 6 8 9 9 S4 4 4 7 9 9 10 S5 4 4 5 8 8 10 S6 4 4 7 8 9 9 S7 4 5 6 7 9 10 S8 4 4 5 7 8 10 S9 4 4 7 9 9 9 S10 4 4 5 8 8 9 Average 4 4.3 6 8.1 8.7 9.5

The following Table 9 shows a ten-point scale of the similarity results of the fragrance (s) contained in the shampoo obtained by evaluating the olfactory sensibility of the seven kinds of fragrance components by the evaluator (professional irrigation and general public).

rater Shampoo with a combination of '#la' 1 wt% 3 wt% 5 wt% 7 wt% 10 wt% S1 10 9 9 4 2 S2 10 8 8 5 2 S3 9 9 8 5 2 S4 9 9 9 4 One S5 10 10 9 5 3 S6 9 8 7 5 3 S7 9 9 9 4 3 S8 10 9 8 6 4 S9 10 9 8 5 2 S10 9 8 8 6 3 Average 9.5 8.8 8.3 4.9 2.5

[ Test Example  5] Cosmetics  Verification of suitability of fragrance composition to fragrance series of fragrance contained in composition

Persistent durability of the perfume (s) contained in the cosmetic composition by the perfume composition containing 7 kinds of perfume ingredients in Test Examples 3 to 4 has been verified and it has been confirmed that the persistence of the perfume (s) It was found that even if a cosmetic composition containing different kinds of fragrance (s) of fragrance series was used by using a combination of #la, the seven fragrance ingredients (S) contained in the cosmetic composition by the perfume composition containing the perfume composition of the present invention is improved.

That is, the fragrance series (for example, citrus fragrance, citrus fragrance such as orange, lemon, grapefruit and the like), fragrance such as rose, jasmine and lily of the valley as floral fragrance; Fruity fragrance is a fragrance of apples, pears, peaches, etc. Oriental Fragrance is a combination of Spice, Balsam, Resin and Animal as basic ingredients Chip Fragrance (Citrus Fragrance) A shampoo containing a perfume (s) of a perfume (s), such as a perfume, a perfume, a perfume, a perfume, a perfume, a perfume, a perfume, a top note, an oakmoss, a resin, , A cosmetic composition containing a flavor-based component which is commonly known and commonly used, or a cosmetic composition containing the cosmetic composition) , And 8 hours later, the professional irrigation and general public evaluated the olfactory sensory evaluation (evaluation criteria in the questionnaire: similarity of the tendency, each calculated on a scale of 10 points; (S) contained in the cosmetic composition was confirmed through the "very low - very low - [4 points] just so - [10 points] very high".

The content of each of the fragrance ingredients added to the shampoo (cosmetic composition) was 5 wt% based on the total weight of the shampoo, and the odor sensitivity was evaluated to be 1.0%.

As a result, as shown in the following Table 10, fragrance compositions containing seven kinds of fragrance components were verified based on the olfactory sensory evaluation. As a result, fragrance exhibiting Floral Fragrance, Oriental Fragrance It was confirmed that the similarity of intestines to each flavor was highest in the shampoo containing the fragrance or the fragrance exhibiting the flavor fragrance (Chypre Fragrance).

The following Table 10 shows the flavor (s) contained in the cosmetic composition obtained by evaluating the odor sensation by the evaluator (professional rheologist and the general public) on the suitability of the perfume composition containing seven kinds of fragrance components to the fragrance series of the fragrance contained in the shampoo, The results of the similarity of the direction of the 10 points scale.

rater Shampoo with a combination of '#la' Citrus fragrance
(Citrus Fragrance) Flower scent
(Floral
Fragrance) Fruit fragrance
(Fruity Fragrance) Oriental fragrance
(Oriental Fragrance) Chiffon fragrance
(Chypre Fragrance) Aromatic Scent
(Aromatic Fragrance) S1 4 8 6 10 9 3 S2 3 7 5 8 8 3 S3 3 7 6 9 8 2 S4 2 8 7 9 9 3 S5 3 7 6 8 8 3 S6 2 8 7 9 8 2 S7 3 6 5 8 9 3 S8 3 8 6 7 8 4 S9 3 7 6 8 9 3 S10 4 8 5 9 8 3 Average 3 7.4 5.9 8.5 8.4 2.9

While the present invention has been particularly shown and described with reference to specific embodiments thereof, those skilled in the art will appreciate that such specific embodiments are merely preferred embodiments and that the scope of the present invention is not limited thereby. something to do. It is therefore intended that the scope of the invention be defined by the claims appended hereto and their equivalents.

Claims (10)

And at least one selected from the group consisting of Clearwood tm, Dartanol, Heliotropine and Polysantol and at least one selected from the group consisting of Galaxolide 70 MIP, Helvetolide ) And Muscenone Delta as an active ingredient.
The method according to claim 1, wherein the scent is selected from the group consisting of Citrus Fragrance, Floral Fragrance, Fruity Fragrance, Oriental Fragrance, Chypre Fragrance and Aromatic Fragrance. &Lt; RTI ID = 0.0 &gt; 1, &lt; / RTI &gt;
The perfume composition according to claim 1, wherein the total weight of the active ingredient is from 0.1 to 99.9% by weight, based on the total weight of the composition.
The perfume composition of claim 1, wherein the perfume composition comprises 5 to 10% by weight of Clearwood tm, 5 to 40% by weight of Dartanol, 10 to 30% 5 to 30% by weight of Helvololide, 10 to 30% by weight of Muscenone Delta, and 5 to 30% by weight of Galaxolide 70 MIP, 5 to 10% by weight of Heliotropin, And 10% by weight of polyglycolic acid, and 10% by weight of Polysantol.
A cosmetic composition comprising the perfume composition according to any one of claims 1 to 4.
The cosmetic composition according to claim 5, wherein the cosmetic composition is selected from the group consisting of Citrus Fragrance, Floral Fragrance, Fruity Fragrance, Oriental Fragrance, Chypre Fragrance and Aromatic Fragrance And at least one kind of perfume exhibiting at least one kind of aroma selected from the group consisting of:
6. The cosmetic composition according to claim 5, wherein the perfume composition comprises 1 to 10% by weight based on the total weight of the cosmetic composition.
6. The cosmetic composition according to claim 5, wherein the composition further comprises at least one selected from the group consisting of surfactants, preservatives, thickeners, viscosity regulators, pH adjusting agents, perfumes, dyes and hair conditioning agents.
The composition according to claim 5, wherein the composition is selected from the group consisting of perfume, softening agent, convergent lotion, nutritional lotion, eye cream, nutritional cream, massage cream, cleansing cream, cleansing foam, cleansing water, powder, essence, shampoo, Hair lotion, hair shampoo, hair lotion, hair lotion, hair lotion, hair lotion, hair lotion, hair lotion, Wherein the cosmetic composition is formulated into any one selected from the group consisting of sunflower oil, sunflower oil, and pomade.
A cosmetic product produced by the cosmetic composition of claim 5.