KR20180031110A - How to create a material of the inorganic water-resistant adhesive is hardened using the process of the natural mineral and nano by him for producing a multi-inorganic adhesive - Google Patents

How to create a material of the inorganic water-resistant adhesive is hardened using the process of the natural mineral and nano by him for producing a multi-inorganic adhesive Download PDF

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KR20180031110A
KR20180031110A KR1020160119028A KR20160119028A KR20180031110A KR 20180031110 A KR20180031110 A KR 20180031110A KR 1020160119028 A KR1020160119028 A KR 1020160119028A KR 20160119028 A KR20160119028 A KR 20160119028A KR 20180031110 A KR20180031110 A KR 20180031110A
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adhesive
inorganic
materials
weight
parts
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정청식
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정청식
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D1/00Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D1/00Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
    • C09D1/02Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances alkali metal silicates
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00Inks
    • C09D11/02Printing inks
    • C09D11/04Printing inks based on proteins
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J2400/00Presence of inorganic and organic materials

Abstract

The present invention is an invention related to an adhesive comprising the inorganic materials which are not harmful to the human body, are eco-friendly, have no risk of fire at all, and are incombustible by succeeding in the preparation of 100% inorganic materials as an adhesive which is applied with inorganic materials carefully selected from the nature. A method of preparing an inorganic adhesive material of the present invention comprises: a process of selecting one or more from sodium silicate, sodium hydroxide, and potassium hydroxide to put 5 to 30 parts by weight of the selected one or more into distilled water to prepare a saturated solute solution; and a process of selecting one from silicon dioxide (SiO_2), borax, and boric acid pre-selected in the step of heating the saturated solute solution to the temperature of within 100°C, putting 2 to 20 parts by weight of the selected one into the saturated solute solution to prepare a transparent high concentrated solute solution, wherein the transparent high concentrated solute solution is prepared in the form of an over-concentrate. When manufacturing boards for construction materials, various types of molded products, and the like as an object to be adhered, i.e., matrix by using cellulose-based adhesives containing organic materials and inorganic adhesives containing inorganic materials such as ferrite, vermiculite, loess, general field soil, mineral powder, and the like, multifunctional boards can be manufactured into building interior and exterior decoration materials by using an inorganic adhesive binder of the present invention. The inorganic adhesive binder according to the present invention prevents the building materials from being slightly burnt even in conditions that heat-resistant temperature and fire-resistant temperature are poor depending on the materials, and enables the building materials to have various functional performances as inorganic materials to stand fire. The market will be dominated in advance by satisfying consumers in the future market requiring materials which are excellent in insulation performance, are eco-friendly, have incombustible performance, and do not generate carbon monoxide (CO) gas or carbon dioxide (CO_2) gas at all. The materials must be requirements in a global building material market as well as a domestic market. Therefore, the binder can be widely used as a multifunctional binder which is applicable to various uses including a floor covering adhesive, an industrial adhesive, an interlayer noise shielding agent, a toilet shed noise shielding agent, an ultra-lightweight incombustible insulation material, a texture adhesive, a board adhesive, and the like.

Description

천연 광물질을 나노의 공정을 이용하여 내수성이 강화된 무기 접착제의 물질을 조성하는 방법과 그를 이용하여 멀티 무기 접착제를 제조하는 방법{How to create a material of the inorganic water-resistant adhesive is hardened using the process of the natural mineral and nano by him for producing a multi-inorganic adhesive}BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a method for producing a multi-inorganic adhesive using a nano-process using natural minerals, and a method for producing a multi-inorganic adhesive using the same of the natural mineral and nano by him for producing a multi-inorganic adhesive}

본 발명은 천연 소재들로 채택된 친환경소재들이면서 화재의위험이 전혀 없는 불연성이며 부착성이 매우 탁월한 접착제에 관한 것이다The present invention relates to adhesives which are environmentally friendly materials which are adopted as natural materials and which are excellent in nonflammable and adhesive properties without any risk of fire

각종 유기물 소재 및 무기물 소재로 된 비드 및 파우더 등을 접착시켜 보드나 성형품등을 제조를 하고자할 때에는 유, 무기접착제 바인더를 사용하게 되는데 이에 대하여 여러 가지의 한계 때문에 활용의 범위가 제한적일 수밖에는 없었다.In order to manufacture a board or a molded product by adhering various organic materials and inorganic materials such as beads and powders, an oil or inorganic adhesive binder is used. However, due to various limitations, the range of application is limited.

