KR20170085366A - A composite of natural antibiosis abstergent by using sintered cockle shell powder and manufactoring methods thereof - Google Patents
A composite of natural antibiosis abstergent by using sintered cockle shell powder and manufactoring methods thereof Download PDFInfo
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- KR20170085366A KR20170085366A KR1020160004903A KR20160004903A KR20170085366A KR 20170085366 A KR20170085366 A KR 20170085366A KR 1020160004903 A KR1020160004903 A KR 1020160004903A KR 20160004903 A KR20160004903 A KR 20160004903A KR 20170085366 A KR20170085366 A KR 20170085366A
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- shell
- powder
- calcined
- present
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/02—Inorganic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/02—Inorganic compounds
- C11D7/04—Water-soluble compounds
- C11D7/10—Salts
- C11D7/12—Carbonates bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/26—Organic compounds containing oxygen
- C11D7/265—Carboxylic acids or salts thereof
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Detergent Compositions (AREA)
Abstract
The present invention relates to a natural antimicrobial detergent composition using a calcined shellfish powder and a method for producing the same, and more particularly, to an antimicrobial detergent composition prepared by adding a calcined shellfish powder and citric acid or sodium percarbonate to an environmentally- The present invention also provides a water-soluble natural antimicrobial detergent composition and a method for producing the same, which are capable of improving the antibacterial performance and washing performance of a water-soluble natural antimicrobial detergent composition which is harmless to the human body and has no side effects and is harmless to the human body.
Description
More particularly, the present invention relates to a natural antimicrobial cleanser composition using a crustacean crumbly fired powder, and more particularly, to a method for producing a natural antimicrobial cleanser composition using a crumbly crust, To a water-soluble natural antimicrobial detergent composition and a method for producing the same, wherein the antimicrobial agent has no adverse effect compared to the antimicrobial agent and is harmless to the human body but can be improved in antibacterial activity compared to the conventional antimicrobial agent having only the calcined shell powder.
Today, due to global environmental changes such as global warming, human beings are exposed to indiscriminate attacks of new pathogens such as new influenza, which have not been dealt with so far. Moreover, as international exchanges are frequent here, the infectious disease infection rate rapidly crosses the continent, The range is spreading globally.
The most convenient way to prevent the propagation of pathogens at the general citizen level during the war against viruses and germs is to clean and clean various articles such as hands and germs, especially the propagation medium of human body parts.
Therefore, although the antimicrobial composition for the purpose of washing hands or cleaning various articles is sold in the market as described above, most of them are chemically synthesized and produced, and many side effects have occurred.
In order to prevent the above-mentioned side effects, various shells such as petiels, abalone, oyster, shellfish, scallop shellfish, pearl shellfish, pearl mussel, and shellfish have been recently recycled for antibacterial purposes Are being developed.
As a related prior art, Korean Patent Laid-Open No. 10-2008-0080317 discloses a method for producing a pulverized product by washing, crushing, crushing and crushing a shell at low temperature in a non-oxidizing atmosphere at a low temperature of 500 to 600 캜, An antifungal and antimicrobial agent consisting of a calcined shell powder having a mean particle diameter of not more than 40 mu m, which is then calcined at 900 DEG C again and finely pulverized.
Korean Patent Laid-Open No. 10-2002-0011412 discloses an antibacterial agent obtained by baking shellfish shell powder of Hambak shells as a raw material and firing the shell shell powder at an ultimate temperature of 700 to 2500 ° C in an inert gas atmosphere. .
Korean Patent Laid-Open No. 10-2008-0069884 discloses an antiviral agent containing a micro-calcined pulverized product obtained by roughly crushing and crushing shell or shell.
Korean Patent Laid-Open No. 10-2009-0054314 discloses a skin fungal therapeutic agent obtained by heating scallop shells at a temperature of 1,200 to 1,300 DEG C for 3 to 4 hours and pulverizing to a size of 50 to 900 nm.
Korean Patent Laid-Open No. 10-2009-0065820 discloses a harmful substance remover which burns and crushes a shellfish twice and mixes a diatomaceous earth component and a germanium component in an appropriate amount.
Korean Patent No. 10-1078163 discloses an anti-controlling agent containing calcined calcium as an active ingredient obtained by baking the shell.
That is, the above prior arts are techniques for obtaining a calcined powder mainly composed of burnt lime by calcining and crushing the shell, and using it as various compositions for antibacterial purposes.
However, it is a certain theory that the quicklime which is the main ingredient for the antibacterial and washing function has a function of antibacterial function to remove microorganisms and pathogens as strong alkaline properties, but the antibacterial characteristics are different according to the content of quicklime and crystal form.
In addition, the quicklime has a function of sterilization, but it is also a problem of the above-mentioned technology that sterilized pathogens or microorganisms can not be completely removed and remain on the surface.
