KR20180018634A - The insecticidal composition for controlling borer consisting of mustard oil as an efficient component - Google Patents
The insecticidal composition for controlling borer consisting of mustard oil as an efficient component Download PDFInfo
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- 239000000203 mixture Substances 0.000 title claims abstract description 50
- ZOJBYZNEUISWFT-UHFFFAOYSA-N allyl isothiocyanate Chemical compound C=CCN=C=S ZOJBYZNEUISWFT-UHFFFAOYSA-N 0.000 title claims abstract description 41
- 239000008164 mustard oil Substances 0.000 title claims abstract description 41
- 230000000749 insecticidal effect Effects 0.000 title claims abstract description 29
- 239000010655 horseradish oil Substances 0.000 claims abstract description 7
- 239000003921 oil Substances 0.000 claims abstract description 7
- 239000007788 liquid Substances 0.000 claims abstract description 5
- 239000007921 spray Substances 0.000 claims description 8
- 239000000443 aerosol Substances 0.000 claims description 2
- 239000002023 wood Substances 0.000 abstract description 22
- 241000238631 Hexapoda Species 0.000 abstract description 19
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- 235000013399 edible fruits Nutrition 0.000 abstract 1
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- 239000000243 solution Substances 0.000 description 13
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 12
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 12
- 238000005507 spraying Methods 0.000 description 12
- 239000002917 insecticide Substances 0.000 description 11
- 239000004744 fabric Substances 0.000 description 9
- 241000256602 Isoptera Species 0.000 description 8
- 239000004480 active ingredient Substances 0.000 description 8
- 238000000034 method Methods 0.000 description 8
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- 244000195452 Wasabia japonica Species 0.000 description 6
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- 239000008158 vegetable oil Substances 0.000 description 4
- 241000254173 Coleoptera Species 0.000 description 3
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
- 239000003814 drug Substances 0.000 description 3
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- 239000000126 substance Substances 0.000 description 3
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- 235000004977 Brassica sinapistrum Nutrition 0.000 description 2
- 241000243771 Bursaphelenchus xylophilus Species 0.000 description 2
- 206010061217 Infestation Diseases 0.000 description 2
- 239000004698 Polyethylene Substances 0.000 description 2
- -1 alkyl phenols Chemical class 0.000 description 2
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- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 2
- 241000894007 species Species 0.000 description 2
- 235000021419 vinegar Nutrition 0.000 description 2
- 239000000052 vinegar Substances 0.000 description 2
- 241001124076 Aphididae Species 0.000 description 1
- 241000256844 Apis mellifera Species 0.000 description 1
- 206010008631 Cholera Diseases 0.000 description 1
- 240000007049 Juglans regia Species 0.000 description 1
- 235000009496 Juglans regia Nutrition 0.000 description 1
- 241000219098 Parthenocissus Species 0.000 description 1
- 244000046052 Phaseolus vulgaris Species 0.000 description 1
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 1
- 235000014676 Phragmites communis Nutrition 0.000 description 1
- 235000008585 Pinus thunbergii Nutrition 0.000 description 1
- 241000218686 Pinus thunbergii Species 0.000 description 1
- 208000037386 Typhoid Diseases 0.000 description 1
- 244000126002 Ziziphus vulgaris Species 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000000845 anti-microbial effect Effects 0.000 description 1
- 239000004566 building material Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000010632 citronella oil Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 239000013039 cover film Substances 0.000 description 1
- 239000001941 cymbopogon citratus dc and cymbopogon flexuosus oil Substances 0.000 description 1
- 230000002542 deteriorative effect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000013399 early diagnosis Methods 0.000 description 1
- 239000002316 fumigant Substances 0.000 description 1
