KR20170087176A - Extraction of curcumin of the components of turmeric - Google Patents
Extraction of curcumin of the components of turmeric Download PDFInfo
- Publication number
- KR20170087176A KR20170087176A KR1020160006858A KR20160006858A KR20170087176A KR 20170087176 A KR20170087176 A KR 20170087176A KR 1020160006858 A KR1020160006858 A KR 1020160006858A KR 20160006858 A KR20160006858 A KR 20160006858A KR 20170087176 A KR20170087176 A KR 20170087176A
- Authority
- KR
- South Korea
- Prior art keywords
- turmeric
- extract
- hot water
- curcumin
- present
- Prior art date
Links
- VFLDPWHFBUODDF-FCXRPNKRSA-N curcumin Chemical compound C1=C(O)C(OC)=CC(\C=C\C(=O)CC(=O)\C=C\C=2C=C(OC)C(O)=CC=2)=C1 VFLDPWHFBUODDF-FCXRPNKRSA-N 0.000 title claims abstract description 77
- VFLDPWHFBUODDF-UHFFFAOYSA-N diferuloylmethane Natural products C1=C(O)C(OC)=CC(C=CC(=O)CC(=O)C=CC=2C=C(OC)C(O)=CC=2)=C1 VFLDPWHFBUODDF-UHFFFAOYSA-N 0.000 title claims abstract description 38
- 229940109262 curcumin Drugs 0.000 title claims abstract description 37
- 235000012754 curcumin Nutrition 0.000 title claims abstract description 37
- 239000004148 curcumin Substances 0.000 title claims abstract description 37
- 235000003373 curcuma longa Nutrition 0.000 title claims description 38
- 235000003392 Curcuma domestica Nutrition 0.000 title claims description 36
- 235000013976 turmeric Nutrition 0.000 title claims description 36
- 238000000605 extraction Methods 0.000 title description 6
- 244000008991 Curcuma longa Species 0.000 title 1
- 235000020240 turmeric extract Nutrition 0.000 claims abstract description 44
- 229940052016 turmeric extract Drugs 0.000 claims abstract description 43
- 239000008513 turmeric extract Substances 0.000 claims abstract description 43
- 238000000034 method Methods 0.000 claims abstract description 36
- 235000013305 food Nutrition 0.000 claims abstract description 25
- 239000000203 mixture Substances 0.000 claims abstract description 17
- 239000004480 active ingredient Substances 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 69
- 239000000284 extract Substances 0.000 claims description 54
- 244000163122 Curcuma domestica Species 0.000 claims description 41
- 238000003809 water extraction Methods 0.000 claims description 21
- 235000013372 meat Nutrition 0.000 claims description 19
- 235000015277 pork Nutrition 0.000 claims description 18
- 238000010298 pulverizing process Methods 0.000 claims description 9
- 238000005406 washing Methods 0.000 claims description 7
- 241000287828 Gallus gallus Species 0.000 claims description 4
- 241000779819 Syncarpia glomulifera Species 0.000 claims description 4
- 235000015278 beef Nutrition 0.000 claims description 4
- 235000013330 chicken meat Nutrition 0.000 claims description 4
- 239000001739 pinus spp. Substances 0.000 claims description 4
- 229940036248 turpentine Drugs 0.000 claims description 4
- 235000009075 Cucumis anguria Nutrition 0.000 claims description 2
- 240000008067 Cucumis sativus Species 0.000 claims description 2
- 235000010799 Cucumis sativus var sativus Nutrition 0.000 claims description 2
- 238000003860 storage Methods 0.000 abstract description 24
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract description 14
- 238000004519 manufacturing process Methods 0.000 abstract description 10
- 229910052757 nitrogen Inorganic materials 0.000 abstract description 7
- 244000005700 microbiome Species 0.000 abstract description 4
- 238000011282 treatment Methods 0.000 description 22
- RVBUGGBMJDPOST-UHFFFAOYSA-N 2-thiobarbituric acid Chemical compound O=C1CC(=O)NC(=S)N1 RVBUGGBMJDPOST-UHFFFAOYSA-N 0.000 description 12
- 244000046052 Phaseolus vulgaris Species 0.000 description 10
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 10
- 239000000523 sample Substances 0.000 description 10
- 240000008574 Capsicum frutescens Species 0.000 description 9
- 235000002568 Capsicum frutescens Nutrition 0.000 description 9
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 9
- 239000000047 product Substances 0.000 description 8
- 235000002566 Capsicum Nutrition 0.000 description 6
- 239000006002 Pepper Substances 0.000 description 6
- 241000722363 Piper Species 0.000 description 6
- 235000016761 Piper aduncum Nutrition 0.000 description 6
- 235000017804 Piper guineense Nutrition 0.000 description 6
- 235000008184 Piper nigrum Nutrition 0.000 description 6
- 235000019197 fats Nutrition 0.000 description 6
- 239000011888 foil Substances 0.000 description 6
- 239000000654 additive Substances 0.000 description 5
- 238000004458 analytical method Methods 0.000 description 5
- 238000002474 experimental method Methods 0.000 description 5
- 150000003839 salts Chemical class 0.000 description 5
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 description 4
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 4