내열온도는 소재에 따라 내열성은 3,000℃이상이며 내화온도는 2,000℃이상에서 견딜 수 있는 무기물질로서 다양한 내기능 성능을 갖도록 하였다.The heat resistance temperature is 3,000 ℃ or more according to the material and the refractory temperature is 2,000 ℃ or more.

앞으로의 시장에서 소비자들의 요구 사항은 단열성능이 우수하면서 친환경이여야하고 불연성이고 연소 시 일산화탄소(CO) 및 이산화탄소 (CO2) 가스가 전혀 발생 하지 않는 물질이어야 시장에서 생명력을 유지를 할 수 있을 것이다.Consumers' requirements in the future market should be environmentally friendly, non-flammable, and have no adverse effects on carbon monoxide (CO) and carbon dioxide (CO2) emissions.

국내시장은 말할 것도 없을 뿐만 아니라 글로벌 건축재의 시장에서도 당연한 요구사항임에는 틀림이 없을 것이다.Not to mention the domestic market, it is surely a requirement in the market of global construction materials.

본 바인더를 이용한 초경량불연단열재, 텍스용, 보드용, 산업체용 등 다양한 곳에 적용을 할 수 있는 멀티형 바인더로서 활용도를 넓일 수 있게 되었다.It can be utilized as a multi-type binder which can be applied to various applications such as ultra light fire retardant insulation material using a binder, text, board, and industrial use.

일반적으로, 무기 접착제란? 내열성이 뛰어나고 부착 후 내수명성이 반영구적인 특성을 가지고 있기 때문에 이를 이용한 산업 및 모든 건축재 등의 전반에 활용 범위가 점차로 늘어나고 있는 실정에 있다.In general, what is an inorganic adhesive? Since it has excellent heat resistance and semi-permanent reputation for water resistance after adhesion, the application range of the industry and all construction materials using it is gradually increasing.

그러나 무기 접착제의 내수성의 문제점과 유기 접착제들이 갖추고 있는 여러가지들의 장점들을 갖추지를 못하였지만 본 발명품은 무기 접착제로서 장기 저장을 하여도 접착제의 기본물성이 변성과 변질이 되지 않도록 하는 한편 접착력의 기능이 반영구적으로 유지되도록 한 것이다.However, although the inorganic adhesive does not have the water resistance and the various advantages of the organic adhesives, the present invention can prevent the basic properties of the adhesive from being denatured and deteriorated even when the inorganic adhesive is stored for a long period of time, Respectively.

더욱이 기존 제품들과의 경쟁력을 높이기 위한 가격 경쟁력과 품질향상 및 차별화를 시켜 줌으로서 이로 인한 수입대체 효과와 더불어 무기접착제의 시장확립하고 무기 접착제의 시장을 주도적으로 이끌어 갈 수 있는 계기가 될 것이다.Moreover, it will provide price competitiveness, quality improvement and differentiation in order to enhance competitiveness with existing products, thereby making it possible to establish a market for inorganic adhesives and to lead the market of inorganic adhesives with import substitution effect.

또한 무기 접착제가 가지고 있는 여러 가지의 장점 중에서 제조를 하는 단계에서도 환경오염을 주지 않는 친환경의 제조의 프로세스와 1차 산업을 발전시킬 수 있는 국내에서 채광을 하고 있는 광산업들의 활성화가 되는 것과, 2차 산업인 분체공장의 가동률이 높아지게 되며, 3차 산업인 접착제의 제조 공장이 가동을 함으로서 많은 은인원이 생산에 참여를 하게 되어 일자리를 창출하게 되고, 4차 산업 판매와 연구 분야 등 많은 인력들이 종사를 할 수 있는 산업이 확대가 되기도 하며, 5차산업 제품의 업그레이드를 시켜주는 연구소의 운영 및 산업과 산업을 연계를 해주는 가교적인 연결이 될 수 있으며, 및 6차 산업에서는 전세계를 연계를 하는 신 물질의 개발과 새로운 페러다임을 형성을 해주는 멀티 기능성 친환경 무기 접착제로서 우리 거주하는 주택들은 물론 이거니와 산업접반에 이르기까지 우리에게 절실히 필요로 하는 산업소재중의 매우 중요한 소재이다.In addition, among the advantages of inorganic adhesives, the process of manufacturing eco-friendly products that do not give environmental pollution even at the stage of manufacturing, and the activation of the mining industry that is developing mining industries that can develop the primary industry, As a result, the operation rate of the powder factory in the industry will increase and the manufacturing factory of the adhesive industry, which is the tertiary industry, will operate. Therefore, many silver workers will participate in production and create jobs. The industry that can do the upgrading of the 5th industrial product can be expanded and it can become a bridge linking the operation of the research institute that provides upgrading of the fifth industrial product and the industry and the industry, As a multifunctional eco-friendly inorganic adhesive that develops materials and forms new paradigms, They chose not to mention a very important material in the industrial materials which require urgent for us ranging from industrial jeopban.