- 238000003958 fumigation Methods 0.000 description 1
- 229940106580 ginkgo biloba leaf extract Drugs 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 238000003306 harvesting Methods 0.000 description 1
- 230000002363 herbicidal effect Effects 0.000 description 1
- 208000015181 infectious disease Diseases 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 150000002540 isothiocyanates Chemical class 0.000 description 1
- 230000002147 killing effect Effects 0.000 description 1
- 230000001418 larval effect Effects 0.000 description 1
- 231100000518 lethal Toxicity 0.000 description 1
- 230000001665 lethal effect Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 239000008194 pharmaceutical composition Substances 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 238000005067 remediation Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 208000010110 spontaneous platelet aggregation Diseases 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 201000008297 typhoid fever Diseases 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 239000012855 volatile organic compound Substances 0.000 description 1
- 235000020234 walnut Nutrition 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
- 230000002087 whitening effect Effects 0.000 description 1
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Classifications
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
- A01N25/06—Aerosols
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Y10S514/919—
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- Agronomy & Crop Science (AREA)
- Environmental Sciences (AREA)
- Zoology (AREA)
- Wood Science & Technology (AREA)
- Plant Pathology (AREA)
- Toxicology (AREA)
- Pest Control & Pesticides (AREA)
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Biotechnology (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
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Abstract
Description
본 발명은 겨자 오일을 유효성분으로 함유하는 천공충 방제용 살충제 조성물에 관한 것으로 더욱 상세하게는 겨자 오일을 유기용매 또는 끈끈이액에 혼합하여 도포제로 사용하게 하거나 또는 스프레이상으로 제조해 분무제로 사용하여 살충 효과를 평가하고 천공충 방제용 살충제를 제공한다.The present invention relates to a pesticidal composition for controlling pest infestation containing mustard oil as an active ingredient, and more particularly, to a pesticidal composition for pest control which contains mustard oil as an active ingredient, and more particularly, The insecticidal effect is evaluated and an insecticide for pest control is provided.
전 국토의 60 % 이상이 산림으로 이루어진 우리나라는 기록된 해충의 종류가 2,600여종으로 알려져 있다(최광식, 특용수 해충도감, 국립산림과학원 연구신서 제 24호, 2007). 특히 농민들의 소득을 높이기 위하여 재배되고 있는 유실수인 호두, 대추 등과 삶의 질이 향상되어 조경수나 정원수 및 분재수에 대한 관심이 높아지고 있지만 해충들에 의해 이러한 수목들이 피해를 받고 있는 실정이다. 수목을 가해하는 해충은 주로 잎을 흡즙(吸汁)하는 흡즙성(吸汁性) 해충인 진딧물류 및 방패벌레와 잎을 식해(食害)하는 식엽성(食葉性) 해충인 나비목 해충류 등이 있으며 이들 해충은 약제를 살포하는 방법만으로도 쉽게 방제가 되는 편이다. 그러나 나무의 목질부 내에서 가해하는 천공성 해충류인 하늘소류와 나무 좀류 및 박쥐나방류 등은 약제를 살포하는 것으로는 방제가 불가능하다. 또한 목재 건축자재 및 목재가구 등 목재가공품을 가해하는 가루나무 좀류와 나무 좀류 및 흰개미 등에 의한 피해도 날로 증가하는 추세이다. 특히 최근 문제가 되고 있는 소나무 재선충병은 소나무 재선충이 매개충에 의해 전파되어 소나무 내에 침입 후 증식함으로 소나무를 고사시키는 병으로 한번 감염되면 치료가 불가능한 병으로 알려져 있다. In Korea, where more than 60% of the whole country is made up of forests, some 2,600 species of pests have been recorded (Choi Kwang-sik, Illustrated Pesticide Species, National Forestry Research Institute, Korea Newspaper No. 24, 2007). Especially, walnut and jujube, which are cultivated to increase the income of farmers, have improved their quality of life, and interest in landscape gardening, gardening, and bonsai has increased, but these trees are being damaged by pests. Insect pests that are planted mainly include aphids, which are sucky pests that harvest leaves, and lepidopteran insects, which are shielded insects and leafy pests that eat leaves. Insect pests are easily controlled by spraying drugs. However, it is impossible to control the pest infestation in the woody part of the tree by spraying medicines. In addition, damage caused by wood dusts, woodchips, termites, and other wood products, such as wood building materials and wooden furniture, is also increasing. Especially, the pine reeves disease which is a recent problem is known as a disease that can not be treated once infected with a pine tree which is propagated by a pine tree and propagated after penetrating into a pine tree.