- 239000012153 distilled water Substances 0.000 description 4
- 239000004615 ingredient Substances 0.000 description 4
- 230000000813 microbial effect Effects 0.000 description 4
- 238000003359 percent control normalization Methods 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- 235000014375 Curcuma Nutrition 0.000 description 3
- 241000254158 Lampyridae Species 0.000 description 3
- WSMYVTOQOOLQHP-UHFFFAOYSA-N Malondialdehyde Chemical compound O=CCC=O WSMYVTOQOOLQHP-UHFFFAOYSA-N 0.000 description 3
- 238000011534 incubation Methods 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 238000005303 weighing Methods 0.000 description 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 2
- 244000273928 Zingiber officinale Species 0.000 description 2
- 235000006886 Zingiber officinale Nutrition 0.000 description 2
- 238000002835 absorbance Methods 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- 230000001093 anti-cancer Effects 0.000 description 2
- 230000003110 anti-inflammatory effect Effects 0.000 description 2
- CUFNKYGDVFVPHO-UHFFFAOYSA-N azulene Chemical compound C1=CC=CC2=CC=CC2=C1 CUFNKYGDVFVPHO-UHFFFAOYSA-N 0.000 description 2
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 2
- 239000004327 boric acid Substances 0.000 description 2
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 2
- 239000000706 filtrate Substances 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 235000008397 ginger Nutrition 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- VLTRZXGMWDSKGL-UHFFFAOYSA-N perchloric acid Chemical compound OCl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-N 0.000 description 2
- 239000001967 plate count agar Substances 0.000 description 2
- 241001550224 Apha Species 0.000 description 1
- FRPHFZCDPYBUAU-UHFFFAOYSA-N Bromocresolgreen Chemical compound CC1=C(Br)C(O)=C(Br)C=C1C1(C=2C(=C(Br)C(O)=C(Br)C=2)C)C2=CC=CC=C2S(=O)(=O)O1 FRPHFZCDPYBUAU-UHFFFAOYSA-N 0.000 description 1
- 235000019750 Crude protein Nutrition 0.000 description 1
- 206010013911 Dysgeusia Diseases 0.000 description 1
- 208000005171 Dysmenorrhea Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241000134253 Lanka Species 0.000 description 1
- 239000001888 Peptone Substances 0.000 description 1
- 108010080698 Peptones Proteins 0.000 description 1
- 206010037660 Pyrexia Diseases 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 241000270666 Testudines Species 0.000 description 1
- ZMIQNSSHYBJKIL-UHFFFAOYSA-N Tumerone Chemical compound CC(C)=CC(=O)CC(C)C1=CC=C(C)CC1 ZMIQNSSHYBJKIL-UHFFFAOYSA-N 0.000 description 1
- 240000008042 Zea mays Species 0.000 description 1
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 1
- 241000234299 Zingiberaceae Species 0.000 description 1
- 239000002671 adjuvant Substances 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000002790 anti-mutagenic effect Effects 0.000 description 1
- 230000000259 anti-tumor effect Effects 0.000 description 1
- 230000000840 anti-viral effect Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- XOCANRBEOZQNAQ-KGLIPLIRSA-N ar-turmerone Natural products C[C@H](CC(=O)C=C(C)C)[C@@H]1CC=C(C)C=C1 XOCANRBEOZQNAQ-KGLIPLIRSA-N 0.000 description 1
- 230000000711 cancerogenic effect Effects 0.000 description 1
- 231100000357 carcinogen Toxicity 0.000 description 1
- 239000003183 carcinogenic agent Substances 0.000 description 1
- 235000005822 corn Nutrition 0.000 description 1
- 239000002285 corn oil Substances 0.000 description 1
- 235000005687 corn oil Nutrition 0.000 description 1
- 235000019784 crude fat Nutrition 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 230000037213 diet Effects 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 239000012470 diluted sample Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000009313 farming Methods 0.000 description 1
- 210000003195 fascia Anatomy 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 229930003935 flavonoid Natural products 0.000 description 1
- 150000002215 flavonoids Chemical class 0.000 description 1
- 235000017173 flavonoids Nutrition 0.000 description 1
- 238000004108 freeze drying Methods 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000004128 high performance liquid chromatography Methods 0.000 description 1
- 235000013622 meat product Nutrition 0.000 description 1
- 239000002609 medium Substances 0.000 description 1
- CEQFOVLGLXCDCX-WUKNDPDISA-N methyl red Chemical compound C1=CC(N(C)C)=CC=C1\N=N\C1=CC=CC=C1C(O)=O CEQFOVLGLXCDCX-WUKNDPDISA-N 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 229940124595 oriental medicine Drugs 0.000 description 1
- 239000008188 pellet Substances 0.000 description 1
- 229940116257 pepper extract Drugs 0.000 description 1
- 235000019319 peptone Nutrition 0.000 description 1