더욱이 무기 접착제에서 지금까지 도달하지 못한 기술 중 제일 어려운 폴리표면에 부착을 할 수 있는 100%무기 접착제가 지금까지 존재 하지를 못하였다.Furthermore, there has been no 100% inorganic adhesive capable of attaching to the most difficult poly surface of the technology that has not yet been achieved in inorganic adhesives.

그러나 본 발명품은 플라스틱 표면은 물론 이거니와 석재류, 흙종류, 종이류 현지토를 이용하여 패널을 조성을 할 수 있을 뿐만 아니라 고온용 접착제 소성용 접착제, 자연경화용 접착제, 각종 유기 물질인 톱밥, 왕겨, 볏짚, 폴리 화이버 등을 Matrix로 이용하여 가벼운 불연성 텍스와 보드, 샌드위치패널 등을 만들 수 있는 기초 바인더로서 이용을 할 수 있도록 하였다.However, the present invention is not only capable of forming a panel using the plastic surface but also using stone soils, soil types, and paper soils, as well as being capable of forming a panel using a high temperature adhesive firing adhesive, a natural hardening adhesive, various organic materials such as sawdust, , And polyfibers as matrices to make light nonflammable textiles, boards and sandwich panels.

지금까지 매우 불이나 혹은 화기만으로도 폭발을 하거나 인화가 되는 화약과 다름없는 소재인 스티로폼은 석유에서 뽑아낸 물질을 이용하여 만들어졌기 때문에 이의 소재에 난연성을 아무리 업그레이드를 시켜주어도 연소성 물질을 불연화를 시켜주는 데에는 한계점에 도달을 할 수 밖에는 없다.Styrofoam, which is a material that is explosive or flammable, is a material that is extracted from petroleum. Therefore, even if the flame retardancy is upgraded to its material, the combustion material is unfavorably softened. There is no other way to reach the limit in giving.

그러나 본 발명품은 100% 무기 소재로 조성된 물질은 3,000℃가 되어야 용융점이 되는 초고온용 무기물질들로 조성이 되어져 있기 때문에 불로 인하여 연소 및 배연가스로부터 염려는 제로이며 방음성과 호흡성은 그 어느 건축자재 보다 우수하고, 내수 명성은 반영구적이며 친환경성이라 다 사용을 하고 남은 자재나 혹은 수명이 다되어 버릴때 에는 제2차의 환경오염을 주지를 않는 멀티기능성 친환경 접착제의 제조에 관한 것이다.However, since the material of the present invention is composed of inorganic materials of ultra-high temperature which becomes a melting point at a temperature of 3,000 ° C, the material of 100% inorganic material is zero, so there is no concern about combustion and flue gas. Which is superior in terms of water resistance, is a semi-permanent and eco-friendly, and relates to the production of a multi-functional environmentally friendly adhesive which does not give secondary pollution to the remaining materials or when the life span is over.