소나무 재선충 병의 방제는 주로 화학농약에 의한 매개충 구제와 약제나무주사에 의한 예방이 주 방제방법이며 매개충 구제 방법으로는 죽은 나무를 벌채하여 쌓은 다음 훈증 약제를 주입하고 피복필름을 씌워 가스에 의한 살충작용을 하는 방법이 주된 방제법으로 사용되고 있지만 작업의 부주의로 인해 매개충이 생존할 가능성이 있다. 이와 같이 매개충이 생존하여 소나무 재선충을 확산시킬 것을 우려해 화학살충제를 이용한 항공약제살포를 병행하고 있으며 그 방법으로 벌근부(그루터기)에 서식하는 하늘소 방제의 경우 훈증 약제를 처리하고 피복제를 덮어 훈증 방제하거나 병의 진전이 수간의 아랫부분부터 진전됨으로 그루터기를 낮추어 베는 방법을 사용하고 있다(Tan et al., A Study on disease development and early diagnosis of pine wood nematode, Bursaphelenchus xylophilus, infection of japanese black pine, Nematology 7: 481-485, 2005). 그러나 이와 같은 방법은 산림의 입지 여건상 방제에 어려움이 많아 방제의 실효성이 떨어지고 있으므로 보다 실효성이 높은 방제방법의 제시가 필요하다.The control of pine creeper disease is mainly controlled by chemical pesticide remedy and prevention by injection of medicinal wood. In the method of remediation of the pesticide tree, dead wood is piled up, and then fumigation medicine is injected and cover film is covered, Although the method of acting is the main control method, there is a possibility that the insect can survive due to the carelessness of the operation. In order to prevent the spread of the pine tree reed dander, the insecticide is sprayed with a chemical insecticide. In this case, in case of the pest control inhabiting the bee root (stump), the fumigant is treated, Or the progression of the disease has progressed from the bottom to the lower part of the stomach (Tan et al., A study on development and early diagnosis of pine wood nematode, Bursaphelenchus xylophilus, infection of japanese black pine, Nematology 7: 481-485, 2005). However, since this method is difficult to control due to the location of the forest, it is necessary to propose a more effective control method because the effectiveness of the control is deteriorating.
천연 식물성 정유인 이소치오시아네이트(Isothiocyanate)는 고추냉이의 주된 성분으로 추출된 정유 중에 약 80%를 차지하며 항균작용에 주성분으로 작용해 콜레라균 및 장티푸스균과 같은 식중독 세균 등에 대하여 항균활성을 나타내는 것으로 알려져 있다(Kumagai H, Analysis of volatile components in essential oil of upland wasabi and their inhibitory effects on platelet aggregation, Biosci. Biotech. Biochem 58:2131-2135, 1994). Isothiocyanate, a natural vegetable essential oil, accounts for about 80% of the essential oil extracted as a main component of wasabi, and acts as a main component for the antimicrobial action. It exhibits antibacterial activity against foodborne bacteria such as cholera and typhoid bacteria (Kumagai H, Analysis of volatile components in essential oil of upland wasabi and their inhibitory effects on platelet aggregation, Biosci. Biotech. Biochem 58: 2131-2135, 1994).
본 발명의 선행기술로 참나무 목초액의 추출물 또는 분획물을 유효성분으로 함유하는 문화재 보존용 방충 또는 살충용 조성물이 제10-1270630호에 개시된 바 있으나 이는 주로 참나무 목초액의 메틸렌 클로라이드 분획물을 유효성분으로 함유하는 권연벌래의 방충 또는 살충용 약학적 조성물을 제공하여 문화재를 보존하는 방법에 관한 것이다. 또 식물성 천연물질을 이용한 선택적 흰개미 기피제 조성물이 대한민국 등록특허 제10-1261359호에 개시된 바 있으나 이는 식물성 천연물질인 시트로넬라 오일, 레몬그래스 오일 및 은행나무잎 추출물을 이용하여 환경오염 등의 부작용이 없는 흰개미 기피제 조성물의 제공에 관한 것이다. 포충용 끈끈이액 및 제조방법이 대한민국 등록특허 제10-1179251호에 개시되어 있으나 이는 간단한 방법으로 단시간에 제조가 가능한 친환경적인 포충용 끈끈이액 및 그 제조방법에 관한 것이다. 한편 유채의 추출물을 유효성분으로 하는 식물 유해곤충 방제용 조성물이 대한민국 등록특허 제10-1061038호에 개시되어 있으나 이는 기능성 천연 살충제로 유채의 추출물 또는 농축액 및 이들의 혼합물을 유효성분으로 함유하는 식물 유해곤충 방제용 조성물에 관한 것이다. As a prior art of the present invention, an insecticidal or insecticidal composition for preserving a cultural heritage containing an extract or fraction of oak wood vinegar as an active ingredient is disclosed in Japanese Patent Application No. 10-1270630. However, this is because the methylene chloride fraction of oak wood vinegar The present invention relates to a method for preserving cultural properties by providing a pharmaceutical composition for pest insect or insect pest. In addition, a selective termite detergent composition using a plant natural substance is disclosed in Korean Patent No. 10-1261359. However, the use of citronella oil, lemongrass oil, and Ginkgo biloba leaf extract, which are natural plant substances, Lt; RTI ID = 0.0 > termites < / RTI > The present invention relates to an environmentally friendly encapsulating sticky liquor capable of being produced in a short time by a simple method and a method for producing the same. Meanwhile, Korean Patent No. 10-1061038 discloses a plant harmful insect control composition containing an extract of rape seed as an active ingredient, but this is a functional natural insecticide, which is a plant harmful agent containing an extract or concentrate of rapeseed and a mixture thereof as an active ingredient To an insect control composition.