- 230000001766 physiological effect Effects 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 238000013207 serial dilution Methods 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 235000011149 sulphuric acid Nutrition 0.000 description 1
- 230000007306 turnover Effects 0.000 description 1
- 238000009461 vacuum packaging Methods 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
- 239000001841 zingiber officinale Substances 0.000 description 1
Images
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B4/00—General methods for preserving meat, sausages, fish or fish products
- A23B4/14—Preserving with chemicals not covered by groups A23B4/02 or A23B4/12
- A23B4/18—Preserving with chemicals not covered by groups A23B4/02 or A23B4/12 in the form of liquids or solids
- A23B4/20—Organic compounds; Microorganisms; Enzymes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3463—Organic compounds; Microorganisms; Enzymes
- A23L3/3472—Compounds of undetermined constitution obtained from animals or plants
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2200/00—Function of food ingredients
- A23V2200/30—Foods, ingredients or supplements having a functional effect on health
- A23V2200/308—Foods, ingredients or supplements having a functional effect on health having an effect on cancer prevention
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2200/00—Function of food ingredients
- A23V2200/30—Foods, ingredients or supplements having a functional effect on health
- A23V2200/3262—Foods, ingredients or supplements having a functional effect on health having an effect on blood cholesterol
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2250/00—Food ingredients
- A23V2250/20—Natural extracts
- A23V2250/21—Plant extracts
- A23V2250/2112—Curcumin, turmeric
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2250/00—Food ingredients
- A23V2250/20—Natural extracts
- A23V2250/21—Plant extracts
- A23V2250/2116—Flavonoids, isoflavones
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2250/00—Food ingredients
- A23V2250/50—Polysaccharides, gums
- A23V2250/51—Polysaccharide
- A23V2250/5118—Starch
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/10—Drying, dehydrating
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/14—Extraction
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/31—Mechanical treatment
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/38—Multiple-step
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Polymers & Plastics (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Food Science & Technology (AREA)
- Microbiology (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Botany (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention relates to a method for producing a turmeric extract containing a large amount of curcumin, more particularly to a method for producing a curcumin-containing turmeric extract, a food composition for improving shelf life comprising a turmeric extract as an active ingredient, and a method for improving the shelf- will be. The method of the present invention for producing a turmeric extract can produce a turmeric extract containing a large amount of curcumin as an active ingredient through a comparatively simple and safe process. The turmeric extract prepared through the above process, when applied to foods, The storage stability can be greatly improved by effectively lowering the fat acidity, volatile basic nitrogen and total microorganisms.
Description
The present invention relates to a method for producing a turmeric extract containing a large amount of curcumin, more particularly to a method for producing a curcumin-containing turmeric extract, a food composition for improving shelf life comprising a turmeric extract as an active ingredient, and a method for improving the shelf- will be.
Curcuma longa (薑黄) is a dried perennial root of Curcuma longa L., a perennial herbaceous ginger belonging to the ginger family. It has a bad taste, It has been known that there is an efficacy of a fever (血血 行 气) and a menstrual pain (通 经 止痛).
Curcumin contains 1 ~ 3% of curcumin, 1 ~ 5% of essential oil and 30 ~ 40% of starch, and curcumin is the main component of yellow crab. In addition, it contains various ingredients such as ρ-methydollrucabinole, tumerone, azulene, campfa flavonoid, and plant fiber.
Curcumin [1,7 - bis - (4 - hydroxy - 3 - methoxyphenyl) - 1,6 - heptadiene - 3, 5 - dione] is a yellowish substance of turmeric which is anti - inflammatory and anti - Many studies have been published as it has been found to be effective.
Curcumin has been used for a long period of time in diets, especially in India for centuries. In India, it has been reported that 60 to 100 milligrams of curcumin are ingested per day, and there is no reported side effect when an adult takes 8,000 milligrams of curcumin for three months per day.