It is an object of the present invention to solve the above problems and to provide a water-soluble antimicrobial composition by adding a calcined shell powder and citric acid or sodium percarbonate to a water-soluble antimicrobial composition, which has no side effects, harmless to human body It is an object of the present invention to provide a water-soluble natural antimicrobial detergent composition and a method for producing the same, which are capable of improving its antibacterial activity compared with antimicrobial agents composed of only calcined shell powder.
The present invention relates to a natural antimicrobial detergent composition and a method for producing the same,
Cleanly washing the shell shell; Calcining the washed shell at a temperature in the range of 900 to 1200 DEG C for 60 to 120 minutes; Pulverizing the calcined shellfish powder and collecting it in a size range of 0.1 to 0.5 mu m; Mixing the pulverized crust with calcined powder with water; There is provided a method for producing a natural antimicrobial detergent using a crumb shell calcined powder, which comprises mixing citric acid or sodium percarbonate with a mixture of calcined powder and water,
Mixing 91 to 99% by weight of a mixture of crumb shell firing powder mixture with 1 to 15% by weight of crumb shell firing powder in the range of 0.1 to 0.5 占 퐉 and 85 to 99% by weight of clean water and 1 to 9% by weight of citric acid or sodium percarbonate The present invention also provides a natural antimicrobial detergent composition using the calcined shell powder.
The present invention relates to a water-soluble antimicrobial detergent composition prepared by adding a water-soluble antimicrobial composition and a microbial-derived enzyme to a body part intended for antibacterial or sterilizing purposes, or for washing vegetables, fruits, by doing,
There is no side effect compared to the chemically synthesized antimicrobial agent, and the antimicrobial agent and the washing performance can be improved compared with the antimicrobial agent which is harmless to the human body and composed of only the conventional calcined shell powder.
Also, the natural antimicrobial detergent composition of the present invention is a natural antimicrobial detergent composition, which is produced from natural materials as a raw material, has a high firing process at an elevated temperature and is environmentally friendly, has good human immunity due to use of citric acid or sodium percarbonate which is harmless to human body, .
In addition, the natural antimicrobial detergent composition of the present invention is advantageous in that it is easy to mass-produce and has excellent economical efficiency.
Hereinafter, the antimicrobial detergent composition of the present invention and its preparation method will be described in detail.
In addition, unless otherwise defined, technical terms and scientific terms used in the present invention have the same meaning as commonly understood by one of ordinary skill in the art to which the present invention belongs. In the following description, A description of the known function and configuration that can be blurred is omitted.
Also, units of% used unclearly in the present invention means weight percent.
INDUSTRIAL APPLICABILITY The present invention provides a strong antimicrobial detergent composition as well as an excellent human body harmlessness by using a natural organic calcium oxide component produced by firing of shellfish shell and using citric acid or sodium percarbonate as a washing auxiliary component.
Specifically, the natural organic calcium oxide of the present invention maximizes the sterilizing ability under a strong alkaline condition by using calcium oxide as a main component, which is produced by baking shell shell, shell shell, at 900 to 1200 ° C, and is capable of binding with citric acid or sodium percarbonate There is an advantage that it is possible to minimize the possibility of harmful to human skin caused by strong alkali.
Hereinafter, the natural antimicrobial detergent composition of the present invention will be described in detail.
The present invention provides a natural antimicrobial detergent composition comprising calcium oxide powder, citric acid or sodium percarbonate obtained by calcining shell shell at 900 to 1200 ° C for 60 to 120 minutes.
In one example of the present invention, the calcium oxide powder obtained by calcining the shell shell at 900 to 1200 DEG C for 60 to 120 minutes may mean an organic calcium oxide powder obtained from, for example, natural shellfish.
Generally, when baked at a high temperature, the calcium oxide is produced by a known technique. However, calcium oxide produced at this time has a problem in that crystal sizes are different from each other. Most of known techniques generally use these pulverized powders.
That is, prior art techniques known in the art are techniques for obtaining a calcined powder mainly composed of burnt lime by calcining and crushing the shell, and utilizing the resulting calcined powder as various compositions for antibacterial purposes.
However, it is a certain theory that the quicklime which is the main ingredient for the antibacterial and washing function has a function of antibacterial function to remove microorganisms and pathogens as strong alkaline properties, but the antibacterial characteristics are different according to the content of quicklime and crystal form.
Also, it is a problem of the prior art that the function of sterilization of the quicklime is clearly shown, but sterilized pathogens or microorganisms can not be completely removed and remain on the surface.
However, the natural antimicrobial detergent composition of the present invention can precisely control the calcination conditions of the shell of shellfish and combine the calcined shellfish calcined with fine crystals to citric acid or sodium percarbonate, Can not be completely removed and can remain on the surface.
In one example of the present invention, calcined calcium oxide has a calcination time of 60 minutes to 120 minutes at 900 to 1200 ° C. Since calcium oxide crystals produced by the calcination include a large amount of pores, It is possible to produce calcined shell calcined calcium oxide powder which can exhibit antimicrobial activity.