문헌 1. 특허등록번호 제200253964호 (2001.10.31등록)Document 1. Patent Registration No. 200253964 (registered on October 31, 2001) 문헌 2. 특허등록번호 제101240667 호(2013.02.28 등록)Document 2. Patent Registration No. 101240667 (Registered on Feb. 28, 2013) 문헌 3. 특허공개번호 제101155639 호(2012.06.05 등록)Document 3. Patent Publication No. 101155639 (registered on June 5, 2012) 문헌 4. 실용신안등록번호 제100563366호 (2006.03.15등록)Document 4. Utility Model Registration No. 100563366 (Registered on March 15, 2006)

따라서 본 발명은 이러한 종래의 결점을 해소하기 위하여 안출된 것으로, 본 발명의 해결과제는, 무기접착제가 가지고있는 열악한 조건들을 개성읗 k여 주는것은 물론 다양한 곳에 적용을 할 수 있도록 해주는 발명의 목적이다.SUMMARY OF THE INVENTION Accordingly, it is an object of the present invention to solve the conventional drawbacks of the prior art, and it is an object of the present invention to provide a method of applying various conditions to inorganic adhesives, .

무기 접착력의 문제점들 중에서 물성의 변질이 되지 않도록 하는 한편 접착력의 기능이 외부적인 요인으로 말미암아 물성이 변하지 않으면서 반영구적으로 성능이 유지되도록 한 것이다.In order to prevent deterioration of physical properties among the problems of inorganic adhesive force, the performance of the adhesive force is maintained semi-permanently without changing physical properties due to external factors.

더욱이 기존의 무기 접착제의 제품들과의 제품의 ??리티와 가격경쟁력을 높이기 위한 종합적인 품질향상 및 차별화를 시켜 줌으로서 이로 인한 수입대체 효과와 더불어 무기접착제의 시장을 주도적으로 이끌어 갈 수 있는 계기가 될 것이다.Furthermore, it provides comprehensive quality improvement and differentiation to enhance the product competitiveness and price competitiveness of products with existing inorganic adhesive products, thereby leading the market of inorganic adhesives along with import substitution effect .

더욱이 무기 접착제를 이용하여 지금까지 도달하지 못한 기술 중 제일 어려운 폴리표면에 부착을 할 수 있는 접착제로서 100%무기 접착제가 존재 하지를 못하였다.Furthermore, the use of an inorganic adhesive has failed to provide a 100% inorganic adhesive as an adhesive capable of adhering to the most difficult poly surface of the technology that has not been achieved so far.

그러나 본 발명품은 플라스틱 표면은 물론 이거니와 종이접착제, 석재류, 흙종류, 현지토를 이용하여 패널을 조성을 할 수 있을 뿐만 아니라 고온용 접착제 소성용 접착제, 자연경화용 접착제, 각종 유기 물질인 톱밥, 왕겨, 볏집, 폴리화이버등을 모재(Matrix)로 이용하여 이를 표면에 코팅을 하여 압축 건조를 하여 가벼운 불연 텍스와 보드, 샌드위치 패널 등을 만들 수 있는 기초 바인더로서 이용을 할 수 있도록 하였으며 또한 바닥 접착로서 도 매우 적합하게 적용을 할 수 있도록 하였다.However, the present invention can not only provide a plastic surface but also a panel using a paper adhesive, a stone material, a soil type, and a local soil, as well as an adhesive for firing high temperature adhesives, a natural hardening adhesive, sawdust , Straw, and polyfibers as a matrix, coated on the surface, and then compressed and dried to be used as a base binder for making light incombustible textiles, boards, sandwich panels, etc. Also, So that it can be applied very well.

지금까지 화약이나 오일과 다름없는 스티로폼은 석유에서 뽑아낸 물질을 이용하여 만들어졌기 때문에 이를 우리가 임의로 난연성을 아무리 업그레이드를 시켜주어도 연소성 물질을 불연화에는 불가능 하다.So far, styrofoam, which is just like gunpowder or oil, was made using materials extracted from petroleum, so it is impossible to unburden combustible materials even if we upgrade the flame retardancy arbitrarily.

그러나 본 발명품인 무기 접착제는 원래 불연성무기물 조합물질들로서 100% 무기 소재로 조성된 물질은 3,000℃가 되어야 용융점이 되는 초고온용 무기물질들로 조성이 되어져 있기 때문에 불로 인하여 연소 및 배연가스로부터 질식사 혹은 가스유해성으로부터 보호를 받을 수 있는 발명품이다.However, the inorganic adhesive of the present invention is originally a nonflammable inorganic compound material, and since a material composed of 100% inorganic material is composed of inorganic materials for ultrahigh temperature which becomes a melting point at a temperature of 3,000 DEG C, It is an invention that can be protected from harmfulness.

더욱이 다공성을 조성된 패널은 방음성과 호흡성은 그 어느 건축자재 보다 우수하고, 내수명성은 반영구적이며 친환경성이라 제2차의 환경오염을 주지를 않는 멀티 기능성 친환경성 멀티접착제이며 더욱이 다 쓰고 남은 폐자재를 잘게 분쇄시켜 논이나 혹은 밭에 뿌려주면 훌륭한 규산질 비료가 되는 친환경 접착제를 제공하는 것을 목적으로 한다.Furthermore, the porous panel is superior in soundproofness and breathability to any construction material, and its water resistance is semi-permanent and eco-friendly. It is a multifunctional eco-friendly multi-adhesive that does not give a second environmental pollution. Which is excellent in siliceous fertilizer when it is finely pulverized and sprinkled on rice field or field.

본 발명은 멀티 접착제의 성능을 가질 수 있도록 하기 위해서 다음과 같은 방식으로 샘플을 진행하였다.In order to enable the multi-adhesive performance to be achieved, the present invention was carried out in the following manner.

Sodium silicate. Sodium hydroxide, potassium hydroxide 중에서 하나이상을 선택을 하여 5~30중량부를 당량을 하여 증류수에 서서히 첨가하여 투명한 용질액을 수득을 하고,Sodium silicate. Sodium hydroxide and potassium hydroxide are selected and added in an amount of 5 to 30 parts by weight to distilled water to obtain a transparent solute liquid,

이를 다시 Silicon dioxide(SiO2) 입자크기 325메쉬 7~40중량부를 뜨거운 상태70℃~90℃온도에서 규사 졸을 수득을 하는 단계와,(7) to 40 parts by weight of a silicon dioxide (SiO2) particle size of 325 mesh to obtain a silica sol at a hot state at a temperature of 70 DEG C to 90 DEG C,

이를 다시 Barium sulfate, barium chloride, lithium sulfate, lithium chloride, zinc sulfate, zinc chloride, zinc acetate, nickel chloride, copper chloride, magnesium chloride 중에서 한가지 이상을 선별을 하여 2~20중량부를 서서히 첨가를 시켜주는 제조의 단계로서 이때에 한번에 몽땅 투입을 할 시에는 응집이 될 우려가 생김으로 서서히 넣는 것을 유의를 하여야 하며,It is also possible to add 2 to 20 parts by weight of barium sulfate, barium chloride, lithium sulfate, lithium chloride, zinc sulfate, zinc chloride, zinc acetate, nickel chloride, As a step, when putting all at once, there is a possibility of coagulation, so be careful to put it slowly,

Aluminum hydroxide, bentonite, mica, talc, diatomaceous earth, kaolin중에서 하나 이상을 선정을 하여 3~20중량부를 서서히 첨가를 하여 멀티기능 성 접착제를 완료를 해주는 제조의 공정이다.Aluminum hydroxide, bentonite, mica, talc, diatomaceous earth and kaolin are selected and 3 ~ 20 parts by weight are gradually added to complete the multifunctional adhesive.

본 발명은 우리가 거주를 하는 주택은 물론이거니와 산업용으로도 널리 이용을 할 수 있는 멀티 접착체로서 건축내장재인 경량성 텍스용 패널, 불연성 , 방음성, 보온성 성능을 갖는 보드 및 판넬들을 만들 수 있는 멀티 내기능성 접착제의 제조에 관한 것이다.The present invention relates to a lightweight text panel which is a multi-adhesive material which can be widely used not only for a residential house but also for an industrial use, To the production of functional adhesives.

방바닥에 붙이는 온돌마루장판을 붙이는 접착제로서의 활용은 우리 몸에 여러 가지의 효능과 효과를 줄 수 있다.Applying as an adhesive that attaches floor coverings to the floor can give various effects and effects to our body.

방바닥의 붙임강도는 유기 바인더보다도 강도가 더욱더 탁월하고 불에도 연소의 염려가 없기 때문에 그 효율성은 매우 높게 평가될 수 있다.The adhesive strength of the floor is more excellent than the organic binder and the efficiency is very high because there is no fear of burning in the fire.

더욱이 우리가 매일 오랜 시간을 머므르고있는 집에서의 친환경성을 요구하고 있지만 현실은 그렇지 못할때가 많이 있을 수 밖에는 없다.Moreover, while we demand eco-friendliness at home where we stay for a long time each day, there are times when the reality is not so.

건축자재에서의 발암성 물질의 방출, 포름알데히드의 방출, 수십년이 지나도 방출되는 라돈 가스등 이러한 문제점들을 해결안을 주는 본 친환경성 접착제의 만남으로 건강의 효과를 동시에 발현을 하는 우리 몸에 유익함을 주는 것이다.It is beneficial for our body to simultaneously manifest the effect of health by the meeting of this environment-friendly adhesive which solves these problems such as release of carcinogenic substance in building materials, release of formaldehyde, radon gas released after decades. .

도 1 은 본 발명의 바람직한 실시예를 나타낸 비누의 표면도
도 2 는 본 발명의 바람직한 실시예를 나타낸 비누의 내면도
도 3 은 본 발명의 벨트에 대한 주요 성분의 내면도
BRIEF DESCRIPTION OF THE DRAWINGS Figure 1 is a side view of a soap showing a preferred embodiment of the present invention.
2 is a side view of a soap showing a preferred embodiment of the present invention
Figure 3 is an internal view of the major components of the belt of the present invention

이하에서 본 발명의 바람직한 실시예를 첨부시킨 도면에 따라서 보다 상세하게 설명하기로 한다. 본 발명은 Sodium silicate. Sodium hydroxide, potassium hydroxide 중에서 하나이상을 선택을 하여 5~30중량부를 증류수의 물에 포화 용질액을 만들어 주는 공정과 이를 다시 열을 100℃이내의 온도로 가열해주는 단계에서 미리 선별된 Silicon dioxide (SiO2), Borax, boric acid중의 한가지를 선택을 하여 2~20 중량부를 넣은 후 투명한 고농축 용질액으로 만들어 주는 공정으로서 이때에 과 농축액으로 만들어 주는 제조의 공정이며,Hereinafter, preferred embodiments of the present invention will be described in more detail with reference to the accompanying drawings. The present invention relates to a sodium silicate. Sodium hydroxide and potassium hydroxide, and 5 to 30 parts by weight of water are added to the distilled water to prepare a saturating solution. After heating the mixture to a temperature of 100 ° C or less, ), Borax, and boric acid, and adding 2 to 20 parts by weight of the solution to make a transparent concentrated enantiomer. In this case,

상기에서 얻어진 물질에 이를 Barium sulfate, barium chloride, lithium sulfate, lithium chloride, zinc sulfate, zinc chloride, zinc acetate, nickel chloride, copper chloride, magnesium chloride 중에서 한가지 이상을 선별을 하여 3~20중량부를 서서히 첨가를 시켜주는 제조의 단계로서 이때에 한번에 몽땅 투입을 할 시에는 응집이 될 우려가 생김으로 서서히 첨가를 시키면서 분산이 원활하게 될 수 있도록 하는 것이 무었보다도 중요하기 때문에 교반의 속도는 RPM500 이상으로 교반을 해주는 것이 매우 바람직하고 교반기의 내부에는 입자들을 해쇠를 원활할 수 있는 버블판을 샤우드 옆에 3개 이상 특별히 제작된 교반기가 제일 적합한 것으로 파악 되었으며 소량생산부터 대량생산에 이르기까지 매우 적합하였다.At least one of Barium sulfate, barium chloride, lithium sulfate, zinc sulfate, zinc chloride, zinc acetate, nickel chloride, copper chloride and magnesium chloride is selected and added slowly to the material obtained above. In this case, it is important to add slowly to the dispersion while gradually adding the mixture at a time so that there is a fear of aggregation. In this case, the mixing speed is preferably higher than RPM 500 It is very desirable that three or more specially designed stirrers are most suitable for the agitator with a bubble plate that can smooth the particles in the inside of the agitator and it is very suitable from small volume production to mass production.

Aluminum hydroxide, bentonite, mica, talc, diatomaceous earth, kaolin중에서 하나 이상을 선정을 하여 3~20중량부에서 이들은 무기 접착제에서 접착력을 높이어 주는 것은 물론 이거니와 미네날에서의 가지고있는 매우 유익한 내기능성을 주는 절대적인 필러로서 무기 접착제가 갖는 특성을 가질 수 있도록하는 절대적인 필러가 되기도 하는 물질이다.Aluminum hydroxide, bentonite, mica, talc, diatomaceous earth and kaolin are selected and added at 3 ~ 20 parts by weight. In addition to these, they improve adhesion in inorganic adhesives. In addition, they have an excellent filler Which is an absolute filler that allows the inorganic adhesive to have the properties of an inorganic adhesive.

본 발명은 100% 천연 미네날 성분들만을 가지고 조성을 한 멀티타입의 천연 접착제로서 이를 이용하여 접목을 할 수 있는 적용처는 방바닥, 거실용, 강당바닥, 마루 접착제로서 매우 적합하며, 스티로폼 접착제로서 적용을 하여 샌드위치 판넬 접착제, 천연 현지토 (황토, 마사토, 찰흙, 각종 흙) 접착제. 퍼라이트(경량, 초경량 비드) 패널용 접착제. 질석 패널 접착제, 유기(폴리화이버, 셀룰로우스, 왕겨, 톱밥) 화이버용 접착제 등..The present invention is a multi-type natural adhesive having only 100% natural minerals, and is suitable for flooring, living room, auditorium floor, flooring adhesive, and is applied as a styrofoam adhesive Sandwich panel adhesives, natural local soil (loess, marathon, clay, various soil) adhesives. Glue for perlite (lightweight, lightweight bead) panel. Vermiculite panel adhesives, adhesives for organic (polyfibers, cellulose, chaff, sawdust) fibers, etc.

다양한 용도와 효과를 제공하는 매우 유용한 발명품을 제공하는 것이다.It is an object of the present invention to provide a very useful invention which provides various uses and effects.

10 : 접착제의 공정10: Process of adhesive

Claims (7)

Sodium silicate. Sodium hydroxide, potassium hydroxide 중에서 하나이상을 선택을 하여 2~20중량부와,
Silicon dioxide(SiO2), Borax, boric acid 중에서 하나를 선정을 하여 3~20중량부와, Barium sulfate, barium chloride, lithium sulfate, lithium chloride, zinc sulfate, zinc chloride, zinc acetate, nickel chloride, copper chloride, magnesium chloride 중에서 한가지 이상을 선별을 하여 2~20중량부를 서서히 첨가를 시켜주는 제조의 단계로서 이때에 한번에 몽땅 투입을 할 시에는 응집이 될 우려가 생김으로 서서히 넣는 것을 유의를 하여야 하며,
Aluminum hydroxide, bentonite, mica, talc, diatomaceous earth, kaolin중에서 하나 이상을 선정을 하여 3~20중량부.
Sodium silicate. Sodium hydroxide, and potassium hydroxide, and 2 to 20 parts by weight,
Barium sulfate, barium chloride, lithium sulfate, lithium chloride, zinc sulfate, zinc chloride, zinc acetate, nickel chloride, copper chloride, magnesium chloride, and gradually adding 2 to 20 parts by weight of the magnesium chloride. When the magnesium chloride is added at one time, there is a fear of agglomeration. Therefore,
Aluminum hydroxide, bentonite, mica, talc, diatomaceous earth, kaolin and 3 ~ 20 parts by weight.
제1항에 있어서 Sodium silicate. Sodium hydroxide, potassium hydroxide 중에서 하나이상을 선택을 하여 2~20중량부와 증류수 100중량부에 서서히 첨가하여 투명한 용질액을 수득을 하는 것을 특징으로하는 무기질 접착제 제조의 방법과,2. The method of claim 1, wherein the sodium silicate. Sodium hydroxide, and potassium hydroxide, and gradually adding to 2 to 20 parts by weight of distilled water and 100 parts by weight of distilled water to obtain a transparent solute liquid. 이를 다시 상기 제2항에 있어서 Silicon dioxide(SiO2), Borax, boric acid 중에서 하나를 선정하여 2~ 20중량부를 용질액의 온도를 70℃~90℃온도로 데워주는 것을 특징으로 하는 무기질 접착제 제조의 방법과,2 to 20 parts by weight of one of Silicon dioxide (SiO 2), Borax and Boric acid is heated to a temperature of 70 ° C. to 90 ° C. according to the second aspect of the present invention. Method, 제3항에 있어서 입자크기 325메쉬 7~40중량부를 뜨거운 상태70℃~90℃온도에서 규사 졸을 수득을 하는 것을 특징으로 하는 무기질 접착제 제조의 방법과,A process for producing inorganic adhesives according to claim 3, wherein 7 to 40 parts by weight of a particle size of 325 mesh is obtained in a hot state at a temperature of 70 to 90 DEG C, 상기 제1항에 있어서 Barium sulfate, barium chloride, lithium sulfate, lithium chloride, zinc sulfate, zinc chloride, zinc acetate, nickel chloride, copper chloride, magnesium chloride 중에서 한가지 이상을 선별을 하여 2~20중량부를 제4항에서 수득된 물질에 서서히 첨가를 시켜서 500RPM의 속도에서 교반을 시켜주는 것을 특징으로 하는 무기질 접착제 제조의 방법과,Wherein at least one of barium sulfate, barium chloride, lithium sulfate, zinc sulfate, zinc chloride, zinc acetate, nickel chloride, copper chloride and magnesium chloride is selected from 2 to 20 parts by weight, And then agitating the mixture at a speed of 500 RPM. The method of producing an inorganic adhesive according to claim 1, 상기 제1항에 있어서 Aluminum hydroxide, bentonite, mica, talc, diatomaceous earth, kaolin중에서 하나이상을 선정을 하여 3~20중량부를 서서히 첨가를 하여 멀티기능 성 접착제를 완료를 하는 것을 특징으로 하는 무기질 접착제 제조의 방법과,3. The method for producing an inorganic adhesive according to claim 1, wherein at least one of aluminum hydroxide, bentonite, mica, talc, diatomaceous earth and kaolin is selected and 3 to 20 parts by weight are gradually added to complete the multifunctional adhesive And 상기 제7항에 있어서 얻어진 물질을 바닥 접착제 및 각종 유 무기 접착제로서 적용이 되는 것을 특징으로 하는 무기질 접착제 제조의 방법이다.Characterized in that the material obtained in the step (7) is applied as a floor adhesive and various organic / inorganic adhesives.
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CN110183904A (en) * 2019-06-13 2019-08-30 广东顺德洋紫薇化工有限公司 Fire-retardant ink and preparation method thereof and inflaming retarding membrane
KR102045518B1 (en) * 2018-11-22 2019-11-15 (주)삼현 Eco-friendly liquide flame retardant composition
KR102045517B1 (en) * 2018-11-22 2019-11-15 (주)삼현 Eco-friendly powder flame retardant composition and manufacturing method thereof
CN112759955A (en) * 2020-12-29 2021-05-07 广西经正涂料有限公司 Water-based inorganic primer for interior walls and preparation method thereof
KR102455700B1 (en) * 2022-07-25 2022-10-18 최영학 admixture for formed concrete, manufacturing method therefor and formed concrete for cast-in-site thereby
KR102473301B1 (en) * 2022-09-07 2022-12-02 최영학 manufacturing method for formed concrete for cast-in-site with enhanced sound insulation
WO2023154497A1 (en) * 2022-02-11 2023-08-17 Armstrong World Industries, Inc. Fire resistant adhesive compositions and methods of preparing and using the same

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102045518B1 (en) * 2018-11-22 2019-11-15 (주)삼현 Eco-friendly liquide flame retardant composition
KR102045517B1 (en) * 2018-11-22 2019-11-15 (주)삼현 Eco-friendly powder flame retardant composition and manufacturing method thereof
CN110183904A (en) * 2019-06-13 2019-08-30 广东顺德洋紫薇化工有限公司 Fire-retardant ink and preparation method thereof and inflaming retarding membrane
CN112759955A (en) * 2020-12-29 2021-05-07 广西经正涂料有限公司 Water-based inorganic primer for interior walls and preparation method thereof
CN112759955B (en) * 2020-12-29 2022-02-11 广西经正涂料有限公司 Water-based inorganic primer for interior walls and preparation method thereof
WO2023154497A1 (en) * 2022-02-11 2023-08-17 Armstrong World Industries, Inc. Fire resistant adhesive compositions and methods of preparing and using the same
KR102455700B1 (en) * 2022-07-25 2022-10-18 최영학 admixture for formed concrete, manufacturing method therefor and formed concrete for cast-in-site thereby
KR102473301B1 (en) * 2022-09-07 2022-12-02 최영학 manufacturing method for formed concrete for cast-in-site with enhanced sound insulation

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