Such curcumin is known to be a pharmaceutically useful ingredient such as anticancer, antimutagenic, anti-tumor, and the like which reduce cholesterol level and inhibit carcinogen. Antioxidant, anti-cancer, anti-inflammatory, antiviral etc. are reported.
On the other hand, in the conventional extraction method of curcumin in curcuma, the solvent extraction method has a problem in that residual wastes and organic solvent remain after extraction, and curcumin extraction efficiency is low.
Accordingly, the present inventor has developed a method of manufacturing a turmeric extract containing curcumin at a high efficiency through a relatively simple method, and a method of improving the quality characteristics of meat by applying the turmeric extract prepared by the above method to meat, The present inventors completed the present invention by confirming that the extract of turmeric which is produced by the production method of the present invention contains a large amount of curcumin and that the preservation of meat is improved when the turmeric extract is processed into meat.
Therefore, an object of the present invention is to provide a method for producing a turmeric extract containing curcumin in a high content.
It is still another object of the present invention to provide a composition for improving shelf-life of a food containing a turmeric extract as an active ingredient.
It is still another object of the present invention to provide a method for improving the storage stability of meat using a turmeric extract.
In order to achieve the above-mentioned object of the present invention,
The present invention relates to a process for the preparation of i) a step for washing turmeric; Ii) pulverizing the washed turmeric; Iii) hot water extraction of the crushed powdered product; Iv) concentrating the hot water extract of turmeric; And v) lyophilizing and pulverizing the concentrated turmeric hot-water extract to obtain a curcumin-containing turmeric extract.
In one embodiment of the present invention, the step iii) is a step of adding water to the pulverized sulfurized product and performing hot water extraction at 75-85 ° C for 1 hour.
The In one embodiment, step iv) is a step of concentrating the hydrothermal extract of turmeric at 145-155 ° C under a pressure of 15-30 mbar using a rotary condenser.
In one embodiment of the present invention, The step (v) is a step of lyophilizing the concentrated hydrous gherkin hot water extract at 5 to 15 Pa, -50 to 60 ° C for 70 to 80 hours, and then pulverizing.
The present invention also provides a food composition for improving shelf-life, comprising a turmeric extract as an active ingredient.
In one embodiment of the present invention, the turmeric extract may be contained in an amount of 10-90 parts by weight based on 100 parts by weight of the composition.
The present invention also provides a method for improving the shelf life of meat, comprising the step of treating the turpentine extract with meat.
In one embodiment of the present invention, the meat may be pork, beef or chicken.
The method of the present invention for producing a turmeric extract can produce a turmeric extract containing a large amount of curcumin as an active ingredient through a comparatively simple and safe process. The turmeric extract prepared through the above process, when applied to foods, The storage stability can be greatly improved by effectively lowering the fat acidity, volatile basic nitrogen and total microorganisms.
FIG. 1A is a schematic view illustrating a process for producing a hot water extract of turmeric according to the present invention, and FIG. 1B is a schematic diagram for schematically illustrating a process for producing a hot water extract of turmeric hot water according to the present invention.
FIGS. 2A to 2H are photographs showing the preparation process of the hot pepper hot water extract and hot water extract foil according to the present invention in detail.
The present invention provides a method for producing a turmeric extract containing a large amount of curcumin.
'Gyulhwang' belongs to Zingiber Officinale Roscoe and its scientific name is Curcuma longa Linne . It is originated from Indian continent and cultivated in southern China, Taiwan, Southeast Asia Thailand, Sri Lanka, Indonesia, Philippines, Vietnam, North America and Central and South America . Curcumin is used not only for edible but also for oriental medicine because of curcumin.
The inventors of the present invention have developed a method for producing a turmeric extract containing a large amount of curcumin by a relatively simple and safe process and found that when the thus prepared turmeric extract is treated with a certain amount of pork loin in a pork loin, the fatty acid turnover, volatile basic nitrogen and total It was confirmed that the storage stability can be greatly improved by effectively lowering the number of microorganisms.
In detail, the present invention relates to a process for the production of iron oxide, comprising the steps of: i) washing the sulfur dioxide; Ii) pulverizing the washed turmeric; Iii) hot water extraction of the crushed powdered product; Iv) concentrating the hot water extract of turmeric; And v) lyophilizing and pulverizing the concentrated hot pepper hot water extract to obtain a curcumin-containing turmeric extract.
The turmeric of the present invention can generally be commercially available turmeric. In the following examples, Jindo turmeric, superior turmeric and golden agricultural turmeric were used.
The step (i) of the present invention is a step of washing the sulfuric acid, which is a step of washing the prepared sulfuric acid several times with flowing water to remove foreign matter. In the following examples of the present invention, after washing the turmeric, dehydration was carried out.
The step (ii) of the present invention is a step of crushing the washed sulfur dioxide. In the following examples, the crushed powder is crushed by using a hood mixer (Hanil Electric Co., Ltd., HMF-3160S).
The step iii) of the present invention is a step of hydrothermally extracting the crushed sulfurized product. More specifically, water can be added to the crushed sulfurized product and the hot extraction can be conducted at 75-85 ° C for 1 hour. In the following examples, (SHAKING WATER BATH SW-90MW, JEIO TECH) at 80 ° C for 1 hour.
The step iv) of the present invention is a step of concentrating the hot water extract of turmeric, more specifically, the hot water extract of turmeric can be concentrated under a pressure of 15 to 30 mbar at 145-155 ° C using a rotary concentrator, The ganghwang hot-water extract was concentrated to 1/10 under a pressure of 15-30 mbar at 150 ° C using a rotary evaporator (Evaporator, product name: EYELA, N-1110).
The step (v) of the present invention is a step of lyophilizing and pulverizing the concentrated hot pepper hot water extract. More specifically, the concentrated hot pepper hot water extract is lyophilized at 5 to 15 Pa, -50 to 60 캜 for 70 to 80 hours In the following examples, the concentrated hot pepper extract was lyophilized at 5 to 15 Pa, -55 ° C for 72 hours, and then pulverized using a firefly.
The turmeric extract prepared through the above process of the present invention can contain curcumin in a concentration of 1700-3010 ppm.
The present invention also provides a food composition for improving shelf-life, comprising a turmeric extract as an active ingredient.
The extract of turmeric of the present invention contains curcumin having various physiological activities at a high concentration of 1700-3010 ppm and thus can be usefully used as a functional material.
In particular, when the corn oil extract of the present invention is processed into meat, the storage stability can be greatly improved by effectively lowering the fat acidity, volatile basic nitrogen and total microorganisms during the storage period, and the composition of the food composition .
The food composition for improving shelf-life comprising the turpentine extract of the present invention as an active ingredient may be used as an adjuvant or an additive to be added to foods, and preferably used as an additive for a source composition applied to meat such as pork, beef or chicken , A preservative, a storage stability improver and the like.
In one embodiment of the present invention, the turmeric extract may be contained in an amount of 10-90 parts by weight based on 100 parts by weight of the composition.
In another embodiment of the present invention, the food composition having improved shelf-life may include other materials that can improve shelf-life in addition to the turmeric extract.
The present invention also provides a method for improving the shelf life of meat, comprising the step of treating the turpentine extract with meat.
In order to improve the shelf life of meat, the content of the turmeric extract may be 0.1-5 parts by weight based on 100 parts by weight of meat, but the range is not particularly limited.
Examples of the meat of the present invention include pork, beef or chicken, but the type of the meat sold on the market is not particularly limited.
Hereinafter, the present invention will be described in more detail with reference to Examples. These examples are for further illustrating the present invention, and the scope of the present invention is not limited to these examples.
< Example 1>
Curcumin Containing Turmeric extract Produce
In this experiment, in order to extract curcumin effectively from turmeric, a turmeric washing process; Milling process; Hot water extraction process; Concentration process; Freeze-drying process; And a powdering process.
In detail, all three types of turmeric sulfur purchased from Table 1 were washed with water, then dehydrated. The dehydrated turmeric was crushed by using a hood mixer (HMF-3160S, Hanil Electric Co., Ltd.), and then 5 liters of water per 1000 g of the crushed sulfurized product was added. The shaking water bath SW-90 MW, JEIO TECH). The hot water extract obtained by filtering the boiled sulfurized crushed water and water was sieved to 1/10 under a pressure of 15 to 30 mbar at 150 ° C using a rotary evaporator (Evaporator, product name: EYELA, N-1110) And concentrated to a level of 10% of the original volume). The concentrated hot-water extract was lyophilized at 5 to 15 Pa, -55 ° C for 72 hours and then pulverized using a firefly. On the other hand, the boiled sulfurized crumbs and the remaining hot water-extracted pellets without water being sieved were separately freeze-dried at 5 to 15 Pa, -55 ° C for 72 hours, and then powdered by using a firefly.
In order to analyze the content of curcumin in the turmeric extract prepared through the above procedure, it was analyzed by HPLC with an internationally recognized testing institute, Korea Polymer Research Institute. As a result, it was confirmed that curcumin was contained in each sample T1-T3 (See Table 2 below).
For reference, the hot water extraction samples (T4 to T6) used in the following experiments were separated to compare the curcumin content with the hot water extract and the quality and storage characteristics when used in meat products.
< Example 2>
Of turmeric extract Pork loin treatment
The pork loin purchased from the butchers in Chungbuk province was removed by fat and fascias, and the mixture was ground to a size of 8 mm in a small size. After the preparation, 0.5 kg of each treatment was prepared. The crude turmeric extract prepared in Example 1, The pepper was mixed at the mixing ratios shown in Table 3 below, vacuum-packed for each treatment, and then used in the experiment after aging for 24 hours in a refrigerator at 4 ° C.
<1-2> Turmeric extract General ingredients, water holding capacity, pH analysis of processed pork loin
In the present experiment, moisture, crude protein, crude fat and ash (%) were measured according to the AOAC method (1990) for general composition analysis of the samples shown in Table 3 above.
The water holding capacity was measured by weighing a 2-ml tube with fine pores according to the method of Laakkonen et al. (1970), weighing exactly 0.5 ± 0.05g of the sample, placing it in a tube, weighing the sample and tube Then, the resultant was heated in a water bath at 80 ° C for 20 minutes and then cooled at room temperature for 10 minutes. After centrifuging at 2,000 rpm at 4 ° C for 10 minutes, the weight was measured and the water holding capacity was determined by the following formula.
The pH was measured by a pH meter (WTW pH 720, Germany) homogenized for 30 seconds with a stomacher (400 lab blender, seward, London, England) with 100 ml of distilled water after collecting 10 g of the sample. The repetition took an average value with 3 iterations.
- Sirloin (pork) 98.5% + Salt 0.4% + Pepper 0.1% + Ganghwangsang hot water extract or Ganghwangsang hot water extract 1%
Control: no additives
T1: Jindo turmeric hot water extract 1%
T2: Superior food Thickened hot water extract 1%
T3: Golden agricultural dried ganghwang bean hot water extract 1%
T4: Jindo cyanide hot water extraction foil 1%
T5: Supercritical food hot water extraction hot pepper 1%
T6: Golden agricultural dried ganjang bean hot water extraction 1%
As shown in Table 4, the water content of all treatments was significantly higher than that of the control, and the T5 treatment showed a significantly higher moisture level than the other treatments. In the case of fat, the treatment with hot water extract was significantly lower than the other treatments. The amount of ash added with hot water extract was significantly lower than that of the control.
- Sirloin (pork) 98.5% + Salt 0.4% + Pepper 0.1% + Ganghwangsang hot water extract or Ganghwangsang hot water extract 1%
Control: no additives
T1: Jindo turmeric hot water extract 1%
T2: Superior food Thickened hot water extract 1%
T3: Golden agricultural dried ganghwang bean hot water extract 1%
T4: Jindo cyanide hot water extraction foil 1%
T5: Supercritical food hot water extraction hot pepper 1%
T6: Golden agricultural dried ganjang bean hot water extraction 1%
As shown in Table 5, the pH was significantly higher at 0 day T6 than at other days of storage, and T4 was significantly lower at 3 days of storage than other treatments. On the 7th day of storage, T5 showed the highest level.
- Sirloin (pork) 98.5% + Salt 0.4% + Pepper 0.1% + Ganghwangsang hot water extract or Ganghwangsang hot water extract 1%
Control: no additives
T1: Jindo turmeric hot water extract 1%
T2: Superior food Thickened hot water extract 1%
T3: Golden agricultural dried ganghwang bean hot water extract 1%
T4: Jindo cyanide hot water extraction foil 1%
T5: Supercritical food hot water extraction hot pepper 1%
T6: Golden agricultural dried ganjang bean hot water extraction 1%
As a result of the water holding capacity analysis, the T3 treatment showed the lowest value as shown in Table 6 above.
<1-3> Turmeric extract Storage characteristics of processed pork loin
During the storage period, TBA, total microbial counts, and volatile basic nitrogen (VBN) were investigated for the storage stability of corn steep liquor. The storage conditions of the experiment were analyzed by vacuum packaging and stored at 4 ℃ for 7 days.
TBA (2-thiobarbituric acid) was slightly modified by Witte et al. (1970) and expressed as 2-thiobarbituric acid (TBA). 15 ml of cold 10% perchloric acid and 25 ml of tertiary distilled water were added to 10 g of sample Homogenize for 10 seconds at 10,000 rpm in a homogenizer. The homogenate was diluted with Whatman No. (DU-650, Beckman, USA) for 5 min. After filtration, 5 ml of filtrate and 5 ml of 0.02 M thiobarbituric acid (TBA) solution were added and mixed thoroughly. Absorbance at a wavelength of < RTI ID = 0.0 > Blank was the third distilled water. TBA values were expressed as mg malonaldehyde (mg malonaldehyde / kg) per 1,000 g of sample. The standard curve used was y = 0.1975x-0.0011 (r = 0.999), and y = absorbance and x = TBA were calculated.
For the volatile basic nitrogen (VBN), 90 ml of distilled water was added to 10 g of the sample using the method of Takasaka (1975) and homogenized at 10,000 rpm for about 30 seconds. 2 filter paper. Add 3 ml of the filtrate into the outer chamber of the Conway unit, add 1 ml of 0.01 N boric acid solution and 3 drops of indicator (0.066% methyl red + 0.066% bromocresol green). Glycerine was applied onto the lid and the lid was closed. 1 ml of 50% K 2 CO 3 was injected into the outer chamber, immediately sealed, and the container was stirred horizontally, followed by incubation at 37 ° C for 120 minutes. After incubation, the boric acid solution of the inner chamber was titrated with 0.02N H2SO4. The value of volatile basic nitrogen (VBN) was expressed in terms of mg (㎎%) per 100g of sample.
VBN = ((a-b) * F * 28.014 * 100) / Amount of sample
- a: Amount of sulfuric acid injected (ml)
- b: Amount of sulfuric acid injected into the blank (ml)
- f: 0.02NH 2 SO 4 standardization index
- 28.014 = 0.02NH 2 SO 4 Amount of N required to consume 1 ml
On the other hand, 90 g of 0.1% peptone solution is added to 10 g of sample using serial dilution method and homogenized for 30 seconds in a stomacher bag. Subsequently, the serially diluted samples were inoculated into PCA (plate count agar) medium and cultured at 37 ° C for 48 hours (APHA, 1992). After the incubation, counts were counted with a colony counter. The unit of total microbial count is expressed as Log cfu / g.
(cfu / g)
- Sirloin (pork) 98.5% + Salt 0.4% + Pepper 0.1% + Ganghwangsang hot water extract or Ganghwangsang hot water extract 1%
Control: no addition
T1: Jindo turmeric hot water extract 1%
T2: Superior food Thickened hot water extract 1%
T3: Golden agricultural dried ganghwang bean hot water extract 1%
T4: Jindo cyanide hot water extraction foil 1%
T5: Supercritical food hot water extraction hot pepper 1%
T6: Golden agricultural dried ganjang bean hot water extraction 1%
As a result, as shown in Table 7, TBA indicating fat licking in the storage characteristics was significantly lower than that of the other treatments at the storage day 0 and TBA value at the storage day 3 Respectively. On day 7 of storage, T1 was the lowest level. The volatile bases indicating protein decay were significantly higher in the control group than in the other treatments, and T2 and T3 were significantly higher on the third day of storage. T4 was significantly higher on the 7th day of storage and T1 was the lowest. Total microbial counts were significantly higher in T6 than in other treatments on day 0, and T2 on day 3 was significantly lower than other treatments. T6 was the highest at 7 days of storage.
The present invention has been described with reference to the preferred embodiments. It will be understood by those skilled in the art that various changes in form and details may be made therein without departing from the spirit and scope of the invention as defined by the appended claims. Therefore, the disclosed embodiments should be considered in an illustrative rather than a restrictive sense. The scope of the present invention is defined by the appended claims rather than by the foregoing description, and all differences within the scope of equivalents thereof should be construed as being included in the present invention.
Claims (8)
Ii) pulverizing the washed turmeric;
Iii) hot water extraction of the crushed powdered product;
Iv) concentrating the hot water extract of turmeric; And
And v) lyophilizing and pulverizing the concentrated turmeric hot-water extract to produce curcumin-containing turmeric extract.
Wherein the step iii) comprises adding water to the crushed sulfurized product, and subjecting the resulting product to hot water extraction at 75-85 DEG C for 1 hour.
Wherein the step (iv) comprises concentrating the extract of turmeric hot water at a temperature of 145 to 155 ° C and a pressure of 15 to 30 mbar using a rotary concentrator.
Wherein the step (v) comprises lyophilizing the concentrated hydrous gherkin hot water extract at 5 to 15 Pa, -50 to 60 < 0 > C for 70 to 80 hours, and pulverizing it.
Wherein the turmeric extract is contained in an amount of 10 to 90 parts by weight based on 100 parts by weight of the composition.
Wherein the meat is pork, beef or chicken.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR1020160006858A KR20170087176A (en) | 2016-01-20 | 2016-01-20 | Extraction of curcumin of the components of turmeric |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR1020160006858A KR20170087176A (en) | 2016-01-20 | 2016-01-20 | Extraction of curcumin of the components of turmeric |
Publications (1)
Publication Number | Publication Date |
---|---|
KR20170087176A true KR20170087176A (en) | 2017-07-28 |
Family
ID=59422218
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1020160006858A KR20170087176A (en) | 2016-01-20 | 2016-01-20 | Extraction of curcumin of the components of turmeric |
Country Status (1)
Country | Link |
---|---|
KR (1) | KR20170087176A (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108047016A (en) * | 2017-12-15 | 2018-05-18 | 河北泽华生物科技有限公司 | A kind of method that bisdemethoxycurcumin is extracted from turmeric |
KR20200069870A (en) | 2018-12-07 | 2020-06-17 | 주식회사 나온스 | Manufacturing method for tumeric extract powders(curcumin) using tumeric and colloidal dispersion solution of curcumin manufactured by the same |
-
2016
- 2016-01-20 KR KR1020160006858A patent/KR20170087176A/en not_active Application Discontinuation
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108047016A (en) * | 2017-12-15 | 2018-05-18 | 河北泽华生物科技有限公司 | A kind of method that bisdemethoxycurcumin is extracted from turmeric |
CN108047016B (en) * | 2017-12-15 | 2021-06-22 | 河北泽华生物科技有限公司 | Method for extracting bisdemethoxycurcumin from turmeric |
KR20200069870A (en) | 2018-12-07 | 2020-06-17 | 주식회사 나온스 | Manufacturing method for tumeric extract powders(curcumin) using tumeric and colloidal dispersion solution of curcumin manufactured by the same |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN101147564A (en) | Natural plant spice with antibacterial effect and preparation method thereof | |
KR101698165B1 (en) | Natural coloring material is curing sausage production method and its composition | |
KR100774498B1 (en) | Producing method for aging-fermentation black garlic using artemisia fumigation | |
KR20100104116A (en) | Smoking sauce for duck meat and manufacturing method smoked duck meat | |
KR101373252B1 (en) | Process for Preparing Fermented Power Tea from Unpolished Rice and Guava Leaves | |
KR20100037782A (en) | Method for producing soybean paste containing scutellariae radix, korean beef and seafoods and the soybean paste produced by the same | |
CN105285924A (en) | Antioxidative flavor chilli sauce and preparation method thereof | |
KR20170087176A (en) | Extraction of curcumin of the components of turmeric | |
KR101819794B1 (en) | Method of manufacturing beef jerky containing natural antioxidant | |
KR101824165B1 (en) | Pickled hizikia fusiformis | |
KR102487459B1 (en) | Manufacturing method of health food having antioxidant activity containing fermented polygonum multiflorum complex extracts and the health food having antioxidant activity thereby | |
KR101816602B1 (en) | method of drying for good antioxidant effect of Cirsium setidens | |
KR101187438B1 (en) | Red pepper paste using Yacon and manufacturing method functional Yacon seasoned with soy sauce | |
KR101212308B1 (en) | Manufacturing method of Lentinus edodes beverage enhanced fragrance | |
KR101808935B1 (en) | Head cheese comprising of turmeric and method for preparing thereof | |
KR101617043B1 (en) | Method of preparing noodles having process suitability and containing berries and extraction of green tea by subcritical speed extraction, and noodles use thereof | |
KR101220483B1 (en) | Seasoned laver using Eriobotrya japonica and its method | |
KR102660383B1 (en) | manufacturing method of scorched rice using curcuma and kimchi | |
KR102285301B1 (en) | Method for producing functional Gochujang Gulbi sauce using Cudrania tricuspidata and medicinal herb | |
KR101373497B1 (en) | A method for preparing the salted changran jeot using by sea mustard oil | |
KR101470993B1 (en) | Perilla frutescens (L.) Britton var. acuta (Thunb.) Kudo Tea, Method for Preparing the Same, Beverage Composition Comprising Perilla frutescens (L.) Britton var. acuta (Thunb.) Kudo Extract, and Method for Preparing the Same | |
KR20120070990A (en) | Manufacturing method of pills comprising opuntia humifusa | |
KR20180007555A (en) | Boneless pettitoes with grape pomace and manufacturing method thereof | |
KR101670813B1 (en) | A method for manufacturing of five-color powder product using anti-oxidant materials, and the five-color powder product manufactured by the method | |
KR101569667B1 (en) | Food stench removal agent using ingredient of Pine Nut Shell and method for preparing the same |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
A201 | Request for examination | ||
E902 | Notification of reason for refusal | ||
E601 | Decision to refuse application |