In one example of the present invention, a mixture of water and calcium carbonate is mixed in the range of 85 to 99% by weight of water and 1 to 15% by weight of crushed calcium carbonate oxide powder. However, this is a preferred example, and the scope of the present invention is not limited thereto.
In one example of the present invention, the natural antimicrobial detergent composition of the present invention may contain 91 to 99% by weight of the mixture of the crustacean crumbly fired powder and 1 to 9% by weight of citric acid or sodium percarbonate.
Generally, the shell cleaning agent has excellent antibacterial activity, but since the sterilized residue after the antibacterial action remains on the surface of the vegetable fruits and the like, it is vulnerable to decay. However, since the above-mentioned citric acid or sodium percarbonate is combined with the component of the present invention of the flaky calcined calcium oxide powder, the sterilized residue after the antibacterial action remains untreated on the surface of the vegetable fruit and the like, can do.
Hereinafter, the present invention will be described in detail with reference to Examples. However, the present invention is described in more detail with reference to the following Examples. However, the scope of the present invention is not limited by the following Examples.
A natural antimicrobial detergent composition was prepared as shown in Table 2 after mixing a mixture of crumb shell calcined calcium oxide powder having the composition ratio shown in Table 1 below.
Specifically, the calcined calcium oxide powder was cleaned and then calcined at 1000 ° C. for 90 minutes. After calcination, the calcined shell was crushed, and the powder having a particle size of 0.3 μm or less was sieved And calcium oxide of size 0.3 μm or less obtained by sieving was used.
To evaluate the antimicrobial activity and the washability, the antibacterial performance evaluation was conducted on broccoli vegetables and apples and tangerines on fruits. The antimicrobial test was carried out by using a portable microorganism or fungus measuring device to measure residual microorganisms or strains.
The procedure of Example 1 was repeated except that the composition ratio was changed according to Table 1.
The procedure of Example 1 was repeated except that the composition ratio was changed according to Table 1.
[Comparative Example 1]
The procedure of Example 1 was repeated except that the composition ratio was changed according to Table 2.
[Comparative Example 2]
The procedure of Example 1 was repeated except that the composition ratio was changed according to Table 2.
Specifically, the experimental results are shown in Table 3.
As a result of the measurement, it was confirmed that all of the antibacterial detergents of the present invention according to Examples 1 to 3 exhibited excellent antibacterial and cleaning performance.
In addition, in the case of Comparative Example 1, it was confirmed that antibacterial performance was significantly lower than that in Examples 1 to 3. In the case of Comparative Example 2 in which sodium percarbonate was not used, it was confirmed that the washing performance was significantly lower than that in Examples 1 to 3.
It will be understood by those skilled in the art that various changes in form and details may be made therein without departing from the spirit and scope of the present invention as defined by the appended claims and their equivalents.
Claims (3)
85 to 99% by weight of water;
91 to 99% by weight of a mixture of the above crustacean shell and calcined powder; And
Citric acid or sodium percarbonate in an amount of 1 to 9% by weight based on the total weight of the detergent composition.
Wherein one or more of citric acid or sodium percarbonate is used as said antifungal agent.
Calcining the washed shell at a temperature in the range of 900 to 1200 DEG C for 60 to 120 minutes;
Crushing the calcined shellfish powder and collecting it in a size range of 0.1 to 0.5 mu m;
Mixing the pulverized calcareous powder with the water; And
And mixing citric acid or sodium percarbonate with the mixture of the calcined powder of crust shell and the water.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1020160004903A KR20170085366A (en) | 2016-01-14 | 2016-01-14 | A composite of natural antibiosis abstergent by using sintered cockle shell powder and manufactoring methods thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1020160004903A KR20170085366A (en) | 2016-01-14 | 2016-01-14 | A composite of natural antibiosis abstergent by using sintered cockle shell powder and manufactoring methods thereof |
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| Publication Number | Publication Date |
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| KR20170085366A true KR20170085366A (en) | 2017-07-24 |
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| Application Number | Title | Priority Date | Filing Date |
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| KR1020160004903A KR20170085366A (en) | 2016-01-14 | 2016-01-14 | A composite of natural antibiosis abstergent by using sintered cockle shell powder and manufactoring methods thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101953189B1 (en) * | 2017-09-04 | 2019-03-04 | 주식회사 케빈오차드 | A solid detergent for fruits and vegetables and a method for manufacturing the same |
| KR20230018266A (en) * | 2021-07-29 | 2023-02-07 | 김민경 | Method for making calcium-ball |
-
2016
- 2016-01-14 KR KR1020160004903A patent/KR20170085366A/en not_active Application Discontinuation
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101953189B1 (en) * | 2017-09-04 | 2019-03-04 | 주식회사 케빈오차드 | A solid detergent for fruits and vegetables and a method for manufacturing the same |
| KR20230018266A (en) * | 2021-07-29 | 2023-02-07 | 김민경 | Method for making calcium-ball |
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