따라서, 상기 특허문헌 어디에도 겨자 오일을 유효성분으로 함유하는 살충제를 제조하여 살충효과를 평가한 천공충 방제용 살충제는 개시되거나 검증된 바 없다.Therefore, no pesticide for pest control has been disclosed or proved in any of the above-mentioned Patent Documents, in which an insecticide containing mustard oil as an active ingredient is prepared to evaluate the insecticidal effect.
따라서, 본 발명의 목적은 겨자 오일을 함유하는 천공충 방제용 살충제 조성물을 제공하는 데 있다.Accordingly, it is an object of the present invention to provide a pesticide composition for pest control containing mustard oil.
본 발명의 다른 목적은 상기 단계에서 얻은 천공충 방제용 조성물을 함유하는 끈끈이액 및 스프레이를 제공하는 데 있다.Another object of the present invention is to provide a detergent liquid and a spray which contain the composition for controlling penetration resistance obtained in the above step.
본 발명의 상기 목적은 겨자 오일을 메탄올과 혼용하여 천공구에 주입하여 결과를 관찰하는 단계와; 상기 단계의 오일과 끈끈이액을 혼합한 조성물을 솔수염 하늘소 침입구에 주입하여 유충의 치사 유무를 조사하는 단계와; 상기 단계의 조성물과 겨자 오일을 에탄올과 혼합한 조성물을 솔수염 하늘소 침입구에 주입하여 유충의 치사 유무를 조사하는 단계와; 상기 단계의 겨자 오일과 끈끈이액을 혼합한 조성물을 스프레이상으로 충진한 후 솔수염 하늘소 천공구에 분사처리하여 살충효과를 조사하는 단계와; 상기 단계의 스프레이상을 솔수염 하늘소가 서식하는 목재표면과 흰개미가 서식하는 목재 표면에 분사하여 살충효과를 조사하는 단계와; 상기 단계의 스프레이 상을 부직포에 분사한 후 침입공 부위에 부착시켜 하늘소 애벌레의 치사 유무를 조사하는 단계를 통하여 달성하였다.The above object of the present invention is achieved by a method for producing a vegetable oil, comprising the steps of: mixing mustard oil with methanol; Injecting a composition obtained by mixing the oil of the step and the glue solution into a brine entrance to investigate whether or not the larvae are killed; Injecting a composition obtained by mixing the composition of the above step and mustard oil with ethanol into a brine entrance to investigate whether or not the larvae are killed; Spraying a composition comprising the mixture of mustard oil and a sticky solution in the above step in a spray form, spraying the composition on a brush bristle tool to examine the insecticidal effect; Spraying the spray of the above step onto a surface of wood on which the dwarf beetle spikelet is inhabited and a wood surface of a termite; Spraying the spray of the above step onto the nonwoven fabric and attaching it to the intrusion hole to investigate whether or not the caterpillars were dead.
본 발명은 겨자오일을 유효성분으로 함유하는 천공충 방제용 조성물을 이용하여 산림 해충 뿐만 아니라 과수 해충 및 목재가공품 해충 등 광범위하게 방제할 수 있는 뛰어난 효과가 있다.The present invention has an excellent effect that can be widely controlled not only for forest pests but also for insect pests and wood-processed insects by using a pest control composition containing mustard oil as an active ingredient.
도 1은 본 발명에 따른 겨자 오일 함유 점착성 스프레이상 사진도이다.
도 2는 본 발명 조성물을 천공구에 주입 처리하는 사진도이다.
도 3는 본 발명 겨자 오일 처리에 의해 치사된 하늘소 사진도이다.
도 4은 본 발명 겨자 오일 처리에 의해 치사된 흰개미 사진도이다.BRIEF DESCRIPTION OF THE DRAWINGS Figure 1 is a photograph of a mustard oil containing viscous spray according to the present invention.
Fig. 2 is a photograph showing the composition of the present invention injected into a cloth tool; Fig.
Fig. 3 is a photograph of a bean sprout killed by the present invention mustard oil treatment.
Fig. 4 is a photograph of termites killed by the present invention mustard oil treatment.
본 발명은 천공충의 서식생태특성을 고려하여 천공충이 목재 내에 서식하는 단계에서 휘발성이 있는 천연물질인 겨자 오일을 주입하여 목재 내에 있는 벌레를 퇴치하는 방법이다. 유실수, 조경수, 분재 및 목재 내 천공충의 천공구가 열려있는 경우에는 조성물을 분무 처리하여 살충하는 방법이 바람직하고 천공구가 폐쇄된 경우 스프레이 분사구를 천공구에 주입하여 조성물이 천공구 내 깊이 주입되도록 하는 것이 바람직하다. 또한 목재가공품의 경우 조성물을 처리하고 필름을 부착하여 살충물질이 천공구내에 충분히 침투되도록 하는 것이 바람직하다. Considering the habitat characteristics of perforated pods, the present invention is a method for podding insects in wood by injecting mustard oil, which is a volatile natural substance, at the stage where perforated pods are inhabited in the wood. In the case of open water mills, landscape waters, bonsai trees and perforated liners in wood, it is preferable to spray the composition by spraying, and when the cloth tool is closed, the spray nozzle is injected into the cloth tool so that the composition is injected deep into the cloth tool . It is also desirable to treat the composition and to affix the film so that the insecticidal material is sufficiently penetrated into the perforations in the case of wood-processed products.
이하, 본 발명의 구체적인 내용을 실시예를 들어 상세하게 설명한다. 하기 실시예는 본 발명을 예시하기 위한 것일 뿐 발명이 하기 실시예에 한정되는 것은 아니다.
Hereinafter, the present invention will be described in detail with reference to examples. The following examples are for illustrative purposes only and are not intended to limit the invention.
실시예Example 1 : 천연식물오일의 벌레 방제 효과 1: Effect of insect control of natural plant oil
본 발명은 인체에 무해한 휘발성 유기화물, 유기주석화합물 및 알킬페놀류 등이 검출되지 않는 끈끈이액과 같은 담체에 (주)BIG로부터 분양받은 천연 식물성 오일인 겨자오일 또는 고추냉이 오일을 사용하여 혼합한 조성물을 벌레가 서식하는 천공구에 주입하거나 천공구 표면에 분무 처리하여 천공충의 퇴치 효과를 조사한 결과 극대화 할 수 있음을 확인하였다.The present invention relates to a composition obtained by mixing a natural vegetable oil, such as mustard oil or horseradish oil, obtained from BIG Co., Ltd., on a carrier such as a sticky liquid in which no harmful volatile organic compounds, organotin compounds and alkyl phenols are detected Was injected into a cloth tool inhabited by insects or sprayed on the surface of a cloth tool to investigate the effect of the puncture pest.
본 발명에 따르면, 상기 천연 식물성 오일인 겨자오일, 고추냉이오일 외에도 다수의 균등물이 사용될 수 있다.
According to the present invention, in addition to the natural vegetable oils such as mustard oil and horseradish oil, many equivalents can be used.
실험예Experimental Example 1 : 천연식물오일의 1: of natural plant oils 천공충에In puncture 대한 살충효과 조사 Investigation of insecticidal effect
본 발명에 따른 겨자오일과 고추냉이오일을 메탄올에 각 5 중량%, 10 중량% 및 20 중량%으로 혼합하여 천공구 당 0.3-0.5 mL 수준으로 주입하고 24시간 경과 후 관찰한 결과 표 1과 같이 100 % 벌레 퇴치(살충)효과를 보였다.The mixture of mustard oil and horseradish oil according to the present invention was mixed with methanol at 5 wt%, 10 wt% and 20 wt%, respectively, at a level of 0.3-0.5 mL per a cloth tool and observed after 24 hours, 100% insecticidal effect (insect) showed.
실험예Experimental Example 2 : 천연식물 오일과 2: Natural vegetable oils and 끈끈이액Sticky solution 혼합 조성물 처리량에 따른 살충효과 조사 Investigation of insecticidal effect according to the amount of mixed composition
본 발명의 겨자오일과 고추냉이 오일을 끈끈이액에 각 5 중량%, 10 중량% 및 20 중량%로 혼합한 조성물을 솔수염 하늘소 침입구에 0.3-0.5 mL 수준으로 주입하여 24시간 경과 후 솔수염 하늘소 유충의 치사유무를 조사한 결과 5 중량% 이상 처리 시 100 %의 벌레퇴치(살충) 효과를 나타냈다(표 2). The composition prepared by mixing the mustard oil and the wasabi oil of the present invention in a sticky liquid at 5 wt%, 10 wt% and 20 wt%, respectively, was injected at 0.3-0.5 mL level into the bristle whitening entry port. After 24 hours, As a result of examining the presence or absence of lethal killings, 100% insecticidal effect (insecticidal effect) was shown when treated at 5 wt% or more (Table 2).
실험예Experimental Example 3 : 겨자오일의 3: of mustard oil 끈끈이액Sticky solution 혼합 조성물에 따른 살충효과 조사 Investigation of insecticidal effect according to mixed composition
한편, 본 발명의 겨자오일을 끈끈이액에 각 5 중량%, 10 중량% 및 20 중량%로 혼합한 조성물과 에탄올에 5 중량%, 10 중량% 및 20 중량%로 혼합한 조성물을 솔수염 하늘소 침입구에 0.1-0.4 mL 수준으로 주입하여 24시간 경과 후 솔수염 하늘소 유충의 치사유무를 조사한 결과 겨자오일과 끈끈이액 혼합 조성물이 에탄올 혼용 처리에 비하여 살충효과가 매우 높게 나타났다(표 3). On the other hand, a composition prepared by mixing the mustard oil of the present invention in an amount of 5 wt%, 10 wt% and 20 wt% in a sticky solution and 5 wt%, 10 wt% and 20 wt% in ethanol, (0.1-0.4 mL). After 24 hours, it was found that the mixture of mustard oil and sticky liquor had a higher insecticidal effect than that of mixed ethanol (Table 3).
실험예Experimental Example 4 : 겨자오일의 4: Of mustard oil 끈끈이액Sticky solution 혼합 조성물에 따른 살충효과 조사 Investigation of insecticidal effect according to mixed composition
본 발명 겨자오일과 끈끈이액 혼합 조성물을 각 5 중량%, 10 중량% 및 20 중량%로 에어로졸 타입으로 충진하고(도 1) 솔수염 하늘소 천공구에 0.5 mL 수준으로 분사 처리한 후(도 2) 상온에서 24시간 및 48시간 경과 후 살충효과를 조사한 결과 5 중량% 이상의 조성물을 처리할 시 살충효과는 100 %로 나타났다(표 4).The mixture of mustard oil and sticky solution according to the present invention was filled into aerosol type at 5 wt%, 10 wt% and 20 wt%, respectively (Fig. 1) The insecticidal effect after 24 hours and 48 hours at room temperature was investigated. As a result, the insecticidal effect was 100% when 5 wt% or more of the composition was treated (Table 4).
실시예Example 2 : 겨자오일의 2: of mustard oil 끈끈이액Sticky solution 혼합 조성물의 목재표면 처리 효과 Wood surface treatment effect of mixed composition
본 발명은 끈끈이액에 겨자오일을 일정비율로 혼합하여 목재 천공충이 서식하고 있는 목재의 표면에 분무 처리하여 천공충의 퇴치 효과를 조사하였다.
In the present invention, an effect of spraying a mustard oil on a sticky liquor at a predetermined ratio and spraying the surface of the wood which is inhabited by the wood perforation was examined.
실험예Experimental Example 5 : 겨자 오일의 목재 표면 분무처리 효과 5: Wood surface spraying effect of mustard oil
본 발명의 겨자 오일을 메탄올에 각 5 중량%, 10 중량% 및 20 중량%로 혼합하여 솔수염 하늘소가 침입하여 서식하고 있는 목재 표면과 흰개미가 서식하고 있는 목재표면에 가장 바람직하게는 0.5 mL/10 ㎠ 분무처리하고 공기투과도가 낮은 폴리에틸렌(PE) 필름을 표면 피복한 다음 24시간 경과 후에 살충효과를 조사한 결과 솔수염 하늘소와 흰개미 모두 조성물 5 중량%를 0.5 mL 수준으로 처리 시 100 % 살충효과를 나타냈다(표 5-6 및 도 3-4).The mustard oil of the present invention is mixed with methanol in an amount of 5 wt%, 10 wt% and 20 wt%, respectively, so that the wood surface on which the bristle whorl is invading and the wood surface inhabited by the termite is most preferably 0.5 mL / After spraying 10 ㎠ sprayed polyethylene (PE) film with low air permeability, the insecticidal effect was investigated after 24 hours. As a result, it was found that 100% insecticidal effect (Table 5-6 and Fig. 3-4).
실험예Experimental Example 6 : 겨자오일 함유 6: contains mustard oil 끈끈이액의Sticky 표면처리 효과 Surface treatment effect
본 발명의 겨자오일과 끈끈이액 혼합 조성물을 부직포에 흡착(1 mL/5 ㎝x5 ㎝)시키고 솔수염 하늘소 칩입공 부위에 부착하여 씰링한 후 하늘소 애벌레의 치사유무를 조사한 결과 24시간 경과 후 100 %의 살충효과를 보였다(표 7).The mixture of mustard oil and sticky solution of the present invention was adsorbed (1 mL / 5 cm x 5 cm) on the nonwoven fabric and attached to the cheeking area of the cheek beetle and examined for the presence or absence of the caterpillars. After 24 hours, 100% (Table 7).
이상 설명한 바와 같이 본 발명은 겨자오일 및 고추냉이오일 등 천연식물오일을 유효성분으로 함유하는 천공충 방제용 살충제 조성물을 제공하는 효과가 있으며 상기 조성물을 이용하여 산림 해충 뿐만 아니라 과수 해충 및 목재가공품 천공충을 광범위하게 방제할 수 있는 뛰어난 효과가 있으므로 임업 및 목재가공 산업상 매우 유용한 발명인 것이다.As described above, the present invention provides an insecticidal composition for perennial herbicidal use containing, as an active ingredient, natural plant oil such as mustard oil and wasabi oil. The composition can be used not only for forest insect pests but also for perennial pests and wood- It is a very useful invention in the forestry and wood processing industries because it has an excellent effect that can control worms extensively.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| KR960000022B1 (en) * | 1986-09-09 | 1996-01-03 | 노르솔로, 어 리미티드 캄패니 | A process for regenerating catalyst and its application to an oxidative dehydrogenation process |
| KR20020087568A (en) * | 2001-05-14 | 2002-11-23 | 주식회사 내츄로바이오텍 | Plant containing insecticidal activity and insecticidal chemical compound |
| KR20030075481A (en) * | 2002-03-19 | 2003-09-26 | 애경산업(주) | Insecticide composition for an acarus and sprayer |
| KR20120021475A (en) * | 2010-08-02 | 2012-03-09 | 대한민국 (관리부서:국립문화재연구소) | The composition comprising the extraction or fraction of oak vinegar having insect resistance or insecticidal activities for protection of cultural heritage |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| KR960000022B1 (en) * | 1986-09-09 | 1996-01-03 | 노르솔로, 어 리미티드 캄패니 | A process for regenerating catalyst and its application to an oxidative dehydrogenation process |
| KR20020087568A (en) * | 2001-05-14 | 2002-11-23 | 주식회사 내츄로바이오텍 | Plant containing insecticidal activity and insecticidal chemical compound |
| KR20030075481A (en) * | 2002-03-19 | 2003-09-26 | 애경산업(주) | Insecticide composition for an acarus and sprayer |
| KR20120021475A (en) * | 2010-08-02 | 2012-03-09 | 대한민국 (관리부서:국립문화재연구소) | The composition comprising the extraction or fraction of oak vinegar having insect resistance or insecticidal activities for protection of cultural heritage